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1. 发明申请

US20120183759A1 PROCESS FOR PRODUCING ZEOLITE FILM, AND ZEOLITE FILM OBTAINED BY THE PROCESS 有权
标题翻译：生产沸石膜的方法和由该方法获得的沸石膜
公开(公告)号：US20120183759A1
公开(公告)日：2012-07-19
申请号：US13433081
申请日：2012-03-28
申请人： Shinji NAKAMURA , Makiko Niino , Makoto Miyahara
发明人： Shinji NAKAMURA , Makiko Niino , Makoto Miyahara
IPC分类号： B32B3/00 , B05D1/30
CPC分类号： C01B39/04 , B01D53/228 , B01D67/0046 , B01D67/0051 , B01D69/02 , B01D71/028 , B01D2325/04 , C01B39/48
摘要： A process for producing a zeolite film is provided in which seed crystals thinly adhere to the surface of a support to form a thin and even zeolite film having fewer defects than conventional zeolite films. Also provided is a zeolite film obtained by the producing process. The process for producing the zeolite film comprises: a particle adhesion step of allowing a slurry, where zeolite particles which become seeds are dispersed, to flow down on the surface of a base material by the self-weight of the slurry, so that the zeolite particles adhere to the base material; and a film formation step of immersing the base material, to which the zeolite particles adhere, into a sol to carry out hydrothermal synthesis, thereby forming the zeolite film on the base material.
摘要翻译：提供了一种制备沸石膜的方法，其中晶种与载体的表面轻薄地粘合以形成比常规沸石膜具有更少缺陷的薄而均匀的沸石膜。还提供了通过制备方法获得的沸石膜。制造沸石膜的方法包括：粒子粘合步骤，其中使分散有成为种子的沸石颗粒的浆料通过浆料的自身重量在基材的表面上向下流动，使得沸石颗粒附着在基材上; 以及成膜步骤，将沉积有沸石颗粒的基材浸入溶胶中进行水热合成，从而在基材上形成沸石膜。

2. 发明授权

US08697760B2 Process for producing zeolite film, and zeolite film obtained by the process 有权
标题翻译：制备沸石膜的方法和通过该方法获得的沸石膜
公开(公告)号：US08697760B2
公开(公告)日：2014-04-15
申请号：US13433081
申请日：2012-03-28
申请人： Shinji Nakamura , Makiko Niino , Makoto Miyahara
发明人： Shinji Nakamura , Makiko Niino , Makoto Miyahara
IPC分类号： B01J49/00 , B01D53/22 , B01D71/02 , B01D15/00
CPC分类号： C01B39/04 , B01D53/228 , B01D67/0046 , B01D67/0051 , B01D69/02 , B01D71/028 , B01D2325/04 , C01B39/48
摘要： A process for producing a zeolite film is provided in which seed crystals thinly adhere to the surface of a support to form a thin and even zeolite film having fewer defects than conventional zeolite films. Also provided is a zeolite film obtained by the producing process. The process for producing the zeolite film comprises: a particle adhesion step of allowing a slurry, where zeolite particles which become seeds are dispersed, to flow down on the surface of a base material by the self-weight of the slurry, so that the zeolite particles adhere to the base material; and a film formation step of immersing the base material, to which the zeolite particles adhere, into a sol to carry out hydrothermal synthesis, thereby forming the zeolite film on the base material.
摘要翻译：提供了一种制备沸石膜的方法，其中晶种与载体的表面轻薄地粘合以形成比常规沸石膜具有更少缺陷的薄而均匀的沸石膜。还提供了通过制备方法获得的沸石膜。制造沸石膜的方法包括：粒子粘合步骤，其中使分散有成为种子的沸石颗粒的浆料通过浆料的自身重量在基材的表面上向下流动，使得沸石颗粒附着在基材上; 以及成膜步骤，将沉积有沸石颗粒的基材浸入溶胶中进行水热合成，从而在基材上形成沸石膜。

