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1. 发明授权

US10273359B2 Polyamide resin composition 有权
公开(公告)号：US10273359B2
公开(公告)日：2019-04-30
申请号：US13395535
申请日：2010-09-14
申请人： Shun Ogawa , Hisayuki Kuwahara , Shinichi Ayuba , Takahiko Sumino , Kentaro Ishii
发明人： Shun Ogawa , Hisayuki Kuwahara , Shinichi Ayuba , Takahiko Sumino , Kentaro Ishii
IPC分类号： C08L77/06 , C08G69/26
摘要： Disclosed is a polyamide resin composition, including: a polyamide (A) containing a diamine unit including 70 mol % or more of a p-xylylenediamine unit and a dicarboxylic acid unit including 70 mol % or more of a linear aliphatic dicarboxylic acid unit having 6 to 18 carbon atoms; and a filler (B), in which the polyamide (A) includes a polyamide having a phosphorus atom concentration of 50 to 1,000 ppm and a YI value of 10 or less in a color difference test in accordance with JIS-K-7105, and a content of the filler (B) is 1 to 200 parts by mass with respect to 100 parts by mass of the polyamide (A).

2. 发明授权

US08440756B2 Flame-retardant polyamide resin composition 有权
标题翻译：阻燃聚酰胺树脂组合物
公开(公告)号：US08440756B2
公开(公告)日：2013-05-14
申请号：US13395541
申请日：2010-09-14
申请人： Kentaro Ishii , Hisayuki Kuwahara , Shun Ogawa , Shinichi Ayuba , Takahiko Sumino
发明人： Kentaro Ishii , Hisayuki Kuwahara , Shun Ogawa , Shinichi Ayuba , Takahiko Sumino
IPC分类号： C08K5/03
CPC分类号： C08L77/06 , C08K3/2279 , C08L25/18
摘要： Disclosed is a flame-retardant polyamide resin composition, including: a polyamide (A) containing a diamine unit including 70 mol % or more of a p-xylylenediamine unit and a dicarboxylic acid unit including 70 mol % or more of a linear aliphatic dicarboxylic acid unit having 6 to 18 carbon atoms; an organic halogen compound (B) that serves as a flame retardant; an inorganic compound (C) that serves as a flame retardant aid; and an inorganic filler (D), in which the polyamide (A) includes a polyamide having a phosphorus atom concentration of 50 to 1,000 ppm and a YI value of 10 or less in a color difference test in accordance with JIS-K-7105, and a content of the organic halogen compound (B), a content of the inorganic compound (C), and a content of the inorganic filler (D) are 1 to 100 parts by mass, 0.5 to 50 parts by mass, and 0 to 100 parts by mass, respectively, with respect to 100 parts by mass of the polyamide (A).
摘要翻译：公开了一种阻燃性聚酰胺树脂组合物，其包含：含有70摩尔％以上的对苯二甲胺单元的二胺单元的聚酰胺（A）和包含70摩尔％以上的直链脂肪族二羧酸的二羧酸单元具有6至18个碳原子的单元; 用作阻燃剂的有机卤素化合物（B）; 用作阻燃助剂的无机化合物（C）; 和无机填料（D），其中聚酰胺（A）在根据JIS-K-7105的色差试验中包含磷原子浓度为50〜1000ppm，YI值为10以下的聚酰胺，有机卤素化合物（B）的含量，无机化合物（C）的含量和无机填料（D）的含量为1〜100质量份，为0.5〜50质量份，0〜相对于100质量份的聚酰胺（A），分别为100质量份。

