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    • 7. 发明授权
    • Method of preparing molecular sieve SSZ-74
    • 制备分子筛SSZ-74的方法
    • US07569207B2
    • 2009-08-04
    • US12039291
    • 2008-02-28
    • Stacey I. ZonesAllen W. Burton
    • Stacey I. ZonesAllen W. Burton
    • C01B33/36B01J29/04B01J21/00
    • C01B37/02C01B39/48
    • A method of preparing a crystalline material, herein designated as SSZ-74, comprising contacting under crystallization conditions (1) a source of silicon oxide, (2) a source of another metal oxide, (3) fluoride ions, and (4) a structure directing agent comprising a hexamethylene-1,6-bis-(N-methyl-N-pyrrolidinium)dication. A method of preparing a crystalline material having a defined X-ray powder diffraction pattern, by (1) forming a reaction mixture having one or more metal oxides, one being silicon oxide, and a hexamethylene-1,6-bis-(N-methyl-N-pyrrolidinium)dication, (2) maintaining the reaction mixture at an elevated temperature until crystals are formed, (3) separating the crystalline material, and (4) optionally calcining the crystalline material. A method for preparing a crystalline material, comprising (1) forming a defined reaction mixture, (2) maintaining the reaction mixture under conditions where crystals are formed, (3) separating out the crystalline material, and (4) water-washing and drying the crystalline material such that it has a defined X-ray powder diffraction pattern.
    • 一种制备结晶材料的方法,这里称为SSZ-74,包括在结晶条件下接触(1)氧化硅源,(2)另一种金属氧化物源,(3)氟离子,和(4) 结构导向剂包含六亚甲基-1,6-双 - (N-甲基-N-吡咯烷鎓)二阳离子。 (1)形成具有一种或多种金属氧化物的反应混合物,一种是氧化硅和六亚甲基-1,6-双 - (N-甲基-2-吡咯烷酮)的制备具有规定的X射线粉末衍射图的结晶材料的方法, (2)将反应混合物保持在高温直到形成晶体,(3)分离结晶材料,和(4)任选地煅烧结晶材料。 一种制备结晶材料的方法,包括(1)形成规定的反应混合物,(2)在形成晶体的条件下保持反应混合物,(3)分离结晶材料,和(4)水洗和干燥 结晶材料使得其具有限定的X射线粉末衍射图。