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1. 发明授权

US07771494B2 Process for selective removal of water and impurities from N-(phosphonomethyl)glycine 有权
标题翻译：从N-（膦酰基甲基）甘氨酸中选择性去除水和杂质的方法
公开(公告)号：US07771494B2
公开(公告)日：2010-08-10
申请号：US11669693
申请日：2007-01-31
申请人： Sunder Rangachari , Ed Ries , Eduardo Casanova , Randall Alberts , Todd Friedman , Greg Hartmann
发明人： Sunder Rangachari , Ed Ries , Eduardo Casanova , Randall Alberts , Todd Friedman , Greg Hartmann
IPC分类号： B01D9/00
CPC分类号： C07F9/3813
摘要： Processes for the preparation, concentration and recovery an N-(phosphonomethyl)glycine product from aqueous process streams including contacting mother liquor generated in the precipitation of N-(phosphonomethyl)glycine product crystals with a selective membrane to produce a retentate enriched N-(phosphonomethyl)glycine product and a permeate depleted in N-(phosphonomethyl)glycine product are disclosed.
摘要翻译：从含水工艺流程制备，浓缩和回收N-（膦酰基甲基）甘氨酸产物的方法，包括在N-（膦酰基甲基）甘氨酸产物晶体与选择性膜沉淀中产生的母液接触以产生富集滞留物的N-（膦酰基甲基）甘氨酸产物和耗尽N-（膦酰基甲基）甘氨酸产物的渗透物。

2. 发明申请

US20080178433A1 Process for Selective Removal of Water and Impurities from N-(Phosphonomethyl)Glycine 有权
标题翻译：从N-（膦酰基甲基）甘氨酸中选择性去除水和杂质的方法
公开(公告)号：US20080178433A1
公开(公告)日：2008-07-31
申请号：US11669693
申请日：2007-01-31
申请人： Sunder Rangachari , Ed Ries , Eduardo Casanova , Randall Alberts , Todd Friedman , Greg Hartmann
发明人： Sunder Rangachari , Ed Ries , Eduardo Casanova , Randall Alberts , Todd Friedman , Greg Hartmann
IPC分类号： B01D9/00 , B01D61/38 , C07F9/02
CPC分类号： C07F9/3813
摘要： Processes for the preparation, concentration and recovery an N-(phosphonomethyl)glycine product from aqueous process streams including contacting mother liquor generated in the precipitation of N-(phosphonomethyl)glycine product crystals with a selective membrane to produce a retentate enriched N-(phosphonomethyl)glycine product and a permeate depleted in N-(phosphonomethyl)glycine product are disclosed.
摘要翻译：从含水工艺流程制备，浓缩和回收N-（膦酰基甲基）甘氨酸产物的方法，包括在N-（膦酰基甲基）甘氨酸产物晶体与选择性膜沉淀中产生的母液接触以产生富集滞留物的N-（膦酰基甲基）甘氨酸产物和耗尽N-（膦酰基甲基）甘氨酸产物的渗透物。

3. 发明申请

US20090259068A1 REACTION SYSTEMS FOR MAKING N-(PHOSPHONOMETHYL) GLYCINE COMPOUNDS 审中-公开
标题翻译：制备N-（膦酰基）乙酰化合物的反应体系
公开(公告)号：US20090259068A1
公开(公告)日：2009-10-15
申请号：US12365507
申请日：2009-02-04
申请人： Eric Haupfear , Jerald D. Heise , Amy L. Jorgenson , Michael Rogers , Henry Chien , Eduardo Casanova , William Hooper , William Scholle , Juan Arhancet , Mark A. Leiber , Kent Wittler , Karen A. Wittler
发明人： Eric Haupfear , Jerald D. Heise , Amy L. Jorgenson , Michael Rogers , Henry Chien , Eduardo Casanova , William Hooper , William Scholle , Juan Arhancet , Mark A. Leiber , Kent Wittler , Karen A. Wittler
IPC分类号： C07F9/38 , B01D1/00 , B01D9/00
CPC分类号： C07F9/3813 , Y02P20/582
摘要： This invention generally relates to liquid phase oxidation processes for making N-(phosphonomethyl)glycine (also known in the agricultural chemical industry as glyphosate) and related compounds. This invention, for example, particularly relates to processes wherein an N-(phosphonomethyl)iminodiacetic acid (NPMIDA) substrate (i.e., N-(phosphonomethyl)iminodiacetic acid, a salt of N-(phosphonomethyl)iminodiacetic acid, or an ester of N-(phosphonomethyl)iminodiacetic acid) is continuously oxidized to form an N-(phosphonomethyl)glycine product (i.e., N-(phosphonomethyl)glycine, a salt of N-(phosphonomethyl)glycine, or an ester of N-(phosphonomethyl)glycine). This invention also, for example, particularly relates to processes wherein an N-(phosphonomethyl)iminodiacetic acid substrate is oxidized to form an N-(phosphonomethyl)glycine product, which, in turn, is crystallized (at least in part) in an adiabatic crystallizer.
摘要翻译：本发明一般涉及制备N-（膦酰基甲基）甘氨酸（农业化学工业中也称为草甘膦）和相关化合物的液相氧化方法。本发明特别涉及N-（膦酰基甲基）亚氨基二乙酸（NPMIDA）底物（即N-（膦酰基甲基）亚氨基二乙酸，N-（膦酰基甲基）亚氨基二乙酸的盐或N - （膦酰基甲基）亚氨基二乙酸）连续氧化形成N-（膦酰基甲基）甘氨酸产物（即N-（膦酰基甲基）甘氨酸，N-（膦酰基甲基）甘氨酸的盐或N-（膦酰基甲基）甘氨酸的酯）。本发明还特别涉及其中N-（膦酰基甲基）亚氨基二乙酸底物被氧化以形成N-（膦酰基甲基）甘氨酸产物的方法，其反过来在绝热中结晶（至少部分地）结晶器。