3. 发明申请

US20120172512A1 FLAME-RETARDANT POLYAMIDE RESIN COMPOSITION 有权
标题翻译：阻燃聚酰胺树脂组合物
公开(公告)号：US20120172512A1
公开(公告)日：2012-07-05
申请号：US13395541
申请日：2010-09-14
申请人： Kentaro Ishii , Hisayuki Kuwahara , Shun Ogawa , Shinichi Ayuba , Takahiko Sumino
发明人： Kentaro Ishii , Hisayuki Kuwahara , Shun Ogawa , Shinichi Ayuba , Takahiko Sumino
IPC分类号： C08L77/06 , C08K3/18 , C08K3/38 , C08K3/26 , C08K3/30 , C08K7/14 , C08K3/40 , C08K7/06 , C08K3/36 , C08K3/04 , C08K3/22 , C08K3/34
CPC分类号： C08L77/06 , C08K3/2279 , C08L25/18
摘要： Disclosed is a flame-retardant polyamide resin composition, including: a polyamide (A) containing a diamine unit including 70 mol % or more of a p-xylylenediamine unit and a dicarboxylic acid unit including 70 mol % or more of a linear aliphatic dicarboxylic acid unit having 6 to 18 carbon atoms; an organic halogen compound (B) that serves as a flame retardant; an inorganic compound (C) that serves as a flame retardant aid; and an inorganic filler (D), in which the polyamide (A) includes a polyamide having a phosphorus atom concentration of 50 to 1,000 ppm and a YI value of 10 or less in a color difference test in accordance with JIS-K-7105, and a content of the organic halogen compound (B), a content of the inorganic compound (C), and a content of the inorganic filler (D) are 1 to 100 parts by mass, 0.5 to 50 parts by mass, and 0 to 100 parts by mass, respectively, with respect to 100 parts by mass of the polyamide (A).
摘要翻译：公开了一种阻燃性聚酰胺树脂组合物，其包含：含有70摩尔％以上的对苯二甲胺单元的二胺单元的聚酰胺（A）和包含70摩尔％以上的直链脂肪族二羧酸的二羧酸单元具有6至18个碳原子的单元; 用作阻燃剂的有机卤素化合物（B）; 用作阻燃助剂的无机化合物（C）; 和无机填料（D），其中聚酰胺（A）在根据JIS-K-7105的色差试验中包含磷原子浓度为50〜1000ppm，YI值为10以下的聚酰胺，有机卤素化合物（B）的含量，无机化合物（C）的含量和无机填料（D）的含量为1〜100质量份，为0.5〜50质量份，0〜相对于100质量份的聚酰胺（A），分别为100质量份。

4. 发明授权

US08835596B2 Method for producing polyamide 有权
标题翻译：聚酰胺的制造方法
公开(公告)号：US08835596B2
公开(公告)日：2014-09-16
申请号：US13119249
申请日：2009-09-11
申请人： Hisayuki Kuwahara , Tomomichi Kanda , Shun Ogawa , Shinichi Ayuba , Kentaro Ishii , Takahiko Sumino
发明人： Hisayuki Kuwahara , Tomomichi Kanda , Shun Ogawa , Shinichi Ayuba , Kentaro Ishii , Takahiko Sumino
IPC分类号： C08G69/28
CPC分类号： C08G69/28
摘要： A method of producing polyamide by the direct polycondensation of a diamine component and a dicarboxylic acid component without using a solvent, such as water. The diamine component containing 70 mol % or more of p-xylylenediamine is added to a reaction system containing the dicarboxylic acid component under pressure while maintaining the reaction system in a molten state. After the addition of the diamine component, the pressure of the reaction system is reduced to atmospheric pressure over 50 min or more at a pressure falling speed of 1.0 MPa/h or less. By the production method, polyamide with a small molecular weight dispersion is easily produced.
摘要翻译：通过二胺成分和二羧酸成分的直接缩聚而不使用溶剂如水来生产聚酰胺的方法。将含有70摩尔％以上的对苯二甲胺的二胺成分加入到含有二羧酸成分的反应体系中，同时保持反应体系处于熔融状态。加入二胺成分后，在1.0MPa / h以下的压力下降速度下，反应体系的压力在50分钟以上降至大气压。通过该制造方法，容易制造分子量分散性小的聚酰胺。

