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1. 发明申请

US20100261051A1 SODIUM ION SECONDARY BATTERY AND NEGATIVE ELECTRODE ACTIVE MATERIAL USED THEREIN 审中-公开
标题翻译：钠离子二次电池和负极电极活性材料
公开(公告)号：US20100261051A1
公开(公告)日：2010-10-14
申请号：US12744643
申请日：2008-11-21
申请人： Shigeto Okada , Manabu Nishijima , Takayuki Doi , Jun-ichi Yamaki , Masami Makidera , Taketsugu Yamamoto
发明人： Shigeto Okada , Manabu Nishijima , Takayuki Doi , Jun-ichi Yamaki , Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M6/04 , H01M4/58
CPC分类号： H01M10/054 , H01M4/02 , H01M4/587 , H01M2004/021
摘要： A sodium ion secondary battery having far superior potential stability during discharge when repeatedly charging and discharging, and a negative electrode active material capable of being efficiently doped and dedoped with sodium ions used therefor are provided. The sodium ion secondary battery according to the present invention includes a positive electrode containing a positive electrode active material capable of being doped and dedoped with sodium ions, a negative electrode containing a negative electrode active material containing, as a sole component or as a main component, a glassy carbonaceous material capable of being doped and dedoped with sodium ions, and an electrolyte containing sodium ions. Further, the negative electrode active material for a non-aqueous electrolyte sodium ion secondary battery according to the present invention includes a glassy carbonaceous material as a sole component or as a main component.
摘要翻译：提供了在重复充放电时在放电期间具有非常优异的电位稳定性的钠离子二次电池以及能够有效地掺杂并去除其中使用的钠离子的负极活性物质。根据本发明的钠离子二次电池包括含有能够掺杂和脱掺杂钠离子的正极活性物质的正极，含有负极活性物质的负极作为唯一成分或作为主要成分能够掺杂和脱掺杂钠离子的玻璃质碳质材料和含有钠离子的电解质。此外，本发明的非水电解质钠离子二次电池用负极活性物质，作为单一成分或主要成分，含有玻璃质碳质材料。

2. 发明授权

US10122014B2 Mixed metal oxide and sodium secondary battery 有权
公开(公告)号：US10122014B2
公开(公告)日：2018-11-06
申请号：US12865976
申请日：2009-02-03
申请人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
发明人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M4/00 , H01M4/525 , H01M10/054 , H01M2/16 , H01M4/505 , H01M10/54
摘要： The present invention provides a sodium secondary battery capable of reducing the amount of lithium used, and ensuring a larger discharge capacity maintenance rate when having repeated a charge and discharge, as compared with conventional techniques; and a mixed metal oxide usable as the positive electrode active material therefor. A mixed metal oxide of the present invention comprises Na and M1 wherein M1 represents three or more elements selected from the group consisting of Mn, Fe, Co and Ni with an Na:M1 molar ratio being a:1 wherein a is a value falling within the range of more than 0.5 and less than 1. Also, a mixed metal oxide of the present invention is represented by the following formula (1): NaaM1O2 (1) wherein M1 and a each have the same meaning as above. The positive electrode active material for secondary batteries of the present invention comprises the mixed metal oxide above.

3. 发明授权

US09142860B2 Mixed metal oxide and sodium secondary battery 有权
标题翻译：混合金属氧化物和钠二次电池
公开(公告)号：US09142860B2
公开(公告)日：2015-09-22
申请号：US12865993
申请日：2009-02-03
申请人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
发明人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M2/16 , H01M4/88 , H01M10/054 , H01M4/58 , H01M4/505 , H01M4/525 , H01M10/42 , C01G49/00 , C01G53/00
CPC分类号： H01M10/054 , C01G49/0072 , C01G53/50 , C01P2002/72 , H01M2/1653 , H01M2/1686 , H01M4/505 , H01M4/525 , H01M4/5825 , H01M10/4235 , Y02E60/122
摘要： A sodium secondary battery capable of reducing the amount used of a scarce metal element such as lithium and cobalt and moreover, ensuring a larger discharge capacity after repeating charge/discharge as compared with conventional techniques, and a mixed metal oxide usable as the positive electrode active material therefor. The mixed metal oxide comprises Na, Mn and M1 wherein M1 is Fe or Ni, with a Na:Mn:M1 molar ratio being a:(1−b):b wherein a is a value falling within the range of more than 0.5 and less than 1, and b is a value falling within the range of from 0.001 to 0.5. Another mixed metal oxide is a mixed metal oxide represented by the following formula (1): NaaMn1−bM1bO2 (1) wherein M1, a and b each have the same meaning as above. The positive electrode active material for sodium secondary batteries comprises the mixed metal oxide above.
摘要翻译：能够减少稀有金属元素如锂和钴的量的钠二次电池，并且与常规技术相比，确保重复充电/放电之后的放电容量更大，并且可用作正极活性物质的混合金属氧化物材料。混合金属氧化物包括Na，Mn和M1，其中M1是Fe或Ni，Na：Mn：M1的摩尔比为a：（1-b）：b其中a是大于0.5的范围内的值，小于1，b为0.001〜0.5的范围。另一种混合金属氧化物是由下式（1）表示的混合金属氧化物：NaaMn1-bM1bO2（1）其中M1，a和b各自具有与上述相同的含义。钠二次电池用正极活性物质为上述复合金属氧化物。

