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1. 发明授权

US06281322B1 Coating compositions containing alkoxysilanes 失效
标题翻译：含有烷氧基硅烷的涂料组合物
公开(公告)号：US06281322B1
公开(公告)日：2001-08-28
申请号：US09451539
申请日：1999-12-01
申请人： Stefan Groth , Reinhard Halpaap , Markus Mechtel , Lutz Schmalstieg , Philip E. Yeske
发明人： Stefan Groth , Reinhard Halpaap , Markus Mechtel , Lutz Schmalstieg , Philip E. Yeske
IPC分类号： C08G7726
CPC分类号： C08G18/792 , C08G18/282 , C08G18/289 , C08G18/758 , C09D175/04 , Y10T428/31551 , Y10T428/31663
摘要： The present invention relates to coating compositions containing 40 to 100% by weight, based on resin solids, of an alkoxysilyl-functional polyisocyanate polyurea which is reaction product of A) a polyisocyanate component having an average functionality of 2.5 to 5.5, an NCO content of 11.0 to 20.0% by weight and a monomeric diisocyanate content of less than 10% by weight, and containing at least 50% by weight of a polyisocyanate prepared from 4,4′-diisocyanatodicyclohexyl-methane with B) at least 0.7 equivalents, based on the equivalents of isocyanate groups, of an aminosilane corresponding to formula (I) (RO)nY(3−n)Si—CH2CH2CH2—NHZ (I), wherein R represents methyl or ethyl, Y represents methyl, Z represents H, a C1-C12 alkyl or CH2CH2CH2—Si(OR)nY3−n, and n is 1, 2 or 3, and C) optionally other isocyanate-reactive compounds. The present invention also relates the hydrolyzates/condensates that are prepared by adding water or an aqueous solution of a catalyst to the coating compositions according to the invention.
摘要翻译：本发明涉及基于树脂固体含有40-100重量％的烷氧基甲硅烷基官能多异氰酸酯聚脲的涂料组合物，其是A）平均官能度为2.5至5.5的多异氰酸酯组分，NCO含量为11.0 至20.0重量％，并且单体二异氰酸酯含量小于10重量％，并且含有至少50重量％的由4,4'-二异氰酸根合二环己基甲烷制备的聚异氰酸酯与B）至少0.7当量，基于当量的异氰酸酯基，对应于式（I）的氨基硅烷，其中R表示甲基或乙基，Y表示甲基，Z表示H，C1-C12烷基或CH2CH2CH2-Si（OR）nY3-n，n为1,2或3 ，和C）任选其它异氰酸酯反应性化合物。本发明还涉及通过将水或催化剂的水溶液加入到根据本发明的涂料组合物中制备的水解产物/缩合物。

2. 发明授权

US5756751A Compounds containing alkoxysilane groups and hydantoin groups 失效
标题翻译：含有烷氧基硅烷基和乙内酰脲基团的化合物
公开(公告)号：US5756751A
公开(公告)日：1998-05-26
申请号：US855423
申请日：1997-05-13
申请人： Lutz Schmalstieg , Rainer Rettig , Gotz Limbeck , Richard R. Roesler , Edward P. Squiller , Philip E. Yeske , Stanley F. Siranovich
发明人： Lutz Schmalstieg , Rainer Rettig , Gotz Limbeck , Richard R. Roesler , Edward P. Squiller , Philip E. Yeske , Stanley F. Siranovich
IPC分类号： C08G18/10 , C08G18/38 , C08G18/61 , C08G18/83 , C09D175/04 , C09D183/08 , C09K3/10 , C07D231/00
CPC分类号： C09K3/1021 , C08G18/10 , C08G2190/00
摘要： The present invention relates to compounds containing alkoxysilane and hydantoin groups and corresponding to the formula ##STR1## wherein X represents identical or different organic groups which are inert to isocyanate groups below 100.degree. C., provided that at least one of these groups is an alkoxy group, Z represents COOR.sub.1 or an aromatic ring, R represents the residue obtained by removing the isocyanate groups from an organic monomeric polyisocyanate, a polyisocyanate adduct or an NCO prepolymer, R.sub.1 represents an organic group which is inert to isocyanate groups at a temperature of 100.degree. C. or less, R.sub.3 and R.sub.4 are identical or different and represent hydrogen or organic groups which are inert to isocyanate groups at a temperature of 100.degree. C. or less, n is an integer from 1 to 8 and m has an average value of 1.5 to 6. The present invention also relates to the use of these compounds for the preparation coatings, sealants and adhesives.
摘要翻译：本发明涉及含有烷氧基硅烷和乙内酰脲基团的化合物，并且对应于下式（I），其中X表示对于低于100℃的异氰酸酯基团惰性的相同或不同的有机基团，条件是这些基团中的至少一个是烷氧基，Z表示COOR1或芳香环，R表示通过从有机单体多异氰酸酯除去异氰酸酯基团，多异氰酸酯加合物或NCO预聚物得到的残基，R1表示在一个温度为100℃以下，R3和R4相同或不同，表示在100℃以下的温度下为异氰酸酯基而言为惰性的氢或有机基团，n为1〜8的整数，m为平均值为1.5至6.本发明还涉及这些化合物用于制备涂料，密封剂和粘合剂的用途。

