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1. 发明授权

US08293936B2 Method for producing n-propyl acetate 有权
标题翻译：乙酸正丙酯的制造方法
公开(公告)号：US08293936B2
公开(公告)日：2012-10-23
申请号：US12993224
申请日：2009-05-20
申请人： Shigeru Hatanaka , Masayuki Fujimoto
发明人： Shigeru Hatanaka , Masayuki Fujimoto
IPC分类号： C07C67/283
CPC分类号： C07C67/283 , C07C69/14
摘要： Provided is a method for producing n-propyl acetate capable of suppressing the deterioration of a hydrogenation catalyst to such an extent that the catalyst can be industrially used, for example, in the case where n-propyl acetate is produced by performing a hydrogenation reaction in the presence of the hydrogenation catalyst using, as a raw material liquid, a liquid containing allyl acetate or the like which has been produced from propylene, oxygen and acetic acid and obtained using a purification process such as distillation. In such a method for producing n-propyl acetate, the concentration of a formyl group-containing compound (such as acrolein, propionaldehyde or 2-methylcrotonaldehyde) and the concentration of an acryloyloxy group-containing compound (such as acrylic acid or allyl acrylate) in the raw material liquid are respectively set to 100 ppm by mass or less. As a result, the deterioration of the hydrogenation catalyst can be suppressed to such an extent that the catalyst can be industrially used.
摘要翻译：提供一种生产能够抑制氢化催化剂劣化的乙酸正丙酯的方法，使得催化剂可以在工业上使用，例如在通过进行氢化反应制备乙酸正丙酯的情况下使用由丙烯，氧和乙酸制备并使用蒸馏等纯化方法得到的含有乙酸烯丙酯等的液体作为原料液体的存在。在这种乙酸正丙酯的制造方法中，含有甲酰基的化合物（丙烯醛，丙醛或2-甲基巴豆醛）的浓度和含丙烯酰氧基的化合物（丙烯酸或丙烯酸烯丙酯）的浓度，在原料液中分别设定为100质量ppm以下。结果，可以将氢化催化剂的劣化抑制到可以在工业上使用催化剂的程度。

2. 发明申请

US20110065951A1 METHOD FOR PRODUCING n-PROPYL ACETATE 有权
标题翻译：生产正丙酸乙酯的方法
公开(公告)号：US20110065951A1
公开(公告)日：2011-03-17
申请号：US12993224
申请日：2009-05-20
申请人： Shigeru Hatanaka , Masayuki Fujimoto
发明人： Shigeru Hatanaka , Masayuki Fujimoto
IPC分类号： C07C67/327
CPC分类号： C07C67/283 , C07C69/14
摘要： Provided is a method for producing n-propyl acetate capable of suppressing the deterioration of a hydrogenation catalyst to such an extent that the catalyst can be industrially used, for example, in the case where n-propyl acetate is produced by performing a hydrogenation reaction in the presence of the hydrogenation catalyst using, as a raw material liquid, a liquid containing allyl acetate or the like which has been produced from propylene, oxygen and acetic acid and obtained using a purification process such as distillation. In such a method for producing n-propyl acetate, the concentration of a formyl group-containing compound (such as acrolein, propionaldehyde or 2-methylcrotonaldehyde) and the concentration of an acryloyloxy group-containing compound (such as acrylic acid or allyl acrylate) in the raw material liquid are respectively set to 100 ppm by mass or less. As a result, the deterioration of the hydrogenation catalyst can be suppressed to such an extent that the catalyst can be industrially used.
摘要翻译：提供一种生产能够抑制氢化催化剂劣化的乙酸正丙酯的方法，使得催化剂可以在工业上使用，例如在通过进行氢化反应制备乙酸正丙酯的情况下使用由丙烯，氧和乙酸制备并使用蒸馏等纯化方法得到的含有乙酸烯丙酯等的液体作为原料液体的氢化催化剂的存在。在这种乙酸正丙酯的制造方法中，含有甲酰基的化合物（丙烯醛，丙醛或2-甲基巴豆醛）的浓度和含丙烯酰氧基的化合物（丙烯酸或丙烯酸烯丙酯）的浓度，在原料液中分别设定为100质量ppm以下。结果，可以将氢化催化剂的劣化抑制到可以在工业上使用催化剂的程度。

