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1. 发明授权

US5298469A Fluxed lanthanum chromite for low temperature air firing 失效
标题翻译：用于低温空气烧制的助熔亚铬酸镧
公开(公告)号：US5298469A
公开(公告)日：1994-03-29
申请号：US981444
申请日：1992-11-25
申请人： Stephen Haig , Beili L. Wu , Jean Yamanis
发明人： Stephen Haig , Beili L. Wu , Jean Yamanis
IPC分类号： C01G37/00 , C04B35/42 , C04B35/50 , C04B35/624 , H01M8/02 , H01M8/12 , C04B35/04 , C01G39/00 , C04B35/51
CPC分类号： C04B35/624 , C01G37/006 , C04B35/42 , H01M8/0215 , H01M8/1213 , C01P2002/02 , C01P2002/54 , C01P2006/10 , C01P2006/12 , H01M2008/1293 , H01M2300/0074
摘要： A lanthanum chromite ceramic powder consisting essentially of 1 mol of LaCr.sub.1-x M.sub.x O.sub.3, where M is a divalent metal selected from the group of zinc, copper and mixtures thereof and x ranges from about 0.02 to 0.2, y mols of B.sub.2 O.sub.3, where y ranges from 0.0005 to 0.04, and z mols of La.sub.2 O.sub.3, where the ratio z/y ranges from 1 to 3, the powder is sintered to high density by firing a compact thereof at a temperature of about 1400.degree. C. in air or other atmosphere, and is particularly suited for use as interconnect material for solid oxide fuel cells.
摘要翻译：基本上由1mol LaCr1-xMxO3组成的亚铬酸镧陶瓷粉末，其中M是选自锌，铜及其混合物的二价金属，x在约0.02至0.2摩尔的B2O3中，其中y的范围为 0.0005〜0.04，z2O3为z / y为1〜3的Z2O3，通过在空气或其他大气中在约1400℃的温度下烧结其成型体将粉末烧结成高密度，特别适用于固体氧化物燃料电池的互连材料。

2. 发明授权

US5286686A Air-sinterable lanthanum chromite and process for its preparation 失效
标题翻译：空气烧结的亚铬酸镧及其制备方法
公开(公告)号：US5286686A
公开(公告)日：1994-02-15
申请号：US981633
申请日：1992-11-25
申请人： Stephen Haig , Beili L. Wu , Jean Yamanis
发明人： Stephen Haig , Beili L. Wu , Jean Yamanis
IPC分类号： C01G37/00 , C04B35/42 , C04B35/50 , H01M8/02 , H01M8/12 , C04B35/04 , C01G39/00 , C04B35/51
CPC分类号： C04B35/42 , C01G37/006 , H01M8/0215 , C01P2002/02 , C01P2002/54 , C01P2006/10 , C01P2006/12 , H01M2008/1293 , H01M2300/0074 , H01M8/0219
摘要： A sinter-reactive lanthanum chromite powder is prepared from the lanthanum chromite precursor LaCr.sub.1-x M.sub.x O.sub.3 (Adsorbate). The powder is crystalline, has the formula LaCr.sub.1-x M.sub.x O.sub.3, where M is selected from the group consisting of zinc, copper and mixtures thereof and x ranges from about 0.02 to 0.2, and sinters to densities higher than about 95% of theoretical density at temperature as low as 1400.degree. C. in oxidizing atmospheres. Sintering to such high density at temperatures in the vicinity of 1400.degree. C. makes the powder particularly suited for use as interconnect material for solid oxide fuel cells.
摘要翻译：从铬酸镧原子LaCr1-xMxO3（Adsorbate）制备烧结反应性铬酸镧粉末。粉末是结晶的，具有式LaCr1-xMxO3，其中M选自锌，铜及其混合物，x的范围为约0.02至0.2，并且在温度下烧结至高于理论密度的约95％的密度在氧化气氛中低至1400摄氏度。在1400摄氏度左右的温度下烧结至如此高的密度，使粉末特别适用于固体氧化物燃料电池的互连材料。