3. 发明授权

US5747629A Low surface energy polyisocyanates and their use in one-or two-component coating compositions 失效
标题翻译：低表面能多异氰酸酯及其在单组分或双组分涂料组合物中的用途
公开(公告)号：US5747629A
公开(公告)日：1998-05-05
申请号：US764891
申请日：1996-12-16
申请人： Philip E. Yeske , William E. Slack , Edward P. Squiller
发明人： Philip E. Yeske , William E. Slack , Edward P. Squiller
IPC分类号： C08G18/02 , C08G18/73 , C08G18/77 , C08G18/78 , C08G18/79 , C08G18/80 , C09D175/04 , C08G18/28
CPC分类号： C08G18/8087 , C08G18/773 , C08G18/7837
摘要： The present invention relates to polyisocyanate adducts containing allophanate groups, fluorine and optionally isocyanurate groups that are prepared by reacting compounds a) which i) are substantially free of hydroxyl groups and isocyanate groups, ii) have an average of at least two urethane groups per molecule and iii) contain 0 to 50% by weight of fluorine, based on the weight of the polyisocyanate adducts, with an excess quantity, based on the equivalents of urethane groups, of polyisocyanates b), which optionally contain fluorine, to form polyisocyanate adducts and optionally removing at least a portion of the unreacted excess polyisocyanates b), provided that compounds a) and polyisocyanates b) contain a total of at least 0.001% by weight, of fluorine, based on the weight of the polyisocyanate adducts. The present invention also relates to a process for preparing these polyisocyanates adducts, to blends of the polyisocyanate adducts with other polyisocyanates that do not contain fluorine and to the use of the polyisocyanate adducts or polyisocyanate blends, optionally in blocked form, in one- or two-component coating compositions.
摘要翻译：本发明涉及通过使i）基本上不含羟基和异氰酸酯基的化合物a）制备的含有脲基甲酸酯基团，氟和任选的异氰脲酸酯基团的多异氰酸酯加合物，ii）每个分子平均具有至少两个氨基甲酸酯基团和iii）基于多异氰酸酯加合物的重量，含有0至50重量％的氟，基于氨基甲酸酯基的当量，任选地含有氟的多异氰酸酯b），以形成多异氰酸酯加合物和任选地除去至少一部分未反应的过量多异氰酸酯b），条件是化合物a）和多异氰酸酯b）基于聚异氰酸酯加合物的重量含有总共至少0.001重量％的氟。本发明还涉及一种制备这些多异氰酸酯加成物的方法，多异氰酸酯加合物与不含氟的其它多异氰酸酯的共混物以及任选地以封闭形式在一或二个中使用的多异氰酸酯加合物或多异氰酸酯共混物 - 组分涂料组合物。

4. 发明授权

US5633389A Thermoreversible coating and a process for its manufacture 失效
标题翻译：热可逆涂层及其制造工艺
公开(公告)号：US5633389A
公开(公告)日：1997-05-27
申请号：US448847
申请日：1995-05-24
申请人： Erik H. Jonsson , Philip E. Yeske , Douglas A. Wicks , Harald Pielartzik
发明人： Erik H. Jonsson , Philip E. Yeske , Douglas A. Wicks , Harald Pielartzik
IPC分类号： C07D233/72 , C07D233/78 , C08G18/46 , C09D175/00 , C09D175/02
CPC分类号： C07D233/78 , C08G18/4615 , C09D175/00
摘要： The invention relates to a thermoreversible process for the preparation of a hydantoin comprisng(a) reacting an unsaturated polyester with a monofunctional amine to yield a poly(ester aspartate), and(b) reacting said poly(ester aspartate) with an isocyanate to produce a poly(ester urea), and(c) heating said poly(ester urea) to form a hydantoin compound.The process is useful for the preparation of coatings.
摘要翻译：本发明涉及一种用于制备乙内酰脲的热可逆方法，其包括（a）使不饱和聚酯与单官能胺反应以产生聚（酯天冬氨酸酯），和（b）使所述聚（酯天冬氨酸酯）与异氰酸酯反应以产生聚（酯尿素），和（c）加热所述聚（酯脲）以形成乙内酰脲化合物。该方法可用于制备涂料。