3. 发明授权

US06815796B2 Composite module and process of producing same 失效
标题翻译：复合模块及其生产工艺
公开(公告)号：US06815796B2
公开(公告)日：2004-11-09
申请号：US10313037
申请日：2002-12-06
申请人： Kenichi Ota , Manabu Satomi , Masayuki Fujimoto
发明人： Kenichi Ota , Manabu Satomi , Masayuki Fujimoto
IPC分类号： H01L2900
CPC分类号： H01L23/645 , H01L21/8252 , H01L23/50 , H01L23/5389 , H01L23/642 , H01L24/48 , H01L27/0605 , H01L27/0688 , H01L28/10 , H01L28/40 , H01L2224/05599 , H01L2224/45099 , H01L2224/48091 , H01L2224/48227 , H01L2224/85424 , H01L2924/00014 , H01L2924/01019 , H01L2924/01068 , H01L2924/01078 , H01L2924/09701 , H01L2924/10329 , H01L2924/14 , H01L2924/1423 , H01L2924/15153 , H01L2924/15165 , H01L2924/19041 , H01L2924/30107 , H01L2924/3011 , H01L2924/00 , H01L2224/45015 , H01L2924/207
摘要： A composite module and its production process which allow multiple functions, miniaturization, low power consumption and low costs without requiring any external chip parts at all. A high-frequency integrated circuit is embedded in a silicon substrate, a high-frequency high-capacity bypass capacitor and a matching coil using thin films of different types of materials are also formed on the silicon substrate, a high-frequency high-capacity bypass capacitor is further formed with an interlayer insulation film between them, and these elements and the high-frequency integrated circuit are connected via a wiring layer.
摘要翻译：复合模块及其生产过程，可以实现多种功能，小型化，低功耗和低成本，而无需任何外部芯片部件。高频集成电路嵌入硅衬底中，高频大容量旁路电容器和使用不同类型材料的薄膜的匹配线圈也形成在硅衬底上，高频高容量旁路电容器还在其间形成有层间绝缘膜，并且这些元件和高频集成电路经由布线层连接。

4. 发明授权

US4405478A Dielectric ceramic materials with insulated boundaries between crystal grains, and process for preparation 失效
标题翻译：介电陶瓷材料与晶粒之间具有绝缘边界，以及制备工艺
公开(公告)号：US4405478A
公开(公告)日：1983-09-20
申请号：US443781
申请日：1982-11-22
申请人： Kiyoshi Murase , Nobutatsu Yamaoka , Masayuki Fujimoto
发明人： Kiyoshi Murase , Nobutatsu Yamaoka , Masayuki Fujimoto
IPC分类号： C04B35/47 , H01G4/12 , C04B35/46 , H01B3/12
CPC分类号： H01G4/1281 , C04B35/47
摘要： A dielectric ceramic material composed of primary and secondary ingredients forming in combination a polycrystalline ceramic proper, and of insulating substances diffused throughout the intergranular boundaries of the ceramic proper for an increase in apparent relative dielectric constant. The primary ingredients comprise, in relative proportions, 90.68-99.88 wt. % SrTiO.sub.3, 0.07-5.32 wt. % Nb.sub.2 O.sub.5, and 0.05-4.00 wt. % GeO.sub.2. The secondary ingredients comprise 0.02-0.10 wt. part SiO.sub.2 and 0.01-0.03 wt. part Al.sub.2 O.sub.3 with respect to 100 wt. parts of the primary ingredients, with the weight ratio of SiO.sub.2 to Al.sub.2 O.sub.3 being from 1.5 to 5.0. The insulating substances comprise 0.03-2.90 wt. % PbO, 0.11-4.34 wt. % Bi.sub.2 O.sub.3, and 0.001-0.18 wt. % B.sub.2 O.sub.3 with respect to the total weight of the primary and the secondary ingredients. In the fabrication of bodies of the ceramic the mixture of the insulating substances is coated or otherwise layered on polycrystalline ceramic bodies prepared from the primary and secondary ingredients. The coated ceramic bodies are then heated to cause diffusion of the insulating substances throughout their intergranular boundaries.
摘要翻译：由主要和次要成分组成的介电陶瓷材料，其组合形成多晶陶瓷本身，并且绝缘物质在陶瓷本身的整个晶界处扩散，以增加表观相对介电常数。主要成分以相对比例包含90.68-99.88wt。％SrTiO 3，0.07-5.32wt。％Nb2O5和0.05-4.00wt。％GeO2。次要成分包含0.02-0.10wt。部分SiO2和0.01-0.03wt。部分Al2O3相对于100wt。主要成分的一部分，SiO 2与Al 2 O 3的重量比为1.5-5.0。绝缘物质包含0.03-2.90重量％％PbO，0.11-4.34wt。％Bi 2 O 3和0.001-0.18wt。％B2O3相对于初级和次级成分的总重量。在陶瓷体的制造中，绝缘物质的混合物被涂覆或以其它方式分层在由初级和次级成分制备的多晶陶瓷体上。然后将涂覆的陶瓷体加热，使绝缘物质扩散到其晶间界面。