3. 发明授权

US08597612B2 Method for producing DDR zeolite 有权
标题翻译：生产DDR沸石的方法
公开(公告)号：US08597612B2
公开(公告)日：2013-12-03
申请号：US13445192
申请日：2012-04-12
申请人： Tetsuya Uchikawa , Makiko Niino
发明人： Tetsuya Uchikawa , Makiko Niino
IPC分类号： C01B39/06 , C01B39/48 , B01D53/14
CPC分类号： C01B39/06 , B01D53/14 , B01D53/22 , B01D61/364 , B01D67/0051 , B01D69/10 , B01D71/028 , B01D2253/108 , B01D2323/08 , B01D2323/34 , C01B37/02 , C01B39/48
摘要： Disclosed is a method for producing a DDR zeolite, which can be carried out using materials that are less harmful to the environment. The method for producing a DDR zeolite has a short hydrothermal synthesis time and does not require continuous agitation of the raw material solution. Specifically disclosed is a method for producing a DDR zeolite, which comprises: a raw material solution preparation step in which a raw material solution that contains 1-adamantaneamine, silica (SiO2) and water at a molar ratio 1-adamantaneamine/SiO2 of 0.002-0.5 and a molar ratio water/SiO2 of 10-500 but does not contain ethylenediamine is prepared; and a crystal growth step in which hydrothermal synthesis is carried out while having the raw material solution and a DDR zeolite powder in contact with each other, so that crystals of DDR zeolite are grown using the DDR zeolite powder as a seed crystal.
摘要翻译：公开了可以使用对环境有害的材料进行的DDR沸石的制造方法。 DDR沸石的制造方法具有短的水热合成时间，不需要连续搅拌原料溶液。具体公开的是一种DDR型沸石的制造方法，其特征在于，包括：原料溶液制备工序，其中含有1-金刚烷胺，二氧化硅（SiO 2）和摩尔比1-金刚烷胺/ SiO 2的水的原料溶液为0.002- 0.5，水/ SiO2的摩尔比为10-500，但不含乙二胺; 以及在使原料溶液和DDR沸石粉末彼此接触的同时进行水热合成的晶体生长步骤，使用DDR沸石粉末作为晶种生长DDR沸石的晶体。

4. 发明授权

US07819944B2 Method of dehydration, dehydrating apparatus, and membrane reactor 有权
标题翻译：脱水方法，脱水装置和膜反应器
公开(公告)号：US07819944B2
公开(公告)日：2010-10-26
申请号：US12204994
申请日：2008-09-05
申请人： Kenji Yajima , Kunio Nakayama , Makiko Niino , Toshihiro Tomita
发明人： Kenji Yajima , Kunio Nakayama , Makiko Niino , Toshihiro Tomita
IPC分类号： B01D53/22 , B01D71/02
CPC分类号： B01D71/028 , B01D61/02 , B01D2325/30
摘要： A dehydration method by which water is selectively separated from a water-containing mixture 31 with a separation membrane. The separation membrane is a DDR type zeolite membrane 2. The dehydration method includes bringing the mixture 31 into contact with one side of the DDR type zeolite membrane 2 and causing a pressure difference between that side of the DDR type zeolite membrane 2 which is in contact with the mixture and the other side of the DDR type zeolite membrane 2 to thereby cause the water to selectively permeate and separate out. By the dehydration method, water can be selectively separated from a water-containing mixture without the need of a high energy cost. The separation membrane has excellent acid resistance.
摘要翻译：使用分离膜从含水混合物31选择性分离水的脱水方法。分离膜是DDR型沸石膜2.脱水方法包括使混合物31与DDR型沸石膜2的一侧接触，并且在接触的DDR型沸石膜2的那一侧产生压力差与DDR型沸石膜2的混合物和另一侧，从而使水选择性渗透并分离出来。通过脱水方法，水可以从含水混合物中选择性分离，而不需要高能量成本。分离膜具有优异的耐酸性。

