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JP2004257786A Analytical method of platinum-containing compound 有权
标题翻译：含铂化合物的分析方法
公开(公告)号：JP2004257786A
公开(公告)日：2004-09-16
申请号：JP2003047047
申请日：2003-02-25
申请人： Sumitomo Chem Co Ltd , Sumitomo Pharmaceut Co Ltd , 住友化学工業株式会社 , 住友製薬株式会社
发明人： TERADA TOMOYOSHI , SHIMAKURA HITOSHI , KOMURO SETSUKO
IPC分类号： G01N27/62 , B01J20/283 , G01N30/26 , G01N30/34 , G01N30/72 , G01N30/86 , G01N30/88 , G01N30/48
摘要： PROBLEM TO BE SOLVED: To provide an analytical method capable of analyzing a platinum-containing compound included in a biosample with supersensitivity.
SOLUTION: This analytical method of the platinum-containing compound has the following three processes: (1) a first process for applying a pretreatment to a biosample including the platinum-containing compound for serving it to a high-performance liquid chromatography (HPLC) using a reversed phase column, (2) a second process for separating a secondary analytical sample by serving a primary analytical sample prepared in the first process to the high-performance liquid chromatography using the reversed phase column, and (3) a third process for detecting the platinum-containing compound included in the secondary analytical sample as an element specific platinum element by serving the secondary analytical sample separated in the second process to ICP-MS by using argon gas to which oxygen is mixed at the ratio of 1 to 20%(v/v) as a carrier gas.
COPYRIGHT: (C)2004,JPO&NCIPI
摘要翻译：要解决的问题：提供一种能够以超敏性分析包含在生物样品中的含铂化合物的分析方法。含铂化合物的这种分析方法具有以下三个方法：（1）将包含含铂化合物的生物样品在预处理中应用于高效液相色谱法的第一种方法（ HPLC），（2）通过将第一种方法中制备的主要分析样品与使用反相柱的高效液相色谱法分离第二分析样品的第二种方法，和（3）第三种方法通过将以第二种方法分离的第二级分析样品通过使用比例为1的氧气的氩气与ICP-MS进行比较，来检测包含在第二分析样品中的含铂化合物作为元素特定铂元素的方法 20％（v / v）作为载气。版权所有（C）2004，JPO＆NCIPI

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