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1. 发明授权

US07432340B2 Fluorinated alkyl substituted-thieno[3,4-]thiophene monomers and polymers therefrom 有权
标题翻译：氟化烷基取代噻吩并[3,4-b]噻吩单体及其聚合物
公开(公告)号：US07432340B2
公开(公告)日：2008-10-07
申请号：US11128538
申请日：2005-05-13
申请人： Steffen Zahn , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Kristen Elaine Minnich , Andrew Francis Nordquist , Lloyd Mahlon Robeson , Francis Joseph Waller
发明人： Steffen Zahn , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Kristen Elaine Minnich , Andrew Francis Nordquist , Lloyd Mahlon Robeson , Francis Joseph Waller
IPC分类号： C08G73/24 , C08F4/80 , C08G75/00
CPC分类号： C08G61/123 , C08G61/126
摘要： Partially and fully fluorinated alkyl substituted thienothiophene monomers (and polymers thereof) wherein the monomers are represented by the formula: wherein R is a partially or fully fluorinated primary, secondary or tertiary alkyl having from 1 to 8 carbon atoms; and X and X′ are independently selected from the group consisting of H, F, Cl, Br, I, MgCl, MgBr, Mgl, Sn(R′)3, CH═CHR″, —OR″, —COOR″, —S—COR″, —B(OR″)2, —COR″, —C≡CH, and a polymerizable cyclic pi-conjugated carbon-ring structure optionally comprising S, N or O heteroatoms; wherein R′ is a primary, secondary or tertiary alkyl having from 1 to 6 carbon atoms, and R″ is H or a primary, secondary or tertiary alkyl having from 1 to 6 carbon atoms.
摘要翻译：部分和完全氟化的烷基取代的噻吩并噻吩单体（及其聚合物），其中单体由下式表示：其中R是具有1至8个碳原子的部分或完全氟化的伯，仲或叔烷基; 并且X和X'独立地选自H，F，Cl，Br，I，MgCl，MgBr，MgI，Sn（R'）3，CH-CHR“， - OR“，-COOR”，-S-COR“，-B（OR”）2，-COR“，-C≡CH和可聚合的环状π-共轭碳任选地包含S，N或O杂原子的环结构; 其中R'是具有1至6个碳原子的伯，仲或叔烷基，R“是H或具有1至6个碳原子的伯，仲或叔烷基。

2. 发明授权

US07572879B2 Fluorinated alkyl substituted-thieno[3,4-b]thiophene monomers and polymers therefrom 有权
标题翻译：氟化烷基取代噻吩并[3,4-b]噻吩单体及其聚合物
公开(公告)号：US07572879B2
公开(公告)日：2009-08-11
申请号：US11418317
申请日：2006-05-05
申请人： Steffen Zahn , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Kristen Elaine Minnich , Andrew Francis Nordquist , Lloyd Mahlon Robeson , Francis Joseph Waller
发明人： Steffen Zahn , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Kristen Elaine Minnich , Andrew Francis Nordquist , Lloyd Mahlon Robeson , Francis Joseph Waller
IPC分类号： C08G73/24 , C08G75/00 , C08F4/80
CPC分类号： C07D495/04 , C08G61/126 , C08G2261/146 , C08G2261/3243 , C08L25/12 , C08L25/18 , C08L27/12 , C08L33/02 , C08L35/00 , C08L65/00 , H01B1/127 , H01G11/48 , H01L51/0036 , Y02E60/13 , C08L2666/06 , C08L2666/04
摘要： Partially and fully fluorinated alkyl substituted thienothiophene monomers (and polymers thereof) wherein the monomers are represented by the formula: wherein R is a partially or fully fluorinated primary, secondary or tertiary alkyl having from 1 to 8 carbon atoms; and X and X′ are independently selected from the group consisting of H, F, Cl, Br, I, MgCl, —COR″, —C≡CH, and a polymerizable cyclic pi-conjugated carbon-ring structure optionally comprising S, N or O heteroatoms; wherein R′ is a primary, secondary or tertiary alkyl having from 1 to 6 carbon atoms, and R″ is H or a primary, or tertiary alkyl having from 1 to 6 carbon atoms.
摘要翻译：部分和完全氟化的烷基取代的噻吩并噻吩单体（及其聚合物），其中单体由下式表示：其中R是具有1至8个碳原子的部分或完全氟化的伯，仲或叔烷基; 并且X和X'独立地选自H，F，Cl，Br，I，MgCl，-COR“，-C≡CH，以及任选地包含S的可聚合环状π-共轭碳环结构， N或O杂原子; 其中R'是具有1至6个碳原子的伯，仲或叔烷基，R“是H或具有1至6个碳原子的伯或叔烷基。

