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1. 发明专利

JPS59155358A 4,5,6,7-tetrahydro-2h-isoindole-1,3-dione derivative, its preparation and herbicide containing said derivative as active component 失效
标题翻译： 4,5,6,7-四氢-2H-异吲哚-1,3-二酮衍生物，其制备和除草剂含有作为活性成分的所述衍生物
公开(公告)号：JPS59155358A
公开(公告)日：1984-09-04
申请号：JP2910883
申请日：1983-02-22
申请人： Sumitomo Chem Co Ltd
发明人： NAGANO HIDEYOSHI , HASHIMOTO SHIYUNICHI , YOSHIDA AKIRA , MATSUMOTO KEIJI , KAMOSHITA KATSUZOU
IPC分类号： C07D209/48 , A01N37/32 , A01N43/38
摘要： NEW MATERIAL:4,5,6,7-Tetrahydro-2H-isoindole-1,3-dione derivative of formula I (R
1 and R
2 are H or methyl; R
3 is lower alkyl).
EXAMPLE: 2-[4-Chloro-2-fluoro-5-(2-ethoxycarbonylvinylene)phenyl]-4,5,6,7-tetrahydro-2H-isoindole-1,3-dione.
USE: A herbicide exhibiting little phytotoxicity to rice plant.
PREPARATION: The objective compound of formula I can be prepared by reacting the aniline derivative of formula II with 3,4,5,6-tetrahydrophthalic anhydride in a solvent at 80°CW the boiling point of the solvent for 1W24hr.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新物质：式I的4,5,6,7-四氢-2H-异吲哚-1,3-二酮衍生物（R1和R2是H或甲基; R3是低级烷基）。实施例：2- [4-氯-2-氟-5-（2-乙氧基羰基亚乙烯基）苯基] -4,5,6,7-四氢-2H-异吲哚-1,3-二酮。用途：对水稻植物具有很小的植物毒性的除草剂。制备：式I的目的化合物可以通过使式II的苯胺衍生物与3,4,5,6-四氢邻苯二甲酸酐在溶剂中在80℃ - 溶剂的沸点反应1-24小时来制备。

2. 发明专利

JPS59118776A 1,6-dihydro-1,2,4-triazine-5(4h)-one derivative, its preparation, and herbicide containing it as active ingredient 失效
标题翻译： 1,6-二氢-1,2,4-三氮杂-5（4H） - 酮衍生物，其制备和除草剂作为活性成分
公开(公告)号：JPS59118776A
公开(公告)日：1984-07-09
申请号：JP23128782
申请日：1982-12-27
申请人： Sumitomo Chem Co Ltd
发明人： MIZUTANI MASATO , SATOU MAKOTO , SANEMITSU MINORU , HASHIMOTO SHIYUNICHI
IPC分类号： C07D253/06 , A01N43/64 , A01N43/707
摘要： NEW MATERIAL:A compound shown by the formula I [R is lower alkyl, or cycloalkyl; R
1 is H, lower alkyl, lower alkenyl, lower alkynyl, or group shown by the formula IIWIII (R
5 and R
6 are H, lower alkyl, halogen, or haloalkyl; R
7 is lower alkyl); R
2 and R
3 are lower alkyl, lower alkenyl, and R
3 is further H, or COR
8 (R
8 is lower alkyl); R
4 is H, or R
3 and R
4 are linked to form group shown by the formula IV (R
9 and R
10 are H, lower alkyl, or phenyl)].
EXAMPLE: 3-Methylthio-4-amino-6-t-butyl-1,6-dihydro-1,2,4-triazin-5(4H)-one.
USE: A herbicide.
PROCESS: A compound shown by the formula V is reacted with a compound shown by the formula R
2 X (X is halogen) to give a compound shown by the formula I (R
1 =R
3 =R
4 =H). Or, a compound shown by the formula VI is reacted with a compound shown by the formula R
11 Y (Y is halogen) to give a compound shown by the formula I (R
1 is not H).
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：由式I表示的化合物[R是低级烷基或环烷基; R 1为H，低级烷基，低级烯基，低级炔基或式II-III所示的基团（R 5和R 6为H，低级烷基，卤素或卤代烷基; R 7为低级烷基）。 R2和R3为低级烷基，低级烯基，R3为H，或COR8（R8为低级烷基）; R 4是H，或者R 3和R 4连接成式IV所示的基团（R 9和R 10是H，低级烷基或苯基）]。实施例：3-甲硫基-4-氨基-6-叔丁基-1,6-二氢-1,2,4-三嗪-5（4H） - 酮。用途：除草剂。方法：将式V所示的化合物与式R2X（X为卤素）所示的化合物反应，得到式I所示的化合物（R1 = R3 = R4 = H）。或者，使式VI所示的化合物与式R 11 Y（Y为卤素）所示的化合物反应，得到式I所示的化合物（R1不为H）。