4. 发明申请

US20100323232A1 MIXED METAL OXIDE AND SODIUM SECONDARY BATTERY 审中-公开
标题翻译：混合金属氧化物和钠二次电池
公开(公告)号：US20100323232A1
公开(公告)日：2010-12-23
申请号：US12865976
申请日：2009-02-03
申请人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
发明人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M2/14 , H01M4/40 , H01M4/505 , H01M4/485 , H01M10/054
CPC分类号： H01M4/525 , H01M2/1653 , H01M2/1686 , H01M4/505 , H01M10/054 , H01M10/54 , Y02W30/84
摘要： The present invention provides a sodium secondary battery capable of reducing the amount of lithium used, and ensuring a larger discharge capacity maintenance rate when having repeated a charge and discharge, as compared with conventional techniques; and a mixed metal oxide usable as the positive electrode active material therefor. A mixed metal oxide of the present invention comprises Na and M1 wherein M1 represents three or more elements selected from the group consisting of Mn, Fe, Co and Ni with an Na:M1 molar ratio being a:1 wherein a is a value falling within the range of more than 0.5 and less than 1. Also, a mixed metal oxide of the present invention is represented by the following formula (1): NaaM1O2 (1) wherein M1 and a each have the same meaning as above.The positive electrode active material for secondary batteries of the present invention comprises the mixed metal oxide above.
摘要翻译：本发明提供一种能够减少所使用的锂的量的钠二次电池，并且与现有的技术相比，能够在重复进行充放电时确保更大的放电容量维持率。和可用作其的正极活性物质的混合金属氧化物。本发明的混合金属氧化物包含Na和M1，其中M1表示选自Mn，Fe，Co和Ni中的三种或更多种元素，Na：M1摩尔比为a：1，其中a为落入范围大于0.5且小于1.此外，本发明的混合金属氧化物由下式（1）表示：NaaM1O2（1）其中M1和a各自具有与上述相同的含义。本发明的二次电池用正极活性物质包含上述复合金属氧化物。

5. 发明授权

US08790831B2 Powder for positive electrode active material, positive active electrode active material, and sodium secondary battery 有权
标题翻译：正极活性物质粉末，正极活性物质活性物质，钠二次电池
公开(公告)号：US08790831B2
公开(公告)日：2014-07-29
申请号：US12866148
申请日：2009-02-03
申请人： Masami Makidera , Taketsugu Yamamoto
发明人： Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M4/50 , H01B1/02 , H01M4/52
CPC分类号： H01M2/1653 , H01M4/505 , H01M4/525 , H01M10/056 , Y10T428/2982
摘要： The present invention provides a positive electrode active material that can suppress the necessity of performing sieving and is suitable for use in secondary batteries, particularly sodium secondary batteries. Also provided is a powder for a positive electrode active material as a raw material for the positive electrode active material. The powder for a positive electrode active material of the present invention comprises Mn-containing particles. In the cumulative particle size distribution on the volume basis of particles constituting the powder, D50, which is the particle diameter at a 50% cumulation measured from the smallest particle, is in the range of from 0.1 μm to 10 μm, and 90 vol % or more of the particles constituting the powder are in the range of from 0.3 times to 3 times D50. The powder for a positive electrode active material comprises Mn-containing particles, and 90 vol % or more of the particles constituting the powder are in the range of from 0.6 μm to 6 μm. The positive electrode active material is a powdery positive electrode active material obtained by calcining a mixture of the powder for positive electrode active material and a sodium compound. The positive electrode for sodium rechargeable batteries comprises the positive electrode active material.
摘要翻译：本发明提供能够抑制进行筛分的必要性的正极活性物质，适用于二次电池，特别是钠二次电池。还提供了作为正极活性物质的原料的正极活性物质的粉末。本发明的正极活性物质用粉末含有Mn粒子。在构成粉末的粒子的体积基础上的累积粒度分布中，从最小粒子测定的50％累积时的粒径D50为0.1μm〜10μm，90体积％或更多的构成粉末的颗粒在D50的0.3倍至3倍的范围内。用于正极活性物质的粉末包含含Mn颗粒，并且构成粉末的颗粒的90体积％以上在0.6μm至6μm的范围内。正极活性物质是通过煅烧正极活性物质粉末和钠化合物的混合物而获得的粉末状正极活性物质。钠可充电电池用正极包含正极活性物质。