5. 发明授权

US4405474A Dielectric ceramic materials with insulated boundaries between crystal grains, and process for preparation 失效
标题翻译：介电陶瓷材料与晶粒之间具有绝缘边界，以及制备工艺
公开(公告)号：US4405474A
公开(公告)日：1983-09-20
申请号：US443775
申请日：1982-11-22
申请人： Kiyoshi Murase , Nobutatsu Yamaoka , Masayuki Fujimoto
发明人： Kiyoshi Murase , Nobutatsu Yamaoka , Masayuki Fujimoto
IPC分类号： H01B3/12 , C04B35/47 , H01G4/12 , C04B35/46
CPC分类号： H01G4/1281 , C04B35/47
摘要： A dielectric ceramic material composed of primary and secondary ingredients forming in combination a polycrystalline ceramic proper, and of insulating substances diffused throughout the intergranular boundaries of the ceramic proper for an increase in apparent relative dielectric constant. The primary ingredients comprise in relative proportions, 96.70-99.83 wt. % SrTiO.sub.3, 0.15-2.30 wt. % WO.sub.3, and 0.02-1.00 wt. % CuO. The secondary ingredients comprise 0.02-0.10 wt %. part SiO.sub.2 and 0.01-0.03 wt. part Al.sub.2 O.sub.3 with respect to 100 wt. parts of the primary ingredients, with the weight ratio of SiO.sub.2 to Al.sub.2 O.sub.3 being from 1.5 to 5.0. The insulating substances comprise 0.003-2.83 wt. % PbO, 0.10-4.30 wt. % Bi.sub.2 O.sub.3, and 0.001-0.18 wt. % B.sub.2 O.sub.3 with respect to the total weight of the primary and the secondary ingredients. In the fabrication of bodies of the ceramic the mixture of the insulating substances is coated or otherwise layered on polycrystalline ceramic bodies prepared from the primary and secondary ingredients. The coated ceramic bodies are then heated to cause diffusion of the insulating substances throughout their intergranular boundaries.
摘要翻译：由主要和次要成分组成的介电陶瓷材料，其组合形成多晶陶瓷本身，并且绝缘物质在陶瓷本身的整个晶界处扩散，以增加表观相对介电常数。主要成分包括相对比例为96.70-99.83wt。％SrTiO 3，0.15-2.30重量％％WO3和0.02-1.00wt。％CuO。次要成分占0.02-0.10重量％。部分SiO2和0.01-0.03wt。部分Al2O3相对于100wt。主要成分的一部分，SiO 2与Al 2 O 3的重量比为1.5-5.0。绝缘物质包含0.003-2.83wt。％PbO，0.10-4.30wt。％Bi 2 O 3和0.001-0.18wt。％B2O3相对于初级和次级成分的总重量。在陶瓷体的制造中，绝缘物质的混合物被涂覆或以其它方式分层在由初级和次级成分制备的多晶陶瓷体上。然后将涂覆的陶瓷体加热，使绝缘物质扩散到其晶间界面。