4. 发明申请

US20070037708A1 Mitigating necrosis in transgenic glyphosate-tolerant cotton plants treated with herbicidal glyphosate formulations 有权
标题翻译：用除草草甘膦制剂处理的转基因草甘膦耐受棉花植物减轻坏死
公开(公告)号：US20070037708A1
公开(公告)日：2007-02-15
申请号：US11368344
申请日：2006-03-03
申请人： Stephen Prosch , Michael Seitz , Eric Haupfear , Eduardo Casanova , Peter Rogers , David Eaton , David Becher
发明人： Stephen Prosch , Michael Seitz , Eric Haupfear , Eduardo Casanova , Peter Rogers , David Eaton , David Becher
IPC分类号： A01N57/18
CPC分类号： A01N25/32 , A01N57/20 , A01N25/00 , A01N2300/00
摘要： This invention relates generally to improved methods and herbicidal glyphosate compositions for use in controlling the growth of weeds and unwanted vegetation, and particularly for use in controlling weeds in a crop of transgenic glyphosate-tolerant cotton plants by over-the-top, foliar application of a herbicidal glyphosate formulation.
摘要翻译：本发明一般涉及用于控制杂草和不想要的植物生长的改进方法和除草草甘膦组合物，特别是用于控制转基因草甘膦耐受性棉花植物中的杂草，通过顶部，叶面施用除草草甘膦制剂。

5. 发明授权

US08129564B2 Mitigating necrosis in transgenic glyphosate-tolerant cotton plants treated with herbicidal glyphosate formulations 有权
标题翻译：用除草草甘膦制剂处理的转基因草甘膦耐受棉花植物减轻坏死
公开(公告)号：US08129564B2
公开(公告)日：2012-03-06
申请号：US11368344
申请日：2006-03-03
申请人： Stephen D. Prosch , Michael E. Seitz , Eric A. Haupfear , Eduardo Casanova , Peter E. Rogers , David R. Eaton , David Z. Becher
发明人： Stephen D. Prosch , Michael E. Seitz , Eric A. Haupfear , Eduardo Casanova , Peter E. Rogers , David R. Eaton , David Z. Becher
IPC分类号： C07F9/22 , C07C205/00 , A01N57/00
CPC分类号： A01N25/32 , A01N57/20 , A01N25/00 , A01N2300/00
摘要： This invention relates generally to improved methods and herbicidal glyphosate compositions for use in controlling the growth of weeds and unwanted vegetation, and particularly for use in controlling weeds in a crop of transgenic glyphosate-tolerant cotton plants by over-the-top, foliar application of a herbicidal glyphosate formulation.
摘要翻译：本发明一般涉及用于控制杂草和不想要的植物生长的改进方法和除草草甘膦组合物，特别是用于控制转基因草甘膦耐受性棉花植物中的杂草，通过顶部，叶面施用除草草甘膦制剂。