3. 发明专利

JPS59101404A Herbicidal composition 失效
标题翻译：除草组合物
公开(公告)号：JPS59101404A
公开(公告)日：1984-06-12
申请号：JP21005982
申请日：1982-11-30
申请人： Sumitomo Chem Co Ltd
发明人： HASHIMOTO SHIYUNICHI , YOSHIDA AKIRA
IPC分类号： A01N37/18 , A01N37/32 , A01N47/12
CPC分类号： A01N47/12 , A01N37/32 , A01N37/18 , A01N2300/00
摘要： PURPOSE: A herbicidal composition, prepared by incorporating a specific compound of a selective herbicide for weeds in corn field with "Butylate" (S-ethyl- N,N-diisobutylthiolcarbamate) or "EPTC" (S-ethyl-N,N-di-n-propylthiolcarbamate) or a mixture thereof with an antidotal agent ("R-25788") for the corn, and having synergistically increased effect with reduced phytotoxicity.
CONSTITUTION: A herbicidal composition prepared by incorporating (A) N-(4- chloro-2-fluoro-5-isopropoxyphenyl)-3,4,5,6-tetrahydrophthalimide of the formula useful as a selective herbicide for weeds in corn field with (B) "Butylate" (S- ethyl-N,N-diisopropylthiolcarbamate) or "EPTC" (S-ethyl-N,N-di-n-propylthiolcarbamate) or a mixture thereof with "R-25788" (N,N-diallyl-2,2-dichloroacetamide) in 12:1 weight ratio. The amount of the component (B) is 0.2W60pts.wt., preferably 0.5W20pts.wt. based on one pts. wt. component (A).
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过在玉米田中加入“丁酸”（S-乙基-N，N-二异丁基硫代氨基甲酸酯）或“EPTC”（S-ethyl-N）的杂草选择性除草剂的特定化合物，N-二正丙基硫代氨基甲酸酯）或其与抗肿瘤剂（“R-25788”）的混合物，并具有协同增加的效果，降低了植物毒性。构成：通过将（A）N-（4-氯-2-氟-5-异丙氧基苯基）-3,4,5,6-四氢邻苯二甲酰亚胺掺入可用作玉米田杂草的选择性除草剂的制剂中制备的除草组合物，（B）“丁酸酯”（S-乙基-N，N-二异丙基硫代氨基甲酸酯）或“EPTC”（S-乙基-N，N-二正丙基硫代氨基甲酸酯）或其与“R-25788 “（N，N-二烯丙基-2,2-二氯乙酰胺），其重量比为12:1。组分（B）的量为0.2-60pts.wt。，优选0.5-20pts.wt。基于一个点。重量。组分（A）。