6. 发明授权

US4405472A Dielectric ceramic materials with insulated boundaries between crystal grains, and process for preparation 失效
标题翻译：介电陶瓷材料与晶粒之间具有绝缘边界，以及制备工艺
公开(公告)号：US4405472A
公开(公告)日：1983-09-20
申请号：US443773
申请日：1982-11-22
申请人： Kiyoshi Murase , Nobutatsu Yamaoka , Masayuki Fujimoto
发明人： Kiyoshi Murase , Nobutatsu Yamaoka , Masayuki Fujimoto
IPC分类号： H01B3/12 , C04B35/47 , H01G4/12 , C04B35/46
CPC分类号： C04B35/47 , H01G4/1281
摘要： A dielectric ceramic material composed of primary and secondary ingredients forming in combination a polycrystalline ceramic proper, and of insulating substances diffused throughout the intergranular boundaries of the ceramic proper for an increase in apparent relative dielectric constant. The primary ingredients comprise, in relative proportions, 95.18-99.65 wt. % SrTiO.sub.3, 0.33-3.32 wt. % Ta.sub.2 O.sub.5, and 0.02-1.50 wt. % CuO. The secondary ingredients comprise 0.02-0.10 wt. % part SiO.sub.2 and 0.01-0.03 wt. part Al.sub.2 O.sub.3 with respect to 100 wt. parts of the primary ingredients, with the weight ratio of SiO.sub.2 to Al.sub.2 O.sub.3 being from 1.50 to 5.0. The insulating substances comprise 0.03-2.75 wt. % PbO, 0.11-4.22 wt. % Bi.sub.2 O.sub.3, and 0.001-0.18 wt. % B.sub.2 O.sub.3 with respect to the total weight of the primary and the secondary ingredients. In the fabrication of bodies of the ceramic the mixture of the insulating substances is coated or otherwise layered on polycrystalline ceramic bodies prepared from the primary and secondary ingredients. The coated ceramic bodies are then heated to cause diffusion of the insulating substances throughout their intergranular boundaries.
摘要翻译：由主要和次要成分组成的介电陶瓷材料，其组合形成多晶陶瓷本身，并且绝缘物质在陶瓷本身的整个晶界处扩散，以增加表观相对介电常数。主要成分以相对比例包含95.18-99.65wt。％SrTiO3，0.33-3.32wt。％Ta2O5和0.02-1.50wt。％CuO。次要成分包含0.02-0.10wt。％部分SiO 2和0.01-0.03重量％部分Al2O3相对于100wt。主要成分的一部分，SiO 2与Al 2 O 3的重量比为1.50〜5.0。绝缘物质包含0.03-2.75重量％％PbO，0.11-4.22wt。％Bi 2 O 3和0.001-0.18wt。％B2O3相对于初级和次级成分的总重量。在陶瓷体的制造中，绝缘物质的混合物被涂覆或以其它方式分层在由初级和次级成分制备的多晶陶瓷体上。然后将涂覆的陶瓷体加热，使绝缘物质扩散到其晶间界面。

7. 发明授权

US09187338B2 Process for manufacturing needle-shaped strontium carbonate particles 有权
标题翻译：针状碳酸锶粒子的制造方法
公开(公告)号：US09187338B2
公开(公告)日：2015-11-17
申请号：US13985322
申请日：2012-02-15
申请人： Fumio Okada , Takeshi Himoto , Masayuki Fujimoto
发明人： Fumio Okada , Takeshi Himoto , Masayuki Fujimoto
IPC分类号： C01F11/18
CPC分类号： C01F11/187 , C01P2004/03 , C01P2004/10 , C01P2004/54 , C01P2004/60 , C01P2004/61 , C01P2006/12
摘要： Acicular strontium carbonate particles are manufactured by introducing gaseous carbon dioxide into an aqueous solution or suspension of strontium hydroxide having a concentration of 1 to 20 wt. %, at a flow rate of 0.5 to 200 mL/min., relative to one gram of the strontium hydroxide, while stirring the solution or suspension in the presence of a dicarboxylic acid, in which the dicarboxylic acid comprises a divalent linear hydrocarbon group having one to four carbon atoms and carboxyl group bonded to each terminals, with the proviso that the linear hydrocarbon group may be substituted with one or more C1-6 alkyl groups, and thus carbonating the strontium hydroxide.
摘要翻译：通过将气态二氧化碳引入浓度为1〜20重量％的氢氧化锶的水溶液或悬浮液中来制造碳酸锶碳酸盐颗粒。相对于1克氢氧化锶，流速为0.5-200毫升/分钟，同时在二羧酸存在下搅拌溶液或悬浮液，其中二羧酸包含二价直链烃基，其具有一个至四个碳原子和与每个末端键合的羧基，条件是直链烃基可以被一个或多个C 1-6烷基取代，从而使氢氧化锶碳酸化。