6. 发明申请

US20060079712A1 Reaction systems for making N-(phosphonomethyl) glycine compounds 有权
公开(公告)号：US20060079712A1
公开(公告)日：2006-04-13
申请号：US11285721
申请日：2005-11-22
申请人： Eric Haupfear , Jerald Heise , Amy Jorgenson , Michael Rogers , Henry Chien , Eduardo Casanova , William Hooper , William Scholle , Juan Arhancet , Mark Leiber , Kent Wittler , Karen Wittler
发明人： Eric Haupfear , Jerald Heise , Amy Jorgenson , Michael Rogers , Henry Chien , Eduardo Casanova , William Hooper , William Scholle , Juan Arhancet , Mark Leiber , Kent Wittler , Karen Wittler
IPC分类号： C07F9/38
CPC分类号： C07F9/3813 , Y02P20/582
摘要： This invention generally relates to liquid phase oxidation processes for making N-(phosphonomethyl)glycine (also known in the agricultural chemical industry as glyphosate) and related compounds. This invention, for example, particularly relates to processes wherein an N-(phosphonomethyl)iminodiacetic acid (NPMIDA) substrate (i.e., N-(phosphonomethyl)iminodiacetic acid, a salt of N-(phosphonomethyl)iminodiacetic acid, or an ester of N-(phosphonomethyl)iminodiacetic acid) is continuously oxidized to form an N-(phosphonomethyl)glycine product (i.e., N-(phosphonomethyl)glycine, a salt of N-(phosphonomethyl)glycine, or an ester of N-(phosphonomethyl)glycine). This invention also, for example, particularly relates to processes wherein an N-(phosphonomethyl)iminodiacetic acid substrate is oxidized to form an N-(phosphonomethyl)glycine product, which, in turn, is crystallized (at least in part) in an adiabatic crystallizer.

7. 发明申请

US20050059840A1 Process for recovering a crystalline product from solution 有权
标题翻译：从溶液中回收结晶产物的方法
公开(公告)号：US20050059840A1
公开(公告)日：2005-03-17
申请号：US10943783
申请日：2004-09-17
申请人： Eric Haupfear , Eduardo Casanova , Kenneth Meyer , Henry Chien
发明人： Eric Haupfear , Eduardo Casanova , Kenneth Meyer , Henry Chien
IPC分类号： C07F9/02 , C07F9/38 , C07F9/22 , C07F9/28
CPC分类号： C07F9/025 , C07F9/3813
摘要： An improved process for recovering a crystalline product (particularly an N-(phosphonomethyl)glycine product) from a solution comprising both a product subject to crystallization and undesired impurities is provided.
摘要翻译：提供了从包含结晶产物和不期望的杂质的溶液中回收结晶产物（特别是N-（膦酰基甲基）甘氨酸产物）的改进方法。

8. 发明授权

US07504534B2 Reaction systems for making N-(phosphonomethyl) glycine compounds 有权
标题翻译：制备N-（膦酰基甲基）甘氨酸化合物的反应体系
公开(公告)号：US07504534B2
公开(公告)日：2009-03-17
申请号：US11285721
申请日：2005-11-22
申请人： Eric A. Haupfear , Henry Chien , Eduardo Casanova , William B. Hooper
发明人： Eric A. Haupfear , Henry Chien , Eduardo Casanova , William B. Hooper
IPC分类号： C07F9/22
CPC分类号： C07F9/3813 , Y02P20/582
摘要： This invention generally relates to liquid phase oxidation processes for making N-(phosphonomethyl)glycine (also known in the agricultural chemical industry as glyphosate) and related compounds. This invention, for example, particularly relates to processes wherein an N-(phosphonomethyl)iminodiacetic acid (NPMIDA) substrate (i.e., N-(phosphonomethyl)iminodiacetic acid, a salt of N-(phosphonomethyl)iminodiacetic acid, or an ester of N-(phosphonomethyl)iminodiacetic acid) is continuously oxidized to form an N-(phosphonomethyl)glycine product (i.e., N-(phosphonomethyl)glycine, a salt of N-(phosphonomethyl)glycine, or an ester of N-(phosphonomethyl)glycine). This invention also, for example, particularly relates to processes wherein an N-(phosphonomethyl)iminodiacetic acid substrate is oxidized to form an N-(phosphonomethyl)glycine product, which, in turn, is crystallized (at least in part) in an adiabatic crystallizer.
摘要翻译：本发明一般涉及制备N-（膦酰基甲基）甘氨酸（农业化学工业中也称为草甘膦）和相关化合物的液相氧化方法。本发明特别涉及N-（膦酰基甲基）亚氨基二乙酸（NPMIDA）底物（即N-（膦酰基甲基）亚氨基二乙酸，N-（膦酰基甲基）亚氨基二乙酸的盐或N - （膦酰基甲基）亚氨基二乙酸）连续氧化形成N-（膦酰基甲基）甘氨酸产物（即N-（膦酰基甲基）甘氨酸，N-（膦酰基甲基）甘氨酸的盐或N-（膦酰基甲基）甘氨酸的酯）。本发明还特别涉及其中N-（膦酰基甲基）亚氨基二乙酸底物被氧化以形成N-（膦酰基甲基）甘氨酸产物的方法，其反过来在绝热中结晶（至少部分地）结晶器。

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