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1. 发明授权

US5270436A Polyester for electrophotography 失效
标题翻译：聚酯电子照相
公开(公告)号：US5270436A
公开(公告)日：1993-12-14
申请号：US711033
申请日：1991-06-06
申请人： Shinji Kubo , Noriyuki Tajiri , Hitoshi Iwasaki , Masayuki Takyu , Masahiro Itoh , Hirokazu Ito
发明人： Shinji Kubo , Noriyuki Tajiri , Hitoshi Iwasaki , Masayuki Takyu , Masahiro Itoh , Hirokazu Ito
IPC分类号： C08G63/20 , G03G9/087 , C08G63/00
CPC分类号： C08G63/20 , G03G9/08755
摘要： A polyester for electrophotography derived from(a) at least one component selected from tri- or tetra-basic acid components and tri- or tetra-hydric alcohols;(b) at least one component selected from dibasic carboxylic acids and lower alkyl esters thereof; and(c) at least one component selected from aromatic diols and alicyclic diolswherein the proportion of x (mole %) of component (a) to the whole acid components and the proportion y (mole %) of component (c) to the whole acid components satisfies the following formulae (1) and (2):y (253m+170n) log x-(176m+162n) (2)wherein 0

2. 发明授权

US5276127A Polyester resin for toner 失效
标题翻译：聚碳酸酯树脂
公开(公告)号：US5276127A
公开(公告)日：1994-01-04
申请号：US744333
申请日：1991-08-13
申请人： Masayuki Takyu , Noriyuki Tajiri , Hitoshi Iwasaki , Shinji Kubo , Masahiro Itoh , Hirokazu Ito
发明人： Masayuki Takyu , Noriyuki Tajiri , Hitoshi Iwasaki , Shinji Kubo , Masahiro Itoh , Hirokazu Ito
IPC分类号： C08G63/20 , G03G9/087 , C08G63/02
CPC分类号： C08G63/20 , G03G9/08755
摘要： A polyester resin for a toner capable of being stably prepared without an occurrence of an abrupt crosslinking reaction is provided. This polyester resin has a crosslinked structure and is derived from (a) at least one member selected from the group consisting of tribasic and tetrabasic carboxylic acid components and trihydric and tetrahydric alcohol components, (b) an aromatic or alicyclic diol component, at least one of the hydroxyl groups of which is a secondary hydroxyl group, (c) optionally other diol component, and (d) a dicarboxylic acid component, wherein the contents of the units of the component (a) and the units of the component (b) satisfy the requirement represented by the following formula (1):(8m+20n)a-(80m+80n).ltoreq.b.ltoreq.(8m+20n)a-(12m+30n) (1)wherein m represents the molar fraction of the tribasic carboxylic acid component and trihydric alcohol component units in the units derived from the component (a), n represent the molar fraction of the tetrabasic carboxylic acid component units and tetrahydric alcohol component units in the units derived from the component (a), the sum of m and n is equal to 1, and a and b represent the molar ratios (mole %) of the units of the component (a) and the units of the component (b) based on the total of the carboxylic acid components, respectively.
摘要翻译：提供了一种能够稳定地制备而不发生突然交联反应的调色剂用聚酯树脂。该聚酯树脂具有交联结构，并且衍生自（a）选自三元和四元羧酸组分和三元和四元醇组分中的至少一种，（b）芳族或脂环族二醇组分，至少一种其中羟基为仲羟基，（c）任选其它二醇组分，和（d）二羧酸组分，其中组分（a）的单元含量和组分（b）的单元含量，满足由下式（1）表示的要求：（8m + 20n）a-（80m + 80n）<= b <=（8m + 20n）a-（12m + 30n）（1）其中m表示摩尔分数的三元羧酸组分和三元醇组分单元的衍生自组分（a）的单元，n表示衍生自组分（a）的单元中的四元羧酸组分单元和四元醇组分单元的摩尔分数， m和n的和等于1，而 a和b分别表示组分（a）的单元和组分（b）的单元的摩尔比（摩尔％），基于羧酸组分的总量。