8. 发明申请

US20140065052A1 PROCESS FOR MANUFACTURING NEEDLE-SHAPED STRONTIUM CARBONATE PARTICLES 有权
标题翻译：制造针状碳酸锶颗粒的方法
公开(公告)号：US20140065052A1
公开(公告)日：2014-03-06
申请号：US13985322
申请日：2012-02-15
申请人： Fumio Okada , Takeshi Himoto , Masayuki Fujimoto
发明人： Fumio Okada , Takeshi Himoto , Masayuki Fujimoto
IPC分类号： C01F11/18
CPC分类号： C01F11/187 , C01P2004/03 , C01P2004/10 , C01P2004/54 , C01P2004/60 , C01P2004/61 , C01P2006/12
摘要： Acicular strontium carbonate particles are manufactured by introducing gaseous carbon dioxide into an aqueous solution or suspension of strontium hydroxide having a concentration of 1 to 20 wt. %, at a flow rate of 0.5 to 200 mL/min., relative to one gram of the strontium hydroxide, while stirring the solution or suspension in the presence of a dicarboxylic acid, in which the dicarboxylic acid comprises a divalent linear hydrocarbon group having one to four carbon atoms and carboxyl group bonded to each terminals, with the proviso that the linear hydrocarbon group may be substituted with one or more C1-6 alkyl groups, and thus carbonating the strontium hydroxide.
摘要翻译：通过将气态二氧化碳引入浓度为1〜20重量％的氢氧化锶的水溶液或悬浮液中来制造碳酸锶碳酸盐颗粒。相对于1克氢氧化锶，流速为0.5-200毫升/分钟，同时在二羧酸存在下搅拌溶液或悬浮液，其中二羧酸包含二价直链烃基，其具有一个至四个碳原子和与每个末端键合的羧基，条件是直链烃基可以被一个或多个C 1-6烷基取代，从而使氢氧化锶碳酸化。

9. 发明授权

US4405479A Dielectric ceramic materials with insulated boundaries between crystal grains, and process for preparation 失效
标题翻译：介电陶瓷材料与晶粒之间具有绝缘边界，以及制备工艺
公开(公告)号：US4405479A
公开(公告)日：1983-09-20
申请号：US443782
申请日：1982-11-22
申请人： Kiyoshi Murase , Nobutatsu Yamaoka , Masayuki Fujimoto
发明人： Kiyoshi Murase , Nobutatsu Yamaoka , Masayuki Fujimoto
IPC分类号： C04B35/46 , C04B35/47 , H01B3/12 , H01G4/12
CPC分类号： H01G4/1281 , C04B35/47
摘要： A dielectric ceramic material composed of primary and secondary ingredients forming in combination a polycrystalline ceramic proper, and of insulating substances diffused throughout the intergranular boundaries of the ceramic proper for an increase in apparent relative dielectric constant. The primary ingredients comprise, in relative proportions, 95.20-99.80 wt. % SrTiO.sub.3, 0.15-2.30 wt. % WO.sub.3, and 0.05-2.50 wt. % ZnO. The seconary ingredients comprise 0.02-0.10 wt. part SiO.sub.2 and 0.01-0.03 wt. part Al.sub.2 O.sub.3 with respect to 100 wt. parts of the primary ingredients, with the weight ratio of SiO.sub.2 to Al.sub.2 O.sub.3 being from 1.5 to 5.0. The insulating substances comprise 0.03-2.75 wt. % PbO, 0.11-4.23 wt. % Bi.sub.2 O.sub.3, and 0.001-0.18 wt. % B.sub.2 O.sub.3 with respect to the total weight of the primary and the secondary ingredients. In the fabrication of bodies of the ceramic the mixture of the insulating substances is coated or otherwise layered on polycrystalline ceramic bodies prepared from the primary and secondary ingredients. The coated ceramic bodies are then heated to cause diffusion of the insulating substances throughout their intergranular boundaries.
摘要翻译：由主要和次要成分组成的介电陶瓷材料，其组合形成多晶陶瓷本身，并且绝缘物质在陶瓷本身的整个晶界处扩散，以增加表观相对介电常数。主要成分以相对比例包含95.20-99.80wt。％SrTiO 3，0.15-2.30重量％％WO3和0.05-2.50wt。％ZnO。所述第二成分包含0.02-0.10wt。部分SiO2和0.01-0.03wt。部分Al2O3相对于100wt。主要成分的一部分，SiO 2与Al 2 O 3的重量比为1.5-5.0。绝缘物质包含0.03-2.75重量％％PbO，0.11-4.23wt。％Bi 2 O 3和0.001-0.18wt。％B2O3相对于初级和次级成分的总重量。在陶瓷体的制造中，绝缘物质的混合物被涂覆或以其它方式分层在由初级和次级成分制备的多晶陶瓷体上。然后将涂覆的陶瓷体加热，使绝缘物质扩散到其晶间界面。

10. 发明授权

US09102810B2 Alkaline earth metal carbonate micropowder 有权
标题翻译：碱土金属碳酸盐微粉
公开(公告)号：US09102810B2
公开(公告)日：2015-08-11
申请号：US13985328
申请日：2012-02-15
申请人： Fumio Okada , Takeshi Himoto , Masayuki Fujimoto
发明人： Fumio Okada , Takeshi Himoto