4. 发明专利

JPS5967255A N-phenyltetrahydrophthalamic acid derivative, its preparation and herbicide containing said derivative as active component 失效
标题翻译： N-苯基十一碳二酸衍生物，其制备和除草剂含有作为活性成分的所谓衍生物
公开(公告)号：JPS5967255A
公开(公告)日：1984-04-16
申请号：JP17726082
申请日：1982-10-07
申请人： Sumitomo Chem Co Ltd
发明人： TAKEMOTO KAZUKI , FUKUSHIMA MASAYUKI , NAGANO HIDEYOSHI , YOSHIDA AKIRA , HASHIMOTO SHIYUNICHI
IPC分类号： A01N37/30 , C07C67/00 , C07C231/00 , C07C231/02 , C07C233/60
摘要： NEW MATERIAL:The compound of formula I (R is lower alkyl, lower alkenyl, lower alkynyl,or lower alkoxycarbonylmethyl; X is halogen).
EXAMPLE: N-2-Fluoro-4-chloro-5-methoxyphenyltetrahydrophthalamic acid.
USE: A herbicide exhibiting excellent herbicidal activity against broad-leaved weeds, gramineous weeds, cyperaceous weeds, etc., and has no phytotoxicity to corn, soybean, etc.
PROCESS: The compound of formula I can be prepared by reacting the aniline derivative of formula II with 1W1.2 equivalent of 3,4,5,6-tetrahydrophthalic anhydride in a solvent such as hexane, benzene, chloroform, etc. at 0W60°C for 30minW20hr.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：式I化合物（R为低级烷基，低级烯基，低级炔基或低级烷氧基羰基甲基; X为卤素）。实施例：N-2-氟-4-氯-5-甲氧基苯基四氢酞酸。用途：一种对阔叶杂草，禾本科杂草，野草属杂草等具有优异除草活性的除草剂，对玉米，大豆等没有植物毒性。方法：式Ⅰ化合物可以通过将式II与1-1.2当量的3,4,5,6-四氢邻苯二甲酸酐在溶剂如己烷，苯，氯仿等中，在0-60℃下反应30分钟-20小时。

5. 发明专利

JPS5965074A 2-phenyl-4,5,6,7-tetrahydro-2h-isoindole derivative, its preparation and herbicide containing it as active ingredient 失效
标题翻译： 2-苯基-4,5,6,7-四氢-2H- -2H-吲哚衍生物，其制备和除草剂含有活性成分
公开(公告)号：JPS5965074A
公开(公告)日：1984-04-13
申请号：JP17682782
申请日：1982-10-06
申请人： Sumitomo Chem Co Ltd
发明人： NAGANO HIDEYOSHI , HASHIMOTO SHIYUNICHI , YOSHIDA AKIRA , MATSUMOTO KEIJI , KAMOSHITA KATSUZOU
IPC分类号： C07D209/48 , A01N43/12
摘要： NEW MATERIAL:A 2-phenyl-4,5,6,7-tetrahydro-2H-isoindole derivative shown by the formula I (R
1 is H, or lower alkyl; R
2 is lower alkyl, lower alkenyl, cycloalkyl, phenyl, or aralkyl; X is halogen).
EXAMPLE: 2-( 2-Fluoro-4-chloro-5-ethylthiocarbonylmethoxy )phenyl-4,5,6,7-tetrahydro-2H-isoindole.
USE: Useful as a herbicide. Effective against various kinds of weeds in plowed field such as broadleaf weeds, e.g., spleen amaranth, etc., gramineous weeds such barnyard grass, gramineous weeds such as Echinochloa oryzicola Vasing, etc. in paddy field, broadleaf weeds such as false pimpernel, etc., and weeds in paddy field.
PROCESS: A compound shown by the formula II is reacted with a haloacetic acid thiol ester shown by the formula III (Y is halogen) to give a compound shown by the formula I .
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新物质：式I所示的2-苯基-4,5,6,7-四氢-2H-异吲哚衍生物（R1为H或低级烷基; R2为低级烷基，低级烯基，环烷基，苯基或芳烷基 ; X为卤素）。实施例：2-（2-氟-4-氯-5-乙硫基羰基甲氧基）苯基-4,5,6,7-四氢-2H-异吲哚。用途：用作除草剂。有效防止诸如阔叶杂草如en藜等犁田中的各种杂草，禾本科杂草如稗草，禾本科杂草如稗草等在稻田，阔叶杂草如假p nel等稻田杂草。方法：将式II化合物与式III所示的卤代乙酸硫羟酸酯（Y为卤素）反应，得到式I所示的化合物。