5. 发明申请

US20120177937A1 POLYAMIDE RESIN COMPOSITION 审中-公开
标题翻译：聚酰胺树脂组合物
公开(公告)号：US20120177937A1
公开(公告)日：2012-07-12
申请号：US13395535
申请日：2010-09-14
申请人： Shun Ogawa , Hisayuki Kuwahara , Shinichi Ayuba , Takahiko Sumino , Kentaro Ishii
发明人： Shun Ogawa , Hisayuki Kuwahara , Shinichi Ayuba , Takahiko Sumino , Kentaro Ishii
IPC分类号： C08L77/06 , C08K7/14 , C08K7/06 , C08K3/34 , C08K3/30 , B32B27/34 , C08K3/26 , C08K3/22 , C08K3/10 , B32B15/088 , C08L27/18 , C08L1/02 , C08K3/28
CPC分类号： C08L77/06 , C08G69/26 , C08G69/265 , Y10T428/31681
摘要： Disclosed is a polyamide resin composition, including: a polyamide (A) containing a diamine unit including 70 mol % or more of a p-xylylenediamine unit and a dicarboxylic acid unit including 70 mol % or more of a linear aliphatic dicarboxylic acid unit having 6 to 18 carbon atoms; and a filler (B), in which the polyamide (A) includes a polyamide having a phosphorus atom concentration of 50 to 1,000 ppm and a YI value of 10 or less in a color difference test in accordance with JIS-K-7105, and a content of the filler (B) is 1 to 200 parts by mass with respect to 100 parts by mass of the polyamide (A).
摘要翻译：公开了一种聚酰胺树脂组合物，其包含：含有70摩尔％以上的对苯二甲胺单元的二胺单元的聚酰胺（A）和含有70摩尔％以上的具有6个碳原子的直链脂肪族二羧酸单元的二羧酸单元至18个碳原子; 和填料（B），其中聚酰胺（A）在根据JIS-K-7105的色差试验中包含磷原子浓度为50〜1000ppm，YI值为10以下的聚酰胺，以及相对于100质量份的聚酰胺（A），填料（B）的含量为1〜200质量份。

6. 发明申请

US20120065327A1 POLYAMIDE RESIN 审中-公开
标题翻译：聚酰胺树脂
公开(公告)号：US20120065327A1
公开(公告)日：2012-03-15
申请号：US13322519
申请日：2010-05-28
申请人： Shun Ogawa , Shinichi Ayuba , Takahiko Sumino , Hisayuki Kuwahara , Kentaro Ishii
发明人： Shun Ogawa , Shinichi Ayuba , Takahiko Sumino , Hisayuki Kuwahara , Kentaro Ishii
IPC分类号： C08G69/30 , C08L77/06 , C08G69/26
CPC分类号： C08G69/30 , C08G69/26 , C08G69/28 , C08K3/34 , C08K5/0083 , C08K11/00 , C08L77/06
摘要： A polyamide resin which comprises a diamine unit containing 70 mol % or more of a paraxylylenediamine unit and a dicarboxylic acid unit containing 70 mol % or more of a linear aliphatic dicarboxylic acid unit having from 6 to 18 carbon atoms, and which has a phosphorus atom concentration of from 50 to 1,000 ppm and a YI value of 10 or less in the color difference test in accordance with JIS-K-7105.
摘要翻译：一种聚酰胺树脂，其包含含有70摩尔％以上的对苯二甲苯单元的二胺单元和含有70摩尔％以上的碳原子数为6〜18的直链脂肪族二羧酸单元的二羧酸单元，其具有磷原子浓度为50〜1000ppm，YI值为10以下的色差试验中按照JIS-K-7105。