3. 发明授权

US4849495A Polyester resin from tri- or higher polycarboxylic acid for toner and process for its production 失效
标题翻译：用于调色剂的三元或更多的多元羧酸的聚酯树脂及其制备方法
公开(公告)号：US4849495A
公开(公告)日：1989-07-18
申请号：US200416
申请日：1988-05-31
申请人： Ryo Funato , Shinji Kubo , Noriyuki Tajiri , Hirokazu Ito , Hitoshi Iwasaki
发明人： Ryo Funato , Shinji Kubo , Noriyuki Tajiri , Hirokazu Ito , Hitoshi Iwasaki
IPC分类号： C08G63/12 , C08G63/20 , C08G63/78 , G03G9/087
CPC分类号： C08G63/20 , G03G9/08755
摘要： A polyester resin for toner, which consists essentially of (a) from 5 to 60 equivalent %, based on the entire carboxylic acid components, of at least one member selected from the group consisting of tribasic and higher polybasic carboxylic acids, anhydrides thereof and lower alkyl esters thereof, (b) at least one member selected from the group consisting of dicarboxylic acids and lower alkyl esters thereof, (c) at least one aromatic diol and (d) at least one aliphatic diol, and which has a softening temeprature of from 100.degree. to 170.degree. C., a glass transition temperature (Tg) of from 50.degree. to 70.degree. C., an acid value of from 0.5 to 10 mgKOH/g and a gel content of from 3 to 40%.

4. 发明授权

US4866158A Polyester resin for toner and process for its production 失效
标题翻译：用于调色剂的聚酯树脂及其生产工艺
公开(公告)号：US4866158A
公开(公告)日：1989-09-12
申请号：US190099
申请日：1988-05-04
申请人： Shinji Kubo , Ryo Funato , Noriyuki Tajiri , Hirokazu Ito , Hitoshi Iwasaki
发明人： Shinji Kubo , Ryo Funato , Noriyuki Tajiri , Hirokazu Ito , Hitoshi Iwasaki
IPC分类号： C08G63/123 , C08G63/20 , C08G63/78 , G03G9/087
CPC分类号： C08G63/20 , G03G9/08755
摘要： A polyester resin for toner, which consists essentially of (a) from 0.5 to 50 mol %, based on the entire alcohol components, of at least one trihydric or higher polyhydric alcohol, (b) from 50 to 99.5 mol %, based on the entire alcohol components, of at least one diol and (c) at least one member selected from the group consisting of dicarboxylic acids and lower alkyl esters thereof, and which has a softening temperature of from 90.degree. to 170.degree. C., a glass transition temperature (Tg) of from 30.degree. to 70.degree. C., an acid value of from 0.5 to 15 mgKOH/g and a gel content of from 1.5 to 40%.

5. 发明授权

US4988794A Polyester resin for toner and process for its production 失效
标题翻译：用于调色剂的聚酯树脂及其生产工艺
公开(公告)号：US4988794A
公开(公告)日：1991-01-29
申请号：US485762
申请日：1990-02-26
申请人： Shinji Kubo , Ryo Funato , Noriyuki Tajiri , Hirokazu Ito , Hitoshi Iwasaki
发明人： Shinji Kubo , Ryo Funato , Noriyuki Tajiri , Hirokazu Ito , Hitoshi Iwasaki
IPC分类号： C08G63/123 , C08G63/20 , C08G63/78 , G03G9/087
CPC分类号： C08G63/20 , G03G9/08755
摘要： A polyester resin for toner, which consists essentially of (a) from 0.5 to 50 mol %, based on the entire alcohol components, of at least one trihydric or higher polyhydric alcohol, (b) from 50 to 99.5 mol %, based on the entire alcohol components, of at least one diol and (c) at least one member selected from the group consisting of dicarboxylic acids and lower alkyl esters thereof, and which has a softening temperature of from 90.degree. to 170.degree. C., a glass transition temperature (Tg) of from 30.degree. to 70.degree. C., an acid value of from 0.5 to 15 mgKOH/g and a gel content of from 1.5 to 40%.

6. 发明授权

US06103438A Polyester resin for toner, process for its production and toner 失效
标题翻译：用于调色剂的聚酯树脂，其生产工艺和调色剂
公开(公告)号：US06103438A
公开(公告)日：2000-08-15
申请号：US19147
申请日：1998-02-06
申请人： Shinji Kubo , Noriyuki Tajiri , Hitoshi Iwasaki , Yoichi Nagai
发明人： Shinji Kubo , Noriyuki Tajiri , Hitoshi Iwasaki , Yoichi Nagai
IPC分类号： C08G63/195 , C08G63/20 , C08G63/672 , G03G9/087 , G03G9/097
CPC分类号： G03G9/08755 , C08G63/195 , C08G63/672 , G03G9/09733 , C08G63/20
摘要： A polyester resin for toner comprising an acid component containing at least one selected from the group consisting of aromatic dicarboxylic acids and their lower alkyl esters, and an alcohol component containing at least one selected from the group consisting of bisphenol A derivative diols, wherein the content of aldehyde compounds, their decomposition products and by-products in the polyester resin is no more than 200 ppm. Toner polyester resins and toners are obtained which do not generate irritating odors even upon melting and kneading during the toner production or upon heating during the copying process, which provide clear images with no haziness due to reduced light permeability of the copy material, which have a wide range of color tone reproduction, and which provide excellent image precision on copied print.
摘要翻译：一种用于调色剂的聚酯树脂，其包含含有选自芳族二羧酸及其低级烷基酯中的至少一种的酸组分和包含选自双酚A衍生物二醇中的至少一种的醇组分，其中所述含量的醛化合物，它们在聚酯树脂中的分解产物和副产物不超过200ppm。得到调色剂聚酯树脂和调色剂，其即使在调色剂生产期间的熔融和捏合或复印过程中加热时也不会产生刺激性气味，这提供了由于复印材料的透光性降低而提供清晰的图像而不发生混浊，宽范围的色调再现，并且在复印上提供出色的图像精度。