5. 发明授权

US5541281A Low surface energy polyisocyanates and their use in one- or two-component coating compositions 失效
标题翻译：低表面能多异氰酸酯及其在单组分或双组分涂料组合物中的用途
公开(公告)号：US5541281A
公开(公告)日：1996-07-30
申请号：US359777
申请日：1994-12-20
申请人： Philip E. Yeske , Edward P. Squiller , William E. Slack
发明人： Philip E. Yeske , Edward P. Squiller , William E. Slack
IPC分类号： C08G18/50 , C08G18/78 , C08G18/80 , C08G18/28
CPC分类号： C08G18/8061 , C08G18/5015 , C08G18/7837 , C08G18/8054 , C08G18/8087
摘要： The present invention is directed to a polyisocyanate mixturei) having an NCO content of 5 to 35% by weight and prepared from an organic diisocyanate,ii) containing less than 5% by weight of isocyanurate groups (calculated as N.sub.3, C.sub.3, O.sub.3, MW 126),iii) containing allophanate groups in an amount such that there are more equivalents of allophanate groups than urethane groups andiv) containing fluorine (calculated as F, AW 19) in an amount of 0.001 to 50% by weight, based on solids.,wherein fluorine is incorporated with compounds containing two or more carbon atoms, one or more hydroxyl groups and one or more fluorine atoms. The present invention is also directed to a process for the production of this polyisocyanate mixture and to its use, optionally in blocked form, as an isocyanate component in one- or two-component coating compositions.
摘要翻译：本发明涉及NCO含量为5-35重量％并由有机二异氰酸酯制备的多异氰酸酯混合物，ii）含有少于5重量％的异氰脲酸酯基（按N 3，C 3，O 3， MW 126），iii）含有脲基甲酸酯基团，其含量使得相对于氨基甲酸酯基团具有更多当量的脲基甲酸酯基，和iv）含有以（以F，AW 19计算）的氟（以F，AW 19计算），其量为0.001至50重量％，基于固体，其中氟与含有两个或更多个碳原子的化合物，一个或多个羟基和一个或多个氟原子结合。本发明还涉及在单组分或双组分涂料组合物中制备该多异氰酸酯混合物及其用途，任选为封闭形式的异氰酸酯组分的方法。

6. 发明授权

US5726273A Heat-curable compositions based on cyclic isocyanate addition reproducts 失效
标题翻译：基于环状异氰酸酯加成物的可热固化组合物
公开(公告)号：US5726273A
公开(公告)日：1998-03-10
申请号：US658786
申请日：1996-06-05
申请人： Douglas A. Wicks , Robert J. Kumpf , Sze-Ming Lee , Duane B. Priddy, Jr. , Philip E. Yeske
发明人： Douglas A. Wicks , Robert J. Kumpf , Sze-Ming Lee , Duane B. Priddy, Jr. , Philip E. Yeske
IPC分类号： C08L75/00 , C08G18/08 , C08G18/10 , C08G18/80 , C08G18/74
CPC分类号： C08G18/8012 , C08G18/0852 , C08G18/10 , C08G2101/00 , C08G2120/00
摘要： The present invention relates to heat-curable, cyclic isocyanate addition products i) which are the reaction products of a polyisocyanate having two or more isocyanate groups with a compound containing two or more isocyanate-reactive groups and ii) in which at least 10% by weight of the reaction products are in the form of cyclic groups containing urea and/or urethane groups. The present invention also relates to a process for the preparation of these cyclic isocyanate addition products and to the products obtained by curing these compositions at elevated temperatures, e.g., coatings, adhesives, molded articles, elastomers and foams.
摘要翻译：本发明涉及作为具有两个以上异氰酸酯基团的多异氰酸酯与含有两个以上异氰酸酯反应性基团的化合物的反应产物的可热固化的环状异氰酸酯加合物i），和ii）其中至少10％反应产物的重量为含脲和/或氨基甲酸酯基团的环状基团的形式。本发明还涉及一种制备这些环状异氰酸酯加成产物的方法以及通过在高温下固化这些组合物获得的产品，例如涂料，粘合剂，模塑制品，弹性体和泡沫。