6. 发明申请

US20110003192A1 MIXED METAL OXIDE AND SODIUM SECONDARY BATTERY 有权
标题翻译：混合金属氧化物和钠二次电池
公开(公告)号：US20110003192A1
公开(公告)日：2011-01-06
申请号：US12865993
申请日：2009-02-03
申请人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
发明人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M2/16 , H01M4/88
CPC分类号： H01M10/054 , C01G49/0072 , C01G53/50 , C01P2002/72 , H01M2/1653 , H01M2/1686 , H01M4/505 , H01M4/525 , H01M4/5825 , H01M10/4235 , Y02E60/122
摘要： The present invention provides a sodium secondary battery capable of reducing the amount used of a scarce metal element such as lithium and cobalt and moreover, ensuring a larger discharge capacity after repeating charge/discharge as compared with conventional techniques, and a mixed metal oxide usable as the positive electrode active material therefor. The mixed metal oxide of the present invention comprises Na, Mn and M1 wherein M1 is Fe or Ni, with a Na:Mn:M1 molar ratio being a:(1-b):b wherein a is a value falling within the range of more than 0.5 and less than 1, and b is a value falling within the range of from 0.001 to 0.5. Another mixed metal oxide of the present invention is a mixed metal oxide represented by the following formula (1): NaaMn1-bM1bO2 (1) wherein M1, a and b each have the same meaning as above. The positive electrode active material for sodium secondary batteries of the present invention comprises the mixed metal oxide above.
摘要翻译：本发明提供一种钠二次电池，其能够减少诸如锂和钴之类的稀有金属元素的使用量，此外，与常规技术相比，确保了重复充电/放电后的放电容量更大，并且可用作正极活性物质。本发明的混合金属氧化物包括Na，Mn和M1，其中M1是Fe或Ni，Na：Mn：M1的摩尔比为a：（1-b）：b其中a是落在大于0.5且小于1，b为0.001至0.5的范围内的值。本发明的另一种混合金属氧化物是由下式（1）表示的混合金属氧化物：NaaMn1-bM1bO2（1）其中M1，a和b各自具有与上述相同的含义。本发明的钠二次电池用正极活性物质包含上述混合金属氧化物。