7. 发明授权

US5807654A Polyester resin for toner, process for its production and toner 失效
标题翻译：用于调色剂的聚酯树脂，其生产工艺和调色剂
公开(公告)号：US5807654A
公开(公告)日：1998-09-15
申请号：US605074
申请日：1996-03-12
申请人： Shinji Kubo , Noriyuki Tajiri , Hitoshi Iwasaki , Yoichi Nagai
发明人： Shinji Kubo , Noriyuki Tajiri , Hitoshi Iwasaki , Yoichi Nagai
IPC分类号： C08G63/195 , C08G63/20 , C08G63/672 , G03G9/087 , G03G9/097
CPC分类号： G03G9/08755 , C08G63/195 , C08G63/672 , G03G9/09733 , C08G63/20
摘要： A polyester resin for toner comprising an acid component containing at least one selected from the group consisting of aromatic dicarboxylic acids and their lower alkyl esters, and an alcohol component containing at least one selected from the group consisting of bisphenol A derivative diols, wherein the content of aldehyde compounds, their decomposition products and by-products in the polyester resin is no more than 200 ppm. Toner polyester resins and toners are obtained which do not generate irritating odors even upon melting and kneading during the toner production or upon heating during the copying process, which provide clear images with no haziness due to reduced light permeability of the copy material, which have a wide range of color tone reproduction, and which provide excellent image precision on copied print.
摘要翻译： PCT No.PCT / JP95 / 01395 Sec。 371日期：1996年3月12日 102（e）1996年3月12日PCT PCT 1995年7月12日PCT公布。出版物WO96 / 02870 日期1996年2月1日一种用于调色剂的聚酯树脂，其包含含有选自芳族二羧酸及其低级烷基酯中的至少一种的酸成分，以及含有选自双酚A衍生物二醇，其中在聚酯树脂中醛化合物，其分解产物和副产物的含量不超过200ppm。得到调色剂聚酯树脂和调色剂，其即使在调色剂生产期间的熔融和捏合或复印过程中加热时也不会产生刺激性气味，这提供了由于复印材料的透光性降低而提供清晰的图像而不发生混浊，宽范围的色调再现，并且在复印上提供出色的图像精度。

8. 发明授权

US6007958A Polyester resin for full color toner 失效
标题翻译：全彩色聚碳酸酯树脂
公开(公告)号：US6007958A
公开(公告)日：1999-12-28
申请号：US973746
申请日：1997-12-22
申请人： Hirokazu Ito , Hitoshi Iwasaki , Noriyuki Tajiri
发明人： Hirokazu Ito , Hitoshi Iwasaki , Noriyuki Tajiri
IPC分类号： C08G63/20 , C08G63/668 , G03G9/087
CPC分类号： C08G63/668 , C08G63/20 , G03G9/08755
摘要： A polyester resin for a full color toner which comprises a) from 0.5 to 5% by mole, based on all the acid components, of a tribasic or higher carboxylic acid component and/or a trihydric or higher alcohol component, b) at least 95% by mole, based on all the acid components, of a dibasic carboxylic acid component, c) from 10 to 80% by mole, based on all the acid components, of an aromatic diol component consisting of or containing a bisphenol A derivative having ethylene oxide added thereto, and d) from 20 to 110% by mole, based on all the acid components, of an aliphatic diol component; and has a softening temperature of 95 to 115.degree. C., a glass transition temperature of 50 to 70.degree. C., an acid value of 6 to 20 mgKOH/g, a melt viscosity at 118.degree. C. of 1000 to 52,000 poises, a ratio of weight average molecular weight (Mw) to number average molecular weight (Mn) of 1.5 to 5 in the molecular weight distribution determined by gel permeation chromatography, a peak TOP molecular weight of 20,000 or less and a gel fraction of 0.5% by weight or less.
摘要翻译： PCT No.PCT / JP96 / 01754 Sec。 371 1997年12月22日第 102（e）日期1997年12月22日PCT提交1996年6月25日PCT公布。出版物WO97 / 01797 日本1997年1月16日一种全彩色调色剂用聚酯树脂，其包含a）基于所有酸组分的0.5至5摩尔％的三元或更高级羧酸组分和/或三元或更高级的醇组分， b）基于所有酸组分的至少95摩尔％的二元羧酸组分，c）基于所有酸组分的10至80摩尔％的由或含有具有环氧乙烷的双酚A衍生物，d）脂肪族二醇成分的全部酸成分为20〜110摩尔％。软化温度为95〜115℃，玻璃化转变温度为50〜70℃，酸值为6〜20mgKOH / g，118℃下的熔融粘度为1000〜52000泊，通过凝胶渗透色谱法测定的分子量分布中的重均分子量（Mw）与数均分子量（Mn）的比为1.5〜5，峰值TOP分子量为20,000以下，凝胶分数为0.5％，通过重量以下。