3. 发明授权

US07094365B2 Pentafluorosulfanyl-substituted thienothiophene monomers and conducting polymers 失效
标题翻译：五氟硫烷基取代的噻吩并噻吩单体和导电聚合物
公开(公告)号：US07094365B2
公开(公告)日：2006-08-22
申请号：US10958054
申请日：2004-10-04
申请人： Steffen Zahn , Andrew Francis Nordquist , Kristen Elaine Minnich , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Axel Klauck-Jacobs
发明人： Steffen Zahn , Andrew Francis Nordquist , Kristen Elaine Minnich , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Axel Klauck-Jacobs
IPC分类号： H01B1/12 , C07D333/00
CPC分类号： C08G61/126 , H01B1/127
摘要： Thienothiophene monomers having an SF5 group and conducting oligomers and polymers formed by the polymerization of such monomers and their use as hole injection materials, charge transport materials, or as semiconductors. The compound may be of the formula: where X and X′ are independently H, halogen atoms (e.g., F, Cl, Br, and I), MgCl, MgBr, MgI, Sn(R′)3, where R′ is C1-6 alkyl or —OC1-6 alkyl, boronic acid, boronic ester, —CH═CHR″ (where R″ is H or C1-6 alkyl), —OC1-6 alkyl, —COOC1-6 alkyl, —S—COR′″ and —COR′″ (where R′″ is H or C1-6 alkyl), —C≡CH, or polymerizable aromatic rings (such as phenyl, naphthalene, pyrrole, dithiophene, thienothiophene, thiophene and so forth.
摘要翻译：具有SF 5 N基团的噻吩并噻吩单体和通过这些单体的聚合形成的导电低聚物和聚合物及其作为空穴注入材料，电荷传输材料或半导体的用途。化合物可以具有下式：其中X和X'独立地为H，卤素原子（例如F，Cl，Br和I），MgCl，MgBr，MgI，Sn（R'）3 >，其中R'是C 1-6烷基或-OC 1-6 - 烷基，硼酸，硼酸酯，-CH-CHR“（其中R” 是H或C 1-6烷基），-OC 1-6烷基，-COOC 1-6烷基，-S-COR' '和-COR''（其中R“'是H或C 1-6烷基），-C≡CH或可聚合的芳环（例如苯基，萘，吡咯，二噻吩噻吩并噻吩，噻吩等。

4. 发明申请

US20130040060A1 Liquid Methylenedianiline Compositions 有权
标题翻译：液体亚甲基二苯胺组合物
公开(公告)号：US20130040060A1
公开(公告)日：2013-02-14
申请号：US13208449
申请日：2011-08-12
申请人： Gauri Sankar Lal , Kristen Elaine Minnich , Pritesh G. Patel , Gamini Ananda Vedage , Garret C. Lau
发明人： Gauri Sankar Lal , Kristen Elaine Minnich , Pritesh G. Patel , Gamini Ananda Vedage , Garret C. Lau
IPC分类号： B05D3/00 , C09K3/00
CPC分类号： C08G59/5033 , C07C211/46 , C07C211/55 , C09K3/00
摘要： A liquid methylenedianiline product is disclosed. The product is produced by reacting aniline and ethylaniline with formaldehyde with an amine to formaldehyde ratio greater than about 2:1. The resulting reaction product is a liquid mixture of methylenedianiline, monoethyl methylenedianiline, and diethyl methylenedianiline having a viscosity of less than about 1000 cps at 40° C.
摘要翻译：公开了一种液体亚甲基二苯胺产物。该产物通过苯胺和乙基苯胺与甲醛反应制得，胺与甲醛的比例大于约2:1。所得反应产物是在40℃下具有小于约1000cps的亚甲基二苯胺，单乙基亚甲基二苯胺和二乙基亚甲基二苯胺的液体混合物。