6. 发明专利

JPS5953466A N-phenyltetrahydrophthalimide derivative, its preparation and herbicide containing said derivative as active component 失效
标题翻译： N-苯基衍生物衍生物，其制备和除草剂含有作为活性组分的衍生物
公开(公告)号：JPS5953466A
公开(公告)日：1984-03-28
申请号：JP16544582
申请日：1982-09-21
申请人： Sumitomo Chem Co Ltd
发明人： NAGANO HIDEYOSHI , HASHIMOTO SHIYUNICHI , YOSHIDA AKIRA , MATSUMOTO KEIJI , KAMOSHITA KATSUZOU
IPC分类号： C07D209/48 , A01N37/32 , A01N43/42
摘要： NEW MATERIAL:The compound of formula I [n is 0 or 1; A is group of formula IIor formula III (R is H, lower alkyl, lower alkenyl or lower alkoxycarbonylmethyl)].
EXAMPLE: N-[4-Chloro-2-fluoro-5-(1-hydroxyiminoethoxy)phenyl]-3, 4, 5, 6-tetrahydrophthalimide.
USE: Herbicide having excellent herbicidal effect to the weeds in paddy field, plowed land, orchard, pasture, lawn, forestry, or uncultured land, and free from phytotoxicity to crops such as rice plant, corn, soybean, cotton, etc.
PROCESS: The compound of formula I can be prepared, e.g. by reacting the halide of formula IV (X is Cl or Br) with N-(4-chloro-2-fluoro-5-hydroxyphenyl)-3,4,5,6- tetrahydrophthalimide in an inert solvent such as toluene in the presence of a base such as triethylamine at 70W100°C.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：式I化合物[n为0或1; A是式II或式III的基团（R是H，低级烷基，低级烯基或低级烷氧基羰基甲基）]。实施例：N- [4-氯-2-氟-5-（1-羟基亚氨基乙氧基）苯基] -3,4,5,6-四氢邻苯二甲酰亚胺。用途：除草剂对稻田，耕地，果园，牧场，草坪，林业或无养殖地的杂草具有优异的除草效果，对水稻，玉米，大豆，棉花等作物无植物毒性。式I的化合物可以制备，例如在惰性溶剂如甲苯中，使式IV的卤化物（X为Cl或Br）与N-（4-氯-2-氟-5-羟基苯基）-3,4,5,6-四氢邻苯二甲酰亚胺反应，的碱如70-100℃的三乙胺。

7. 发明专利

JPS5933293A N-phenyltetrahydrophthalimide derivative, its preparation and herbicide containing the same as active constituent 失效
标题翻译： N-苯基四氢呋喃衍生物，其制备和除草剂含有活性成分
公开(公告)号：JPS5933293A
公开(公告)日：1984-02-23
申请号：JP14437482
申请日：1982-08-19
申请人： Sumitomo Chem Co Ltd
发明人： NAGANO HIDEYOSHI , TAKEMOTO KAZUKI , YOSHIDA AKIRA , HASHIMOTO SHIYUNICHI , FUKUSHIMA MASAYUKI
IPC分类号： A01N57/16 , A01N57/24 , C07F9/572
摘要： NEW MATERIAL:A compound of formula I [X is O or S; Y is O, S or imino; Z is halogen; R
1 is lower alkyl or lower alkoxyl lower alkoxyl lower alkyl; R
2 is lower (halo)alkyl, (lower alkoxyl lower alkoxyl) lower alkoxyl or phenyl].
EXAMPLE: N-[ 4-Chloro-2-fluoro-5-( O,O-dimethylphosphoryloxy )phenyl ]-3,4,5,6- tetrahydrophthalimide.
USE: A herbicide for paddy fields, plowed fields, orchards, lawns, pastures, forests, noncultivated lands, etc.
PROCESS: An N-(2-fluoro-4-halo-5-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide of formula II is reacted with a phosphorochloridate derivative of formula III in a solvent preferably in the presence of a dehydrohalogenating agent at 0W150°C for 30minW10hr.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：式I化合物[X为O或S; Y是O，S或亚氨基; Z是卤素; R1是低级烷基或低级烷氧基低级烷氧基低级烷基; R2是低级（卤代）烷基，（低级烷氧基低级烷氧基）低级烷氧基或苯基]。实施例：N- [4-氯-2-氟-5-（O，O-二甲基磷酰氧基）苯基] -3,4,5,6-四氢邻苯二甲酰亚胺。用途：用于水田，耕地，果园，草坪，牧场，森林，非耕地等的除草剂。方法：N-（2-氟-4-卤代-5-羟基苯基）-3,4,5,6 式II的四氢邻苯二甲酰亚胺在溶剂中，优选在脱卤化氢剂存在下，在0-150℃下反应30分钟-10小时，与式III的氯代氯酸酯衍生物反应。