7. 发明申请

US20110245454A1 METHOD FOR PRODUCING POLYAMIDE 有权
标题翻译：生产聚酰胺的方法
公开(公告)号：US20110245454A1
公开(公告)日：2011-10-06
申请号：US13119249
申请日：2009-09-11
申请人： Hisayuki Kuwahara , Tomomichi Kanda , Shun Ogawa , Shinichi Ayuba , Kentaro Ishii , Takahiko Sumino
发明人： Hisayuki Kuwahara , Tomomichi Kanda , Shun Ogawa , Shinichi Ayuba , Kentaro Ishii , Takahiko Sumino
IPC分类号： C08G69/28
CPC分类号： C08G69/28
摘要： A method of producing polyamide by the direct polycondensation of a diamine component and a dicarboxylic acid component without using a solvent, such as water. The diamine component containing 70 mol % or more of p-xylylenediamine is added to a reaction system containing the dicarboxylic acid component under pressure while maintaining the reaction system in a molten state. After the addition of the diamine component, the pressure of the reaction system is reduced to atmospheric pressure over 50 min or more at a pressure falling speed of 1.0 MPa/h or less. By the production method, polyamide with a small molecular weight dispersion is easily produced.
摘要翻译：通过二胺成分和二羧酸成分的直接缩聚而不使用溶剂如水来生产聚酰胺的方法。将含有70摩尔％以上的对苯二甲胺的二胺成分加入到含有二羧酸成分的反应体系中，同时保持反应体系处于熔融状态。加入二胺成分后，在1.0MPa / h以下的压力下降速度下，反应体系的压力在50分钟以上降至大气压。通过该制造方法，容易制造分子量分散性小的聚酰胺。

8. 发明申请

US20130123439A1 REACTIVE POLYAMIDE RESINS AND POLYAMIDE RESIN COMPOSITIONS 有权
标题翻译：反应性聚酰胺树脂和聚酰胺树脂组合物
公开(公告)号：US20130123439A1
公开(公告)日：2013-05-16
申请号：US13809499
申请日：2012-05-18
申请人： Jun Mitadera , Shinichi Ayuba , Nobuhiko Matsumoto , Kosuke Otsuka
发明人： Jun Mitadera , Shinichi Ayuba , Nobuhiko Matsumoto , Kosuke Otsuka
IPC分类号： C08G69/26 , C08L77/06
CPC分类号： C08G69/26 , C08K7/14 , C08L77/06 , C08L21/00
摘要： Provided is a polyamide resin composition comprising an elastomer etc, and a reactive polyamide resin excellent in reactivity. The polyamide resin composition comprises 0.5 to 100 parts by mass of an elastomer per 100 parts by mass of a reactive polyamide resin, wherein the reactive polyamide resin obtained by polycondensing a diamine (A) containing 70 mol % or more of a diamine structural unit derived from xylylenediamine and a dicarboxylic acid (B) containing 50 mol % or more of a dicarboxylic acid structural unit derived from sebacic acid, and has a concentration of reactive functional groups of 100 μeq/g or more and a molar ratio of reacted diamine to reacted dicarboxylic acid (the number of moles of reacted diamine/the number of moles of reacted dicarboxylic acid) of 1.0 or more.
摘要翻译：提供包含弹性体的聚酰胺树脂组合物和反应性优异的活性聚酰胺树脂。聚酰胺树脂组合物包含相对于反应性聚酰胺树脂100质量份为0.5〜100质量份的弹性体，其中通过缩聚含有70摩尔％以上的二胺结构单元的二胺（A）得到的反应性聚酰胺树脂得到来自苯二甲胺和含有50mol％以上的来自癸二酸的二羧酸结构单元的二羧酸（B），反应性官能团的浓度为100mueq / g以上，反应二胺与反应性的摩尔比二羧酸（反应二胺的摩尔数/反应的二羧酸的摩尔数）为1.0以上。