7. 发明申请

US20100248041A1 NONAQUEOUS ELECTROLYTE SECONDARY BATTERY, ELECTRODE AND CARBONACEOUS MATERIAL 审中-公开
标题翻译：非电解电解质二次电池，电极和碳质材料
公开(公告)号：US20100248041A1
公开(公告)日：2010-09-30
申请号：US12739888
申请日：2008-10-24
申请人： Taketoshi Kikuchi , Kosuke Kurakane , Taketsugu Yamamoto , Takeshi Hattori , Masami Makidera
发明人： Taketoshi Kikuchi , Kosuke Kurakane , Taketsugu Yamamoto , Takeshi Hattori , Masami Makidera
IPC分类号： H01M6/16 , C01B31/02 , H01M4/131 , H01M4/52 , H01M4/583 , H01M4/50
CPC分类号： H01M4/587 , C01B32/05 , C01P2006/11 , C01P2006/12 , H01G11/32 , H01G11/42 , H01M2/1653 , H01M2/1686 , H01M4/0471 , H01M4/133 , H01M4/1393 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/625 , H01M10/05 , H01M10/054 , Y02E60/13 , Y02T10/7022
摘要： The present invention provides a nonaqueous electrolyte secondary battery, an electrode and a carbonaceous material. The nonaqueous electrolyte secondary battery has an electrode containing a carbonaceous material obtained by a production method comprising a step of heating a compound of formula (1) or a calcination product of the compound, under an inert gas atmosphere in the range of from 200° C. to 3000° C.: wherein R represents a hydrocarbon group having 1 to 12 carbon atoms, and a hydroxyl group, an alkyl group, an alkoxyl group, an aryl group, an aryloxy group, a sulfonyl group, a halogen atom, a nitro group, a thioalkyl group, a cyano group, a carboxyl group, an amino group or an amide group may be attached to the hydrocarbon group; R′ represents a hydrogen atom or a methyl group; n represents 3, 5 or 7.
摘要翻译：本发明提供一种非水电解质二次电池，电极和碳质材料。非水电解质二次电池具有含有碳质材料的电极，该制造方法包括在惰性气体气氛中在200℃的范围内加热式（1）的化合物或该化合物的煅烧产物的步骤至3000℃：其中R表示碳原子数1〜12的烃基，羟基，烷基，烷氧基，芳基，芳氧基，磺酰基，卤素原子，硝基，硫代烷基，氰基，羧基，氨基或酰胺基可以连接到烃基上; R'表示氢原子或甲基; n表示3,5或7。

8. 发明授权

US09502714B2 Mixed metal oxide, electrode, and sodium secondary battery 有权
标题翻译：混合金属氧化物，电极和钠二次电池
公开(公告)号：US09502714B2
公开(公告)日：2016-11-22
申请号：US13256159
申请日：2010-03-10
申请人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
发明人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M4/131 , H01M4/50 , C01G45/12 , C01G49/00 , C01G51/00 , C01G53/00 , H01M2/16 , H01M4/48 , H01M4/485 , H01M10/054 , H01M10/0565 , H01M10/0568 , H01M10/0569 , H01M10/36 , H01M4/505 , H01M4/525 , H01M4/02
CPC分类号： H01M4/50 , C01G45/1228 , C01G49/0018 , C01G49/0027 , C01G49/0036 , C01G51/006 , C01G51/42 , C01G53/42 , C01G53/50 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2004/32 , C01P2004/54 , C01P2006/16 , C01P2006/40 , C01P2006/80 , H01M2/16 , H01M2/1686 , H01M4/483 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/054 , H01M10/0565 , H01M10/0568 , H01M10/0569 , H01M10/36 , H01M2004/028 , H01M2200/10 , H01M2300/002 , H01M2300/0025 , H01M2300/0088 , Y02E60/122
摘要： Disclosed is a mixed metal oxide comprising Na, M1, and M2, where M1 represents at least one element selected from the group consisting of Mg, Ca, Sr, and Ba; and M2 represents at least one element selected from the group consisting of Mn, Fe, Co, and Ni, wherein the molar ratio of Na:M1:M2 is a:b:1, where a is a value within the range of not less than 0.5 and less than 1; b is a value within the range of more than 0 and not more than 0.5; and “a+b” is a value within the range of more than 0.5 and not more than 1. An electrode having an active material containing the mixed metal oxide is also disclosed. Further disclosed is an electrode containing the electrode active material as well as a sodium secondary battery comprising the electrode as a positive electrode.
摘要翻译：公开了包含Na，M1和M2的混合金属氧化物，其中M1表示选自Mg，Ca，Sr和Ba中的至少一种元素; M2表示选自Mn，Fe，Co和Ni中的至少一种元素，其中Na：M1：M2的摩尔比为a：b：1，其中a为不小于大于0.5且小于1; b是大于0且不大于0.5的范围内的值; 并且“a + b”是大于0.5且不大于1的范围内的值。还公开了具有含有该混合金属氧化物的活性物质的电极。还公开了含有电极活性物质的电极以及包含该电极作为正电极的钠二次电池。

