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1. 发明申请

US20120028029A1 HIGHLY ORDERED ARRAYS OF NANOHOLES IN METALLIC FILMS AND METHODS FOR PRODUCING THE SAME 有权
标题翻译：金属膜中的高分子量纳米颗粒及其生产方法
公开(公告)号：US20120028029A1
公开(公告)日：2012-02-02
申请号：US13203985
申请日：2009-03-05
申请人： Claudia Pacholski , Stefan B. Quint
发明人： Claudia Pacholski , Stefan B. Quint
IPC分类号： B32B3/26 , B05D3/12 , B05D3/02 , B05D5/00 , B05D3/00 , B82Y99/00 , B82Y40/00
CPC分类号： B05D1/005 , B05D1/322 , B82Y30/00 , B82Y40/00 , C23C18/1605 , C23C18/1689 , C23C18/1692 , C23C18/1882 , C23C18/44 , G01N21/554 , Y10T428/249978
摘要： The present invention relates to highly ordered arrays of nanoholes in metallic films and to an improved method for producing the same. The method according to the invention for producing an highly ordered array of nanoholes in metallic films on a substrate comprises the following steps: a) providing microspheres comprising poly-N-isopropylamide (polyNIPAM), the microspheres being selected from pure poly-N-isopropyl-amide (polyNIPAM) hydrogel microspheres and polymeric or inorganic beads carrying poly-N-isopropylamide (polyNIPAM) hydrogel chains, b) coating an aqueous dispersion of said microspheres onto a substrate and drying the dispersion, which results in a non-close packed ordered array of the microspheres, c) generating a metallic film on the substrate, d) removing the microspheres from the surface of the substrate which results in an ordered array of nanoholes on the substrate, and e) optionally increasing the thickness of the metallic film by selective electroless plating.
摘要翻译：本发明涉及金属膜中纳米孔高度排列的阵列及其制造方法。根据本发明的用于在衬底上的金属膜中制造高度排列的纳米孔阵列的方法包括以下步骤：a）提供包含聚-N-异丙基酰胺（polyNIPAM）的微球，所述微球选自纯的聚-N-异丙基 - 聚酰胺（polyNIPAM）水凝胶微球和携带聚-N-异丙酰胺（polyNIPAM）水凝胶链的聚合物或无机珠，b）将所述微球的水性分散体涂布在基材上并干燥分散体，这导致非紧密堆积的有序微球的阵列，c）在衬底上产生金属膜，d）从衬底表面去除微球，导致在衬底上形成有序排列的纳米孔，以及e）可选地增加金属膜的厚度选择性化学镀。

2. 发明授权

US09132445B2 Highly ordered arrays of nanoholes in metallic films and methods for producing the same 有权
标题翻译：金属膜中的高排列纳米孔阵列及其制造方法
公开(公告)号：US09132445B2
公开(公告)日：2015-09-15
申请号：US13203985
申请日：2009-03-05
申请人： Claudia Pacholski , Stefan B. Quint
发明人： Claudia Pacholski , Stefan B. Quint
IPC分类号： C23C14/04 , C23C18/06 , B05D1/00 , B05D1/32 , B82Y30/00 , B82Y40/00 , C23C18/16 , C23C18/18 , C23C18/44 , G01N21/552
CPC分类号： B05D1/005 , B05D1/322 , B82Y30/00 , B82Y40/00 , C23C18/1605 , C23C18/1689 , C23C18/1692 , C23C18/1882 , C23C18/44 , G01N21/554 , Y10T428/249978
摘要： The present invention relates to highly ordered arrays of nanoholes in metallic films and to an improved method for producing the same. The method according to the invention for producing an highly ordered array of nanoholes in metallic films on a substrate comprises the following steps: a) providing microspheres comprising poly-N-isopropylamide (polyNIPAM), the microspheres being selected from pure poly-N-isopropyl-amide (polyNIPAM) hydrogel microspheres and polymeric or inorganic beads carrying poly-N-isopropylamide (polyNIPAM) hydrogel chains, b) coating an aqueous dispersion of said microspheres onto a substrate and drying the dispersion, which results in a non-close packed ordered array of the microspheres, c) generating a metallic film on the substrate, d) removing the microspheres from the surface of the substrate which results in an ordered array of nanoholes on the substrate, and e) optionally increasing the thickness of the metallic film by selective electroless plating.
摘要翻译：本发明涉及金属膜中纳米孔高度排列的阵列及其制造方法。根据本发明的用于在衬底上的金属膜中制造高度排列的纳米孔阵列的方法包括以下步骤：a）提供包含聚-N-异丙基酰胺（polyNIPAM）的微球，所述微球选自纯的聚-N-异丙基 - 聚酰胺（polyNIPAM）水凝胶微球和携带聚-N-异丙酰胺（polyNIPAM）水凝胶链的聚合物或无机珠，b）将所述微球的水性分散体涂布在基材上并干燥分散体，这导致非紧密堆积的有序微球的阵列，c）在衬底上产生金属膜，d）从衬底表面去除微球，导致在衬底上形成有序排列的纳米孔，以及e）可选地增加金属膜的厚度选择性化学镀。