9. 发明授权

US08128782B2 Amine epoxy resin curing agent, gas barrier epoxy resin composition comprising the curing agent, coating agent, and adhesive agent for laminate 有权
标题翻译：胺环氧树脂固化剂，阻气性环氧树脂组合物，其包含固化剂，涂层剂和层压粘合剂
公开(公告)号：US08128782B2
公开(公告)日：2012-03-06
申请号：US12600114
申请日：2008-05-20
申请人： Shinichi Yonehama , Shigeyuki Hirose , Shinichi Ayuba , Eiichi Honda , Masayoshi Takahashi , Kana Kumamoto
发明人： Shinichi Yonehama , Shigeyuki Hirose , Shinichi Ayuba , Eiichi Honda , Masayoshi Takahashi , Kana Kumamoto
IPC分类号： C09J163/00 , C08L63/00 , C08G69/00 , C08G71/00 , B32B27/26 , B32B27/38
CPC分类号： C08G59/50 , B32B7/12 , B32B27/08 , B32B27/34 , B32B27/38 , B32B2255/20 , B32B2307/306 , B32B2307/714 , B32B2307/7242 , B32B2307/7265 , B32B2439/00 , C09D163/00 , C09J163/00
摘要： The present invention provides an amine based epoxy resin curing agent and an epoxy resin composition containing the curing agent. The epoxy resin composition has a high gas barrier performance, a long pot life, and utility as a coating material or an adhesive for laminates. The amine based epoxy resin curing agent is composed of a reaction product of (A), (B) and (D) or (A), (B), (C) and (D): (A) m-xylylenediamine or p-xylylenediamine; (B) a polyfunctional compound having at least one acyl group, which is capable of forming an amide group site through a reaction with a polyamine and forming an oligomer; (C) a monovalent carboxylic acid having from 1 to 8 carbon atoms and/or its derivative; and (D) a functional compound having at least one carbonate site represented by the formula (2), which is capable of forming a carbamate site represented by the formula (1) through a reaction with a polyamine:
摘要翻译：本发明提供一种胺系环氧树脂固化剂和含有固化剂的环氧树脂组合物。环氧树脂组合物具有高的阻气性能，较长的适用期，以及作为涂料或层压材料的粘合剂的用途。胺基环氧树脂固化剂由（A），（B）和（D）或（A），（B），（C）和（D）的反应产物组成：（A）间苯二甲胺或苯二甲胺（B）具有至少一个酰基的多官能化合物，其能够通过与多胺的反应形成酰胺基位点并形成低聚物; （C）具有1至8个碳原子的一价羧酸和/或其衍生物; 和（D）具有至少一个由式（2）表示的碳酸酯位点的官能化合物，其能够通过与多胺的反应形成由式（1）表示的氨基甲酸酯位点：

10. 发明授权

US08993677B2 Reactive polyamide resins and polyamide resin compositions 有权
标题翻译：活性聚酰胺树脂和聚酰胺树脂组合物
公开(公告)号：US08993677B2
公开(公告)日：2015-03-31
申请号：US13809499
申请日：2012-05-18
申请人： Jun Mitadera , Shinichi Ayuba , Nobuhiko Matsumoto , Kosuke Otsuka
发明人： Jun Mitadera , Shinichi Ayuba , Nobuhiko Matsumoto , Kosuke Otsuka
IPC分类号： C08L77/00 , C08L77/06 , C08G69/26 , C08K7/14
CPC分类号： C08G69/26 , C08K7/14 , C08L77/06 , C08L21/00
摘要： Provided is a polyamide resin composition comprising an elastomer etc, and a reactive polyamide resin excellent in reactivity. The polyamide resin composition comprises 0.5 to 100 parts by mass of an elastomer per 100 parts by mass of a reactive polyamide resin, wherein the reactive polyamide resin obtained by polycondensing a diamine (A) containing 70 mol % or more of a diamine structural unit derived from xylylenediamine and a dicarboxylic acid (B) containing 50 mol % or more of a dicarboxylic acid structural unit derived from sebacic acid, and has a concentration of reactive functional groups of 100 μeq/g or more and a molar ratio of reacted diamine to reacted dicarboxylic acid (the number of moles of reacted diamine/the number of moles of reacted dicarboxylic acid) of 1.0 or more.
摘要翻译：提供包含弹性体的聚酰胺树脂组合物和反应性优异的活性聚酰胺树脂。聚酰胺树脂组合物包含相对于反应性聚酰胺树脂100质量份为0.5〜100质量份的弹性体，其中通过缩聚含有70摩尔％以上的二胺结构单元的二胺（A）得到的反应性聚酰胺树脂得到由二甲苯二胺和含有50摩尔％以上的来自癸二酸的二羧酸结构单元的二羧酸（B），反应性官能团的浓度为100μeq/ g以上，反应二胺与反应性的摩尔比二羧酸（反应二胺的摩尔数/反应的二羧酸的摩尔数）为1.0以上。

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