5. 发明申请

US20080156721A1 LIQUID SEPARATION MEMBRANE INSTALLATION BODY 有权
标题翻译：液体分离膜安装体
公开(公告)号：US20080156721A1
公开(公告)日：2008-07-03
申请号：US12043278
申请日：2008-03-06
申请人： Kenichi Noda , Makiko Niino , Miyuki Yabuki
发明人： Kenichi Noda , Makiko Niino , Miyuki Yabuki
IPC分类号： B01D29/00 , B01D39/00
CPC分类号： B01D69/14 , B01D61/02 , B01D61/362 , B01D67/0041 , B01D67/0046 , B01D69/04 , B01D71/028 , B01D2325/04
摘要： A liquid separation membrane installation body includes a porous base material, and a liquid separation membrane provided on the porous base material, the liquid separation membrane is a porous membrane formed of a dispersant layered inorganic compound, and a membrane thickness of the liquid separation membrane is 0.1 to 1.5 μm. The liquid separation membrane is preferably formed of a sheet-like dispersant layered inorganic compound which has a thickness of 0.1 to 100 nm, a major diameter of 0.01 to 5 μm and an aspect ratio (the major diameter/the thickness) of 3 or more and which is formed into the membrane on the porous base material. There is disclosed the liquid separation membrane installation body capable of increasing a permeation flow rate of a liquid.
摘要翻译：液体分离膜安装体包括多孔基材和设置在多孔基材上的液体分离膜，分离膜是由分散剂层状无机化合物形成的多孔膜，液体分离膜的膜厚为 0.1〜1.5mg。液分离膜优选由厚度为0.1〜100nm，长径为0.01〜5μm，长径比（长径/厚度）为3以上的片状分散剂层状无机化合物形成。并且其形成在多孔基材上的膜中。公开了能够提高液体的渗透流量的液体分离膜安装体。

6. 发明授权

US08778056B2 Zeolite membrane and process for producing zeolite membrane 有权
标题翻译：沸石膜及其制备方法
公开(公告)号：US08778056B2
公开(公告)日：2014-07-15
申请号：US13543977
申请日：2012-07-09
申请人： Tetsuya Uchikawa , Kenji Yajima , Makiko Niino
发明人： Tetsuya Uchikawa , Kenji Yajima , Makiko Niino
IPC分类号： B01D53/22 , B01D71/02 , B01D69/10 , B01D67/00 , B05D5/00
CPC分类号： B01D71/028 , B01D53/228 , B01D61/362 , B01D63/066 , B01D67/0051 , B01D69/02 , B01D2325/02 , C01B39/48
摘要： There are provided a process for producing a zeolite membrane which, even when large, has few defects and which has higher separation performance than conventional zeolite membranes, and a zeolite membrane obtained by the process. In the process, the structure-directing agent is removed in the atmosphere having an O2 concentration of 22.0 vol % or more. Specifically, the process includes: a particle adhesion step of allowing zeolite particles functioning as seeds to flow down the surface of the substrate by means of the weight of the slurry itself, thereby adhering to the substrate and a membrane-forming step of forming a zeolite membrane on the substrate by immersing the substrate having the zeolite particles adhering thereto in sol containing the structure-directing agent for hydrothermal synthesis, thereby forming a zeolite membrane on the substrate.
摘要翻译：提供了一种生产沸石膜的方法，即使大的缺陷也具有比常规沸石膜更高的分离性能，并且通过该方法获得的沸石膜。在该方法中，在O2浓度为22.0体积％以上的气氛中除去结构导向剂。具体而言，该方法包括：粒子粘附工序，其使作为种子的沸石粒子通过浆料本身的重量向下流到基材的表面，从而粘附到基材上，并且形成形成沸石的成膜步骤通过将具有附着在其上的沸石粒子的基材浸渍在含有水热合成用结构导向剂的溶胶中，从而在基材上形成沸石膜，