3. 发明授权

US5169811A Beneficiated lanthanum chromite for low temperature firing 失效
标题翻译：有益于低温燃烧的蓝绿色
公开(公告)号：US5169811A
公开(公告)日：1992-12-08
申请号：US643255
申请日：1991-01-22
申请人： Ned E. Cipollini , Beili L. Wu , Stephen Haig , Jean Yamanis
发明人： Ned E. Cipollini , Beili L. Wu , Stephen Haig , Jean Yamanis
IPC分类号： C01G37/00 , C04B35/42 , C04B35/50 , C04B35/624 , H01M8/02 , H01M8/12
CPC分类号： H01M8/0215 , C01G37/006 , C04B35/42 , C04B35/624 , H01M8/1213 , C01P2002/02 , C01P2002/54 , C01P2006/10 , C01P2006/12 , H01M2008/1293 , H01M2300/0074
摘要： A lanthanum chromite ceramic powder mixture that consists essentially of 1 mol of LaCr.sub.1-x M.sub.x O.sub.3, where M is a divalent metal selected from the group consisting of magnesium, calcium and mixtures thereof and x ranges from 0.03 to 0.3; y mols of B.sub.2 O.sub.3, where y ranges from 0.005 to 0.04; and z mols of La.sub.2 O.sub.3, where the ratio z/y ranges from 1.1 to 3. The mixture is formed into powder compacts and sintered to near full density at temperatures as low as 1400.degree. C.
摘要翻译：基本上由1mol LaCr1-xMxO3组成的亚铬酸镧陶瓷粉末混合物，其中M是选自镁，钙及其混合物的二价金属，x在0.03至0.3的范围内; B2O3的摩尔数，其中y为0.005至0.04; 和zmol的La 2 O 3，其中z / y的比率为1.1至3.将混合物形成粉末压块并在低至1400℃的温度下烧结至接近全密度。

4. 发明授权

US5292489A Ternary silicon-rare earth nitrides and process for their preparation 失效
标题翻译：三元硅 - 稀土氮化物及其制备方法
公开(公告)号：US5292489A
公开(公告)日：1994-03-08
申请号：US720272
申请日：1991-06-24
申请人： Anthony J. Fanelli , Jeffrey P. Solar , Beili L. Wu , Jean Yamanis
发明人： Anthony J. Fanelli , Jeffrey P. Solar , Beili L. Wu , Jean Yamanis
IPC分类号： C04B35/515 , C04B35/584 , C04B35/593 , C04B35/58
CPC分类号： C04B35/5156 , C04B35/584 , C04B35/5935
摘要： This invention provides a compound having the formula LnSi.sub.3 N.sub.5 wherein Ln is selected from the group consisting of scandium, yttrium, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, and lutetium. In addition, there is provided a method for making the compound Ln'Si.sub.3 N.sub.5 wherein Ln' is a radical selected from the group consisting of lanthanum, scandium, yttrium, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium and lutetium, comprising the step of reacting SiO.sub.z, Ln'.sub.x O.sub.y in a nitrogen atmosphere in the presence of carbon at a temperature of from 1200.degree. C. to about 2000.degree. C. for at least 2 hrs., x being an integer equal to or greater than 2, y being an integer equal to or greater than 3, and z being an integer selected from 1 and 2, with the proviso that x and y are selected to result in a stable compound of Ln'.sub.x O.sub.y.
摘要翻译：本发明提供具有式LnSi 3 N 5的化合物，其中Ln选自钪，钇，铈，镨，钕，ium，钐，铕，钆，铽，镝，钬，铒，ium，镱和镥。此外，提供了一种制备化合物Ln'Si3N5的方法，其中Ln'是选自镧，钪，钇，铈，镨，钕，ium，钐，铕，钆，铽，镝的基团钬，铒，ium，镱和镥，包括在碳存在下，在1200℃至约2000摄氏度的温度下，在氮气气氛中使SiO 2，L 1 O 10反应至少2小时的步骤 x是等于或大于2的整数，y是等于或大于3的整数，z是选自1和2的整数，条件是选择x和y以产生稳定的化合物的Ln'xOy。

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