5. 发明授权

US06958415B2 Synthesis of pentafluorosulfuranyl arylenes 有权
标题翻译：五氟硫烷基亚芳基的合成
公开(公告)号：US06958415B2
公开(公告)日：2005-10-25
申请号：US10713231
申请日：2003-11-14
申请人： Gauri Sankar Lal , Kristen Elaine Minnich
发明人： Gauri Sankar Lal , Kristen Elaine Minnich
IPC分类号： C07B61/00 , C07C381/00
CPC分类号： C07C381/00
摘要： A new route has been found leading to the formation of pentafluorosulfuranyl arylenes. In its broadest aspect the process comprises: effecting dehydrohalogenation or dehydrogenation of a pentafluorosulfuranyl cycloaliphatic compound represented by either of the structures: wherein R1-5 are H, halogen, C1-10 alkyl, C1-10 alkoxy, C1-10 thionyl, C1-10 alkyl ether, aryl and substituted aryl, thioether, sulfonyl, carboalkoxy, alkylamino, arylamino, alkylphosphoryl, alkylphosphonyl, arylphosphonyl, arylphosphoryl, and mixtures thereof and X is a halogen atom to form the pentafluorosufuranyl arylene represented by the structures: wherein R1-R5 are as represented above.
摘要翻译：已经发现导致形成五氟硫烷基亚芳基的新途径。在其最广泛的方面，该方法包括：进行由以下任一结构表示的五氟硫烷基环脂族化合物的脱卤化氢或脱氢：其中R 1-5是H，卤素，C 1-10 - 亚烷基，C 1-10烷氧基，C 1-10亚硫酰基，C 1-10烷基醚，芳基和取代的芳基，硫醚磺酰基，烷氧基羰基，烷基氨基，芳基氨基，烷基磷酰基，烷基膦酰基，芳基膦酰基，芳基磷酰基及其混合物，X是卤素原子，形成由以下结构表示的五氟呋喃基亚芳基：其中R 1 -R < > 5 如上所示。

6. 发明授权

US07771611B2 Oxypentafluorosulfate compositions and processes for making them 有权
标题翻译：一氧化五氟硫酸盐组合物及其制备方法
公开(公告)号：US07771611B2
公开(公告)日：2010-08-10
申请号：US11484374
申请日：2006-07-10
申请人： Robert George Syvret , Gauri Sankar Lal , Kristen Elaine Minnich
发明人： Robert George Syvret , Gauri Sankar Lal , Kristen Elaine Minnich
IPC分类号： C09K3/00 , C01B21/22 , C01B21/24 , C01B21/086 , C01B9/08 , C01B17/45 , C07F9/02 , C07C279/04 , C07C211/63 , C07C211/62 , C07D295/04 , C07D207/323 , C07C211/64
CPC分类号： C01B21/086 , C01D15/00 , C07C211/63 , C07C381/12
摘要： Novel compositions are provided containing a compound represented by the formula YOSF5 or ZOSF5, where: (a) Y is: (i) an organic cation other than (Me2N)3S+ or (ii) an inorganic cation, provided that when Y is the inorganic cation, the composition further includes a complexing agent; and (b) Z is C1-20 alkyl, aryl, cycloalkyl, combinations thereof, or analogues thereof containing at least one heteroatom, provided that the compound represented by the formula ZOSF5 is a molecular compound. Processes of making the cationic compounds are disclosed as are processes for using the compositions containing cationic compounds in nucleophilic replacement reactions to prepare the compositions containing molecular compounds including the OSF5 group.
摘要翻译：提供含有由式YOSF5或ZOSF5表示的化合物的新型组合物，其中：（a）Y为：（i）除（Me 2 N）3S +以外的有机阳离子或（ii）无机阳离子，条件是当Y为无机阳离子，该组合物还包含络合剂; 和（b）Z是含有至少一个杂原子的C 1-20烷基，芳基，环烷基，其组合或其类似物，条件是由式ZOSF5表示的化合物是分子化合物。公开阳离子化合物的制备方法是使用含有阳离子化合物的组合物在亲核取代反应中制备包含OSF5基团的分子化合物的组合物的方法。

7. 发明申请

US20080033164A1 Oxypentafluorosulfate compositions and processes for making them 有权
标题翻译：一氧化五氟硫酸盐组合物及其制备方法
公开(公告)号：US20080033164A1
公开(公告)日：2008-02-07
申请号：US11484374
申请日：2006-07-10
申请人： Robert George Syvret , Gauri Sankar Lal , Kristen Elaine Minnich
发明人： Robert George Syvret , Gauri Sankar Lal , Kristen Elaine Minnich
IPC分类号： C07D487/22 , C07C309/00
CPC分类号： C01B21/086 , C01D15/00 , C07C211/63 , C07C381/12
摘要： Novel compositions are provided containing a compound represented by the formula YOSF5 or ZOSF5, where: (a) Y is: (i) an organic cation other than (Me2N)3S+ or (ii) an inorganic cation, provided that when Y is the inorganic cation, the composition further includes a complexing agent; and (b) Z is C1-20 alkyl, aryl, cycloalkyl, combinations thereof, or analogues thereof containing at least one heteroatom, provided that the compound represented by the formula ZOSF5 is a molecular compound. Processes of making the cationic compounds are disclosed as are processes for using the compositions containing cationic compounds in nucleophilic replacement reactions to prepare the compositions containing molecular compounds including the OSF5 group.
摘要翻译：提供含有由式YOSF 5或ZOSF 5 N表示的化合物的新型组合物，其中：（a）Y为：（i）除（Me < 或（ii）无机阳离子，条件是当Y是无机阳离子时，该组合物还包含络合剂（例如，N，N-二甲基氨基乙基） ; 和（b）Z为含有至少一个杂原子的C 1-20烷基，芳基，环烷基，其组合或其类似物，条件是由式ZOSF 5表示的化合物， SUB>是分子化合物。公开了制备阳离子化合物的方法，就是使用含有阳离子化合物的组合物在亲核置换反应中制备含有分子化合物的组合物的方法，包括OSF 5组。