7. 发明申请

US20120272826A1 ZEOLITE MEMBRANE AND PROCESS FOR PRODUCING ZEOLITE MEMBRANE 有权
标题翻译：沸石膜和生产沸石膜的方法
公开(公告)号：US20120272826A1
公开(公告)日：2012-11-01
申请号：US13543977
申请日：2012-07-09
申请人： Tetsuya UCHIKAWA , Kenji Yajima , Makiko Niino
发明人： Tetsuya UCHIKAWA , Kenji Yajima , Makiko Niino
IPC分类号： B01D71/02 , B01D69/04 , B05D5/00 , B01D69/10
CPC分类号： B01D71/028 , B01D53/228 , B01D61/362 , B01D63/066 , B01D67/0051 , B01D69/02 , B01D2325/02 , C01B39/48
摘要： There are provided a process for producing a zeolite membrane which, even when large, has few defects and which has higher separation performance than conventional zeolite membranes, and a zeolite membrane obtained by the process. In the process, the structure-directing agent is removed in the atmosphere having an O2 concentration of 22.0 vol % or more. Specifically, the process includes: a particle adhesion step of allowing zeolite particles functioning as seeds to flow down the surface of the substrate by means of the weight of the slurry itself, thereby adhering to the substrate and a membrane-forming step of forming a zeolite membrane on the substrate by immersing the substrate having the zeolite particles adhering thereto in sol containing the structure-directing agent for hydrothermal synthesis, thereby forming a zeolite membrane on the substrate.
摘要翻译：提供了一种生产沸石膜的方法，即使大的缺陷也具有比常规沸石膜更高的分离性能，并且通过该方法获得的沸石膜。在该方法中，在O2浓度为22.0体积％以上的气氛中除去结构导向剂。具体而言，该方法包括：粒子粘附工序，其使作为种子的沸石粒子通过浆料本身的重量向下流到基材的表面，从而粘附到基材上，并且形成形成沸石的成膜步骤通过将具有附着在其上的沸石粒子的基材浸渍在含有水热合成用结构导向剂的溶胶中，从而在基材上形成沸石膜，

8. 发明授权

US08497223B2 Process for the production of DDR-type zeolite membranes 有权
标题翻译：生产DDR型沸石膜的方法
公开(公告)号：US08497223B2
公开(公告)日：2013-07-30
申请号：US13214590
申请日：2011-08-22
申请人： Makiko Niino , Kenji Yajima
发明人： Makiko Niino , Kenji Yajima
IPC分类号： B01J20/28 , B01J35/00 , B01J29/06
CPC分类号： C01B37/02 , B01D63/061 , B01D63/066 , B01D67/0051 , B01D71/028 , B01D2323/08 , C01B39/48
摘要： A process for production of a DDR-type zeolite membrane, which comprises: both a seed crystal-forming step of immersing a porous substrate in a seed crystal-forming raw material solution which contains a DDR-type zeolite powder dispersed therein and performing hydrothermal synthesis to form plural DDR-type zeolite crystal particles on surface of the porous substrate, and a membrane-forming step of immersing the resulting porous substrate with DDR-type zeolite crystal particles on the surface in a membrane-forming raw material solution which is free from DDR-type zeolite powder and performing hydrothermal synthesis to form a DDR-type zeolite membrane on the surface of the porous substrate. According to the process, a dense DDR-type zeolite membrane can be formed, and the vessel used in the synthesis can be prevented from being damaged.
摘要翻译：一种DDR型沸石膜的制造方法，其特征在于，包括：将多孔质基材浸渍在分散在其中并进行水热合成的DDR型沸石粉末的晶种形成原料溶液中的晶种形成工序在多孔基材的表面上形成多个DDR型沸石结晶粒子，以及成膜工序，将得到的多孔基材与DDR型沸石结晶粒子浸渍在成膜原料溶液中， DDR型沸石粉末，进行水热合成，在多孔质基材的表面形成DDR型沸石膜。根据该方法，可以形成致密的DDR型沸石膜，并且可以防止在合成中使用的容器被损坏。