7. 发明授权

US5691439A Low surface energy polyisocyanates and their use in one- or two-component coating compositions 失效
标题翻译：低表面能多异氰酸酯及其在单组分或双组分涂料组合物中的用途
公开(公告)号：US5691439A
公开(公告)日：1997-11-25
申请号：US767056
申请日：1996-12-16
申请人： William E. Slack , Philip E. Yeske , Edward P. Squiller
发明人： William E. Slack , Philip E. Yeske , Edward P. Squiller
IPC分类号： C08G18/02 , C08G18/61 , C08G18/71 , C08G18/73 , C08G18/77 , C08G18/78 , C08G18/79 , C09D175/04
CPC分类号： C09D175/04 , C08G18/61 , C08G18/718 , C08G18/7831 , C08G18/7837
摘要： The present invention relates to polyisocyanate adducts containing allophanate groups, siloxane groups and optionally isocyanurate groups that are prepared by reacting compounds a) which i) are substantially free of hydroxyl groups and isocyanate groups, ii) have an average of at least two urethane groups per molecule and iii) contain 0 to 50% by weight of siloxane groups, based on the weight of the polyisocyanate adducts, with an excess quantity, based on the equivalents of urethane groups, of polyisocyanates b), which optionally contain siloxane groups, to form polyisocyanate adducts and optionally removing at least a portion of the unreacted excess polyisocyanates b), provided that compounds a) and polyisocyanates b) contain a total of at least 0.001% by weight, of siloxane groups, based on the weight of the polyisocyanate adducts. The present invention also relates to a process for preparing these polyisocyanates adducts, to blends of the polyisocyanates with other polyisocyanates that which do not contain siloxane groups and to the use of the polyisocyanate adducts or polyisocyanate blends, optionally in blocked form, in one- or two-component coating compositions.
摘要翻译：本发明涉及含有脲基甲酸酯基团，硅氧烷基团和任选的异氰脲酸酯基团的多异氰酸酯加合物，其通过使i）基本上不含羟基和异氰酸酯基团的化合物a）制备，ii）平均具有至少两个氨基甲酸酯基团分子和iii）包含0至50重量％的硅氧烷基团，基于多异氰酸酯加合物的重量，基于氨基甲酸酯基团的当量，任选地含有硅氧烷基团的多异氰酸酯b）的过量形成多异氰酸酯加合物和任选地除去至少一部分未反应的过量多异氰酸酯b），条件是化合物a）和多异氰酸酯b）基于多异氰酸酯加合物的重量含有至少0.001重量％的硅氧烷基团。本发明还涉及制备这些多异氰酸酯加合物的方法，多异氰酸酯与不含硅氧烷基团的其它多异氰酸酯的共混物，以及任选地以封闭形式使用多异氰酸酯加合物或多异氰酸酯共混物，双组分涂料组合物。

8. 发明授权

US5574122A Low surface energy polyisocyanates and their use in one- or two-component coating compositions 失效
标题翻译：低表面能多异氰酸酯及其在单组分或双组分涂料组合物中的用途
公开(公告)号：US5574122A
公开(公告)日：1996-11-12
申请号：US536556
申请日：1995-09-29
申请人： Philip E. Yeske , Edward P. Squiller , William E. Slack
发明人： Philip E. Yeske , Edward P. Squiller , William E. Slack
IPC分类号： C08G18/61 , C08G18/28 , C08G18/77 , C08G18/78 , C08G18/79 , C08G18/80 , C09D175/00 , C09D175/04 , C07C269/02 , C07F7/10
CPC分类号： C08G18/809 , C08G18/289 , C08G18/7837 , C08G18/791
摘要： The present invention is directed to a polyisocyanate mixturei) having an NCO content of 5 to 35% by weight and prepared from an organic diisocyanate,ii) containing up to 25% by weight of isocyanurate groups (calculated as N.sub.3, C.sub.3, O.sub.3, MW 126),iii) containing allophanate groups in an amount such that there are more equivalents of allophanate groups than urethane or urea groups and such that the polyisocyanate mixture remains stable and homogeneous in storage for 3 months at 25.degree. C. andiv) containing siloxane groups (calculated as SiO, MW 44) in an amount of 0.002 to 50% by weight,wherein the preceding percentages are based on the solids content of the polyisocyanate mixture, excluding any unreacted organic diisocyanate, and wherein the siloxane groups are incorporated by reacting an isocyanate group with a compound containing one isocyanate-reactive group directly attached to a carbon atom and one or more siloxane groups. The present invention is also directed to a process for the production of this polyisocyanate mixture and to its use, optionally in blocked form, as an isocyanate component in one- or two-component coating compositions.
摘要翻译：本发明涉及NCO含量为5-35重量％并由有机二异氰酸酯制备的多异氰酸酯混合物，ii）含有至多25重量％的异氰脲酸酯基（以N 3，C 3，O 3， MW 126），iii）含有脲基甲酸酯基团，其量使得比氨基甲酸酯或脲基团具有更多当量的脲基甲酸酯基团，并且使得多异氰酸酯混合物在25℃保存3个月时保持稳定和均匀，并且iv）含硅氧烷基团（以SiO，MW 44计），其量为0.002至50重量％，其中前述百分比是基于多异氰酸酯混合物的固体含量，不包括任何未反应的有机二异氰酸酯，并且其中硅氧烷基团通过使异氰酸酯基与含有直接连接到碳原子和一个或多个硅氧烷基团的一个异氰酸酯反应性基团的化合物反应。本发明还涉及在单组分或双组分涂料组合物中制备该多异氰酸酯混合物及其用途，任选为封闭形式的异氰酸酯组分的方法。