9. 发明申请

US20110008668A1 POWDER FOR POSITIVE ELECTRODE ACTIVE MATERIAL, POSITIVE ACTIVE ELECTRODE ACTIVE MATERIAL, AND SODIUM SECONDARY BATTERY 有权
标题翻译：活性电极活性材料，阳极活性电极活性材料和钠二次电池用粉末
公开(公告)号：US20110008668A1
公开(公告)日：2011-01-13
申请号：US12866148
申请日：2009-02-03
申请人： Masami Makidera , Taketsugu Yamamoto
发明人： Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M4/50 , H01B1/02 , H01M4/52 , H01M2/14
CPC分类号： H01M2/1653 , H01M4/505 , H01M4/525 , H01M10/056 , Y10T428/2982
摘要： The present invention provides a positive electrode active material that can suppress the necessity of performing sieving and is suitable for use in secondary batteries, particularly sodium secondary batteries. Also provided is a powder for a positive electrode active material as a raw material for the positive electrode active material. The powder for a positive electrode active material of the present invention comprises Mn-containing particles. In the cumulative particle size distribution on the volume basis of particles constituting the powder, D50, which is the particle diameter at a 50% cumulation measured from the smallest particle, is in the range of from 0.1 μm to 10 μm, and 90 vol % or more of the particles constituting the powder are in the range of from 0.3 times to 3 times D50. The powder for a positive electrode active material comprises Mn-containing particles, and 90 vol % or more of the particles constituting the powder are in the range of from 0.6 μm to 6 μm. The positive electrode active material is a powdery positive electrode active material obtained by calcining a mixture of the powder for positive electrode active material and a sodium compound. The positive electrode for sodium rechargeable batteries comprises the positive electrode active material.
摘要翻译：本发明提供能够抑制进行筛分的必要性的正极活性物质，适用于二次电池，特别是钠二次电池。还提供了作为正极活性物质的原料的正极活性物质的粉末。本发明的正极活性物质用粉末含有Mn粒子。在构成粉末的粒子的体积基础上的累积粒度分布中，从最小粒子测定的50％累积时的粒径D50为0.1μm〜10μm，90体积％或更多的构成粉末的颗粒在D50的0.3倍至3倍的范围内。用于正极活性物质的粉末包含含Mn颗粒，并且构成粉末的颗粒的90体积％以上在0.6μm至6μm的范围内。正极活性物质是通过煅烧正极活性物质粉末和钠化合物的混合物而获得的粉末状正极活性物质。钠可充电电池用正极包含正极活性物质。

10. 发明申请

US20120015230A1 MIXED METAL OXIDE, ELECTRODE, AND SODIUM SECONDARY BATTERY 有权
标题翻译：混合金属氧化物，电极和钠二次电池
公开(公告)号：US20120015230A1
公开(公告)日：2012-01-19
申请号：US13256159
申请日：2010-03-10
申请人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
发明人： Satoru Kuze , Masami Makidera , Taketsugu Yamamoto
IPC分类号： H01M4/131 , H01M2/16
CPC分类号： H01M4/50 , C01G45/1228 , C01G49/0018 , C01G49/0027 , C01G49/0036 , C01G51/006 , C01G51/42 , C01G53/42 , C01G53/50 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2004/32 , C01P2004/54 , C01P2006/16 , C01P2006/40 , C01P2006/80 , H01M2/16 , H01M2/1686 , H01M4/483 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/054 , H01M10/0565 , H01M10/0568 , H01M10/0569 , H01M10/36 , H01M2004/028 , H01M2200/10 , H01M2300/002 , H01M2300/0025 , H01M2300/0088 , Y02E60/122
摘要： Disclosed is a mixed metal oxide comprising Na, M1, and M2, where M1 represents at least one element selected from the group consisting of Mg, Ca, Sr, and Ba; and M2 represents at least one element selected from the group consisting of Mn, Fe, Co, and Ni, wherein the molar ratio of Na:M1:M2 is a:b:1, where a is a value within the range of not less than 0.5 and less than 1; b is a value within the range of more than 0 and not more than 0.5; and “a+b” is a value within the range of more than 0.5 and not more than 1. An electrode having an active material containing the mixed metal oxide is also disclosed. Further disclosed is an electrode containing the electrode active material as well as a sodium secondary battery comprising the electrode as a positive electrode.
摘要翻译：公开了包含Na，M1和M2的混合金属氧化物，其中M1表示选自Mg，Ca，Sr和Ba中的至少一种元素; M2表示选自Mn，Fe，Co和Ni中的至少一种元素，其中Na：M1：M2的摩尔比为a：b：1，其中a为不小于大于0.5且小于1; b是大于0且不大于0.5的范围内的值; 并且“a + b”是大于0.5且不大于1的范围内的值。还公开了具有含有该混合金属氧化物的活性物质的电极。还公开了含有电极活性物质的电极以及包含该电极作为正电极的钠二次电池。

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