9. 发明授权

US08307992B2 Liquid separation membrane installation body 有权
标题翻译：液体分离膜安装体
公开(公告)号：US08307992B2
公开(公告)日：2012-11-13
申请号：US12043278
申请日：2008-03-06
申请人： Kenichi Noda , Makiko Niino , Miyuki Yabuki
发明人： Kenichi Noda , Makiko Niino , Miyuki Yabuki
IPC分类号： B01D29/05 , B01D29/00 , B01D29/46
CPC分类号： B01D69/14 , B01D61/02 , B01D61/362 , B01D67/0041 , B01D67/0046 , B01D69/04 , B01D71/028 , B01D2325/04
摘要： A liquid separation membrane installation body includes a porous base material, and a liquid separation membrane provided on the porous base material, the liquid separation membrane is a porous membrane formed of a dispersant layered inorganic compound, and a membrane thickness of the liquid separation membrane is 0.1 to 1.5 μm. The liquid separation membrane is preferably formed of a sheet-like dispersant layered inorganic compound which has a thickness of 0.1 to 100 nm, a major diameter of 0.01 to 5 μm and an aspect ratio (the major diameter/the thickness) of 3 or more and which is formed into the membrane on the porous base material. There is disclosed the liquid separation membrane installation body capable of increasing a permeation flow rate of a liquid.
摘要翻译：液体分离膜安装体包括多孔基材和设置在多孔基材上的液体分离膜，分离膜是由分散剂层状无机化合物形成的多孔膜，液体分离膜的膜厚为 0.1〜1.5μm。液体分离膜优选由厚度为0.1〜100nm，长径为0.01〜5μm，长径比（长径/厚度）为3以上的片状分散剂层状无机化合物形成。并且其形成在多孔基材上的膜中。公开了能够提高液体的渗透流量的液体分离膜安装体。

10. 发明申请

US20090007780A1 METHOD OF DEHYDRATION, DEHYDRATING APPARATUS, AND MEMBRANE REACTOR 有权
标题翻译：脱水方法，脱水装置和膜反应器
公开(公告)号：US20090007780A1
公开(公告)日：2009-01-08
申请号：US12204994
申请日：2008-09-05
申请人： Kenji Yajima , Kunio Nakayama , Makiko Niino , Toshihiro Tomita
发明人： Kenji Yajima , Kunio Nakayama , Makiko Niino , Toshihiro Tomita
IPC分类号： B01D53/22 , B01D71/02 , B01J15/00
CPC分类号： B01D71/028 , B01D61/02 , B01D2325/30
摘要： A dehydration method by which water is selectively separated from a water-containing mixture 31 with a separation membrane. The separation membrane is a DDR type zeolite membrane 2. The dehydration method includes bringing the mixture 31 into contact with one side of the DDR type zeolite membrane 2 and causing a pressure difference between that side of the DDR type zeolite membrane 2 which is in contact with the mixture and the other side of the DDR type zeolite membrane 2 to thereby cause the water to selectively permeate and separate out. By the dehydration method, water can be selectively separated from a water-containing mixture without the need of a high energy cost. The separation membrane has excellent acid resistance.
摘要翻译：使用分离膜从含水混合物31选择性分离水的脱水方法。分离膜是DDR型沸石膜2.脱水方法包括使混合物31与DDR型沸石膜2的一侧接触，并且在接触的DDR型沸石膜2的那一侧产生压力差与DDR型沸石膜2的混合物和另一侧，从而使水选择性渗透并分离出来。通过脱水方法，水可以从含水混合物中选择性分离，而不需要高能量成本。分离膜具有优异的耐酸性。

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