9. 发明授权

US5243012A Polyurea coating compositions having improved pot lives 失效
标题翻译：具有改善适用期的聚脲涂料组合物
公开(公告)号：US5243012A
公开(公告)日：1993-09-07
申请号：US896702
申请日：1992-06-10
申请人： Douglas A. Wicks , Philip E. Yeske
发明人： Douglas A. Wicks , Philip E. Yeske
IPC分类号： C09D175/02 , C08G18/38 , C09D175/00
CPC分类号： C08G18/3821
摘要： The present invention relates to a coating composition for the preparation of a polyurea coating which containsa) a polyisocyanate component,b) at least one compound corresponding to the formula ##STR1## wherein X represents an organic group which has a valency of n and is inert towards isocyanate groups at a temperature of 100.degree. C. or less,R.sup.1 and R.sup.2 may be identical or different and represent organic groups which are inert towards isocyanate groups at a temperature of 100.degree. C. or less,R.sup.3 and R.sup.4 may be identical or different and represent hydrogen or organic groups which are inert towards isocyanate groups at a temperature of 100.degree. C. or less andn represents an integer with a value of at least 2, andc) 0.001 to 5 weight percent, based on the weight of components a) and b), of a tin(IV) compound which is a catalyst for the reaction between isocyanate groups and hydroxyl groups.

10. 发明授权

US5777061A Blocked polyisocyanate crosslinkers for providing improved flow properties to coating compositions 失效
标题翻译：封闭的多异氰酸酯交联剂，用于为涂料组合物提供改进的流动性能
公开(公告)号：US5777061A
公开(公告)日：1998-07-07
申请号：US601597
申请日：1996-02-14
申请人： Kenneth P. Yonek , Lanny D. Venham , Philip E. Yeske , Edward P. Squiller
发明人： Kenneth P. Yonek , Lanny D. Venham , Philip E. Yeske , Edward P. Squiller
IPC分类号： C08G18/48 , C08G18/77 , C08G18/78 , C08G18/79 , C08G18/80 , C09D5/03 , C09D175/00 , C09D175/06 , C08G18/28
CPC分类号： C08G18/8064 , C08G18/7837 , C08G18/792 , C08G18/807 , C08G18/8087 , C08G2150/20 , Y10T428/31547 , Y10T428/31551
摘要： The present invention is directed to a powder coating composition containing as binder A) a polyisocyanate component which contains blocked isocyanate groups, is present in powder form, is solid below 40.degree. C. and liquid above 150.degree. C., and contains one or more polyisocyanates i) having a blocked NCO content (calculated as NCO, MW 42) of 5 to 25% by weight and ii) containing fluorine (calculated as F, AW 19) in an amount of 0.01 to 20% by weight, wherein the preceding percentages are based on the solids content of the polyisocyanate mixture and B) a polyhydroxyl component containing one or more high molecular weight polyols.
摘要翻译：本发明涉及含有作为粘合剂的粉末涂料组合物A）含有封端异氰酸酯基团的多异氰酸酯组分，以粉末形式存在，固体低于40℃，液体高于150℃，并含有一种或多种多异氰酸酯i）具有5至25重量％的阻塞NCO含量（以NCO计，MW 42计）和ii）含有0.01-20重量％的氟（按F，AW 19计算），其中前述百分数是基于多异氰酸酯混合物的固体含量和B）含有一种或多种高分子量多元醇的多羟基组分。

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