3. 发明授权

US09090987B2 Highly ordered arrays of colloidal 2D crystals and methods for producing the same 有权
标题翻译：高度有序的胶体二维晶体阵列及其制备方法
公开(公告)号：US09090987B2
公开(公告)日：2015-07-28
申请号：US14003005
申请日：2011-03-04
申请人： Stefan B. Quint , Claudia Pacholski
发明人： Stefan B. Quint , Claudia Pacholski
IPC分类号： C30B7/02 , B81C1/00 , B82Y40/00 , H01L21/027 , H01L21/033 , H01L21/311 , C03C17/00 , C23C18/16 , B05D1/18 , C30B29/58 , B05D1/00 , B05D3/12
CPC分类号： C30B7/02 , B05D1/00 , B05D1/005 , B05D1/18 , B05D3/12 , B81C1/00031 , B82Y40/00 , C03C17/007 , C23C18/1605 , C30B29/58 , H01L21/0271 , H01L21/0337 , H01L21/31144
摘要： The present invention relates to highly ordered arrays of colloidal 2D crystals on a substrate and to an improved method for producing the same. The method according to the invention for producing an highly ordered array of colloidal 2D crystals on a substrate comprises the following steps: a) providing a suspension of microspheres comprising poly-N-isopropylamide (polyNIPAM), the microspheres being selected from pure poly-N-isopropylamide (polyNIPAM) hydrogel microspheres, functionalized polyNIPAM microspheres, and polymeric or inorganic beads carrying poly-N-isopropyl-amide (polyNIPAM) hydrogel chains, in an aqueous medium on a substrate, wherein the aqueous medium comprises a mixture of water and a lower alkyl alcohol, b) subjecting the suspension deposited on the substrate after step a) to a shear force, and c) drying the suspension. In a preferred embodiment of the invention, the shear force is generated by applying a pulsed gas stream to the substrate surface. The colloidal 2D crystal arrays obtained by this method have an exceptional high long range order, including monocrystalline domains in the range of square millimeters.
摘要翻译：本发明涉及衬底上胶体二维晶体的高度有序阵列及其制备方法。根据本发明的用于在基材上生产高度有序排列的胶体2D晶体的方法包括以下步骤：a）提供包含聚-N-异丙基酰胺（polyNIPAM）的微球的悬浮液，所述微球选自纯多晶N - 异丙基酰胺（polyNIPAM）水凝胶微球，功能化聚NIPAM微球，以及在基底上的水性介质中携带聚-N-异丙酰胺（polyNIPAM）水凝胶链的聚合或无机小珠，其中水性介质包含水和低级烷基醇，b）在步骤a）之后使沉积在基材上的悬浮液经受剪切力，和c）干燥悬浮液。在本发明的优选实施例中，剪切力通过将脉冲气流施加到基底表面而产生。通过该方法获得的胶体2D晶体阵列具有特别高的长范围顺序，包括在平方毫米范围内的单晶畴。

4. 发明申请

US20130338303A1 HIGHLY ORDERED ARRAYS OF COLLOIDAL 2D CRYSTALS AND METHODS FOR PRODUCING THE SAME 有权
标题翻译：胶体二维晶体的高阶阵列及其生产方法
公开(公告)号：US20130338303A1
公开(公告)日：2013-12-19
申请号：US14003005
申请日：2011-03-04
申请人： Stefan B. Quint , Claudia Pacholski
发明人： Stefan B. Quint , Claudia Pacholski
IPC分类号： C30B7/02 , C30B29/58
CPC分类号： C30B7/02 , B05D1/00 , B05D1/005 , B05D1/18 , B05D3/12 , B81C1/00031 , B82Y40/00 , C03C17/007 , C23C18/1605 , C30B29/58 , H01L21/0271 , H01L21/0337 , H01L21/31144
摘要： The present invention relates to highly ordered arrays of colloidal 2D crystals on a substrate and to an improved method for producing the same. The method according to the invention for producing an highly ordered array of colloidal 2D crystals on a substrate comprises the following steps: a) providing a suspension of microspheres comprising poly-N-isopropylamide (polyNIPAM), the microspheres being selected from pure poly-N-isopropylamide (polyNIPAM) hydrogel microspheres, functionalized polyNIPAM microspheres, and polymeric or inorganic beads carrying poly-N-isopropyl-amide (polyNIPAM) hydrogel chains, in an aqueous medium on a substrate, wherein the aqueous medium comprises a mixture of water and a lower alkyl alcohol, b) subjecting the suspension deposited on the substrate after step a) to a shear force, and c) drying the suspension. In a preferred embodiment of the invention, the shear force is generated by applying a pulsed gas stream to the substrate surface. The colloidal 2D crystal arrays obtained by this method have an exceptional high long range order, including monocrystalline domains in the range of square millimetres.
摘要翻译：本发明涉及衬底上胶体二维晶体的高度有序阵列及其制备方法。根据本发明的用于在基材上生产高度有序排列的胶体2D晶体的方法包括以下步骤：a）提供包含聚-N-异丙基酰胺（polyNIPAM）的微球的悬浮液，所述微球选自纯多晶N - 异丙基酰胺（polyNIPAM）水凝胶微球，功能化聚NIPAM微球，以及在基底上的水性介质中携带聚-N-异丙酰胺（polyNIPAM）水凝胶链的聚合物或无机珠，其中水性介质包含水和低级烷基醇，b）在步骤a）之后使沉积在基材上的悬浮液经受剪切力，和c）干燥悬浮液。在本发明的优选实施例中，剪切力通过将脉冲气流施加到基底表面而产生。通过该方法获得的胶体2D晶体阵列具有特别高的长范围顺序，包括在平方毫米范围内的单晶畴。

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