8. 发明专利

JPS58206559A N-phenyl-3,4,5,6-tetrahydrophthalimide derivative, its preparation and herbicide containing the same as active constituent 失效
标题翻译： 3,4,5-三甲基苯并咪唑衍生物，其制备和除草剂含有活性成分
公开(公告)号：JPS58206559A
公开(公告)日：1983-12-01
申请号：JP9038782
申请日：1982-05-26
申请人： Sumitomo Chem Co Ltd
发明人： NAGANO HIDEYOSHI , HASHIMOTO SHIYUNICHI , YOSHIDA AKIRA , MATSUMOTO KEIJI , KAMOSHITA KATSUZOU
IPC分类号： A01N37/32 , A01N43/38 , C07D209/48
摘要： NEW MATERIAL:An N-phenyl-3,4,5,6-tetrahydrophthalimide derivative of formula I (R
1 is H, methyl or methoxyl; R
2 is cyano or aminocarbonyl of formula II; R
3 and R
4 are H or methoxyl).
EXAMPLE: N-( 4-Chloro-2-fluoro- 5 -dimethylaminocarbonylmethoxyphenyl )-3,4,5,6- tetrahydrophthalimide.
USE: A herbicide having a powerful herbicidal activity against morning glory, Indian mallow, etc. which are strong injurious weeds in fields of soybeans, cottons or corns, fat hen, bird's-eye, etc. in wheat fields and barnyard grass and broad-leaved weeds in paddy fields, etc. without the phytotoxicity to crops.
PROCESS: N-( 4-Chloro-2-fluoro-5-hydroxyphenyl )-3, 4, 5, 6-tetrahydrophthalimide is reacted with a halide of formula III (X is Cl or Br) in the presence of a base to give the compound of formula I .
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：新材料：式I的N-苯基-3,4,5,6-四氢邻苯二甲酰亚胺衍生物（R 1是H，甲基或甲氧基; R 2是氰基或式II的氨基羰基; R 3和R 4是H或甲氧基）。实施例：N-（4-氯-2-氟-5-二甲基氨基羰基甲氧基苯基）-3,4,5,6-四氢邻苯二甲酰亚胺。用途：一种对大麦，棉花或玉米，小母鸡，稗草等大田，棉花，in ard等地区强力杂草具有强力的除草活性的除草剂，具有强力的除草活性，稻田中有叶杂草等，对作物无植物毒性。方法：将N-（4-氯-2-氟-5-羟基苯基）-3,4,5,6-四氢邻苯二甲酰亚胺与式III的卤化物（X是Cl或Br）在碱的存在下反应，得到式I的化合物。