8. 发明授权

US06479645B1 Sulfurpentafluoride compounds and methods for making and using same 失效
标题翻译：四氟化硫化合物及其制备和使用方法
公开(公告)号：US06479645B1
公开(公告)日：2002-11-12
申请号：US10104214
申请日：2002-03-22
申请人： Gauri Sankar Lal , Kristen Elaine Minnich
发明人： Gauri Sankar Lal , Kristen Elaine Minnich
IPC分类号： C07F708
CPC分类号： C07F7/081
摘要： A sulfurpentafluoride and substituted silyl ethyne compound that is useful as precursors for a variety of organic compounds are disclosed. At least one of the substituents on the silicon atom is hindered. Also disclosed are high-yielding processes for making the ethyne compound of the present invention.
摘要翻译：公开了可用作各种有机化合物的前体的五氟化钨和取代的甲硅烷基乙炔化合物。硅原子上的至少一个取代基受到阻碍。还公开了制备本发明的乙炔化合物的高产率方法。

9. 发明授权

US09321881B2 Liquid methylenedianiline compositions 有权
标题翻译：液体亚甲基二胺组合物
公开(公告)号：US09321881B2
公开(公告)日：2016-04-26
申请号：US13208449
申请日：2011-08-12
申请人： Gauri Sankar Lal , Kristen Elaine Minnich , Pritesh G. Patel , Gamini Ananda Vedage , Garret C. Lau
发明人： Gauri Sankar Lal , Kristen Elaine Minnich , Pritesh G. Patel , Gamini Ananda Vedage , Garret C. Lau
IPC分类号： C08G59/50 , C07C211/46 , C07C211/55 , C09K3/00 , B05D3/00
CPC分类号： C08G59/5033 , C07C211/46 , C07C211/55 , C09K3/00
摘要： A liquid methylenedianiline product is disclosed. The product is produced by reacting aniline and ethylaniline with formaldehyde with an amine to formaldehyde ratio greater than about 2:1. The resulting reaction product is a liquid mixture of methylenedianiline, monoethyl methylenedianiline, and diethyl methylenedianiline having a viscosity of less than about 1000 cps at 40° C.
摘要翻译：公开了一种液体亚甲基二苯胺产物。该产物通过苯胺和乙基苯胺与甲醛反应制得，胺与甲醛的比例大于约2:1。所得反应产物是在40℃下具有小于约1000cps的亚甲基二苯胺，单乙基亚甲基二苯胺和二乙基亚甲基二苯胺的液体混合物。

10. 发明授权

US07166755B2 Synthesis of pentafluorosulfanylnaphthalene 失效
标题翻译：五氟硫烷基萘的合成
公开(公告)号：US07166755B2
公开(公告)日：2007-01-23
申请号：US10954719
申请日：2004-09-30
申请人： Gauri Sankar Lal , Kristen Elaine Minnich
发明人： Gauri Sankar Lal , Kristen Elaine Minnich
IPC分类号： C07C19/08
CPC分类号： C07C381/00 , C07C2601/14 , C07F5/027 , C07F7/081
摘要： This invention relates to 2-pentafluorosulfanylnapthalene, substituted derivatives thereof and to a process for producing naphthalene carrying an SF5 group. A 3-step process is employed wherein 1,4-dihydronaphthalene is reacted with pentafluorosulfanyl halide. Next the resulting 3-halo-2-pentafluorosulfanylnaphthalene or derivative is converted to 2-pentafluorosulfanyl-1,4-dihydronaphthalene or derivative by treatment with a base and subsequently transformed into pentafluorosulfanylnaphthalene by removing hydrogen atoms.
摘要翻译：本发明涉及2-五氟硫烷基萘及其取代衍生物，以及一种生产含有SF 5 H 5基团的萘的方法。使用其中1,4-二氢萘与五氟硫烷基卤化物反应的三步法。接下来，通过用碱处理将所得3-卤代-2-五氟硫烷基萘或其衍生物转化为2-五氟硫烷基-1,4-二氢萘或衍生物，随后通过除去氢原子转化成五氟硫烷基萘。

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