9. 发明授权

US5914380A Toner resin and process for its production 失效
标题翻译：调色剂树脂及其生产工艺
公开(公告)号：US5914380A
公开(公告)日：1999-06-22
申请号：US887273
申请日：1997-07-02
申请人： Hirokazu Ito , Hitoshi Iwasaki , Noriyuki Tajiri
发明人： Hirokazu Ito , Hitoshi Iwasaki , Noriyuki Tajiri
IPC分类号： C08F2/18 , C08F212/04 , G03G9/087 , C08F20/06
CPC分类号： C08F212/04 , G03G9/08711 , G03G9/08791 , G03G9/08795 , G03G9/08797
摘要： Toner resin consisting of a polymer which comprises (a) an aromatic vinyl unit, (b) an acrylic or methacrylic compound unit and (c) a polyfunctional compound unit, and which has a tetrahydrofuran insoluble content of 5-60%, a maximum peak molecular weight of no more than 20,000 in the molecular weight distribution of the tetrahydrofuran soluble portion as measured by gel permeation chromatography, and a weight average polymerization degree of no more than 180, as well as a process for its production. The resulting toner resin has an excellent fixing property, non-offsetting property, blocking resistance and image stability.
摘要翻译：由聚合物组成的调色剂树脂，其包含（a）芳族乙烯基单元，（b）丙烯酸或甲基丙烯酸酯化合物单元和（c）多官能化合物单元，其四氢呋喃不溶物含量为5-60％，最大峰通过凝胶渗透色谱法测定的四氢呋喃可溶部分的分子量分布中的分子量不大于20,000，重均聚合度不大于180，以及其制备方法。所得到的调色剂树脂具有优异的定影性，不偏移性，抗粘连性和图像稳定性。

10. 发明授权

US07365150B2 Process for producing polyester resin for toner 有权
标题翻译：生产调色剂用聚酯树脂的方法
公开(公告)号：US07365150B2
公开(公告)日：2008-04-29
申请号：US10481447
申请日：2002-06-19
申请人： Hirokazu Ito , Masaru Sugiura , Kouji Shimizu , Hitoshi Iwasaki
发明人： Hirokazu Ito , Masaru Sugiura , Kouji Shimizu , Hitoshi Iwasaki
IPC分类号： C08K5/00
CPC分类号： G03G9/08755 , C08G63/20 , C08G63/78 , C08L67/00 , C08L91/06
摘要： A polyester resin for toner which is obtained through polymerization in the presence of a release agent ingredient with a melting point of 60–100° C. or a release agent ingredient comprising an alcohol component, and which has a softening temperature of 100–160° C., an acid value of 0.1–30 mgKOH/g and a glass transition temperature of 40–70° C.; a process for producing a polyester resin for toner which comprises conducting polymerization in the presence of a release agent ingredient with a melting point of 60–100° C. or a release agent ingredient comprising an alcohol component; and toner comprising the polyester resin. Toners with excellent non-offset properties and glosses are obtained.
摘要翻译：一种调色剂用聚酯树脂，其通过在熔点为60-100℃的脱模剂成分存在下聚合而获得，或者含有醇成分的脱模剂成分，其软化温度为100-160° C.酸值为0.1-30mgKOH / g，玻璃化转变温度为40-70℃。一种用于生产调色剂用聚酯树脂的方法，其包括在熔点为60-100℃的脱模剂成分存在下进行聚合或包含醇组分的脱模剂成分; 和包含聚酯树脂的调色剂。获得具有优异的非胶印性能和光泽度的调色剂。

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