9. 发明专利

JPS5724373A 5-oxo-2,5-dihydro-1,2,4-triazine derivative, its preparation, and herbicide containing said compound as active component 失效
标题翻译： 5-OXO-2,5-DIHYDRO-1,2,4-三嗪衍生物，其制剂和含有作为活性组分的化合物的除草剂
公开(公告)号：JPS5724373A
公开(公告)日：1982-02-08
申请号：JP9895780
申请日：1980-07-18
申请人： Sumitomo Chem Co Ltd
发明人： SANEMITSU MINORU , SHIROSHITA MASAO , HASHIMOTO SHIYUNICHI , KATOU HARUHIKO , MATSUMOTO KEIJI
IPC分类号： C07D253/06 , A01N43/64 , A01N43/707
摘要： NEW MATERIAL:The compound of formula I (R is halogen, lower alkyl, lower alkoxy, nitro or trihaloalkyl; R
1 is lower alkyl; R
2 is lower alkoxy; n is integer 0W 5; provided that when n is 0, R
1 is not methyl and R
2 is not methoxy).
EXAMPLE: 2-Methyl-3-methoxy-6-(m-chlorophenyl)-5-oxo-2,5-dihydro-1,2,4-triazine.
USE: Herbicide effective remarkably against the weeds of plowed field by the soil treatment before sprouting of the weeds or by the foliar treatment of the weeds at the growing stage. It has also strong effect against annual and perennial weeds in the paddy rice field.
PROCESS: The compound of formula I is prepard by reacting the compound of formula II (R
3 is lower alkylthio) with an alkali metal alkoxide of formula R
2 M (M is alkali metal).
COPYRIGHT: (C)1982,JPO&Japio
摘要翻译：新材料：式I化合物（R为卤素，低级烷基，低级烷氧基，硝基或三卤代烷基; R 1为低级烷基; R 2为低级烷氧基; n为整数0-5;条件是当n为0时，R 1不为甲基，R2不是甲氧基）。实施例：2-甲基-3-甲氧基-6-（间氯苯基）-5-氧代-2,5-二氢-1,2,4-三嗪。用途：除草剂在发芽前通过土壤处理或在生长阶段对叶片进行叶面处理，对犁田的杂草有效显着。对水稻田中的一年生和多年生杂草也有很强的作用。方法：式I化合物通过使式II化合物（R3是低级烷硫基）与式R2M的碱金属醇盐（M是碱金属）反应来制备。

10. 发明专利

JPS59212472A 4,5,6,7-tetrahydro-2h-isoindole-1,3-dione derivative, its production and herbicide containing the same as active constituent 失效
标题翻译： 4,5,6,7-四氢-2H- -2H-吲哚-1,3-二酮衍生物，其生产和除草剂含有活性成分
公开(公告)号：JPS59212472A
公开(公告)日：1984-12-01
申请号：JP8621383
申请日：1983-05-16
申请人： Sumitomo Chem Co Ltd
发明人： NAGANO HIDEYOSHI , YOSHIDA AKIRA , MATSUMOTO KEIJI , HASHIMOTO SHIYUNICHI , KAMOSHITA KATSUZOU
IPC分类号： A01N39/00 , A01N43/38 , C07D209/48
CPC分类号： C07D209/48 , A01N39/00
摘要： NEW MATERIAL:A 4,5,6,7-tetrahydro-2H-isoindole-1,3-dione derivative of formula I (R is lower alkyl, cycloalkyl, lower alkynyl, lower haloalkyl or lower alkoxycarbonyl lower alkyl or lower alkoxyl lower alkyl; X is Cl or Br).
EXAMPLE: 2-(4-Chloro-2-fluoro-5-ethoxycarbonylmethylthio)-4,5,6,7-tetrahydro-2H- isoindole-1,3-dione.
USE: Useful as a herbicide having herbicidal effect on broad-leaved weeds, e.g. black-bindweed, in upland field, gramineous weeds, e.g. Deccan grass, or weeds of the family Cyperaceae, etc. without phytotoxicity to main crops, e.g. soybeans.
PREPARATION: A substituted phenylthioacetic acid of formula II is reacted with an alcohol of formula III in a solvent in the presence of a dehydrating agent at 0W200°C to give the compound of formula I .
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新物质：式I的4,5,6,7-四氢-2H-异吲哚-1,3-二酮衍生物（R是低级烷基，环烷基，低级炔基，低级卤代烷基或低级烷氧基羰基低级烷基或低级烷氧基低级烷基 ; X为Cl或Br）。实施例：2-（4-氯-2-氟-5-乙氧羰基甲硫基）-4,5,6,7-四氢-2H-异吲哚-1,3-二酮。用途：作为对阔叶杂草具有除草效果的除草剂有用。黑bind草，高田，禾本科杂草，杜鹃草或莎草科的杂草等，对主要作物没有植物毒性，例如，大豆。制备：将式II的取代的苯硫基乙酸在溶剂中，在0-200℃的脱水剂存在下，与式III的醇反应，得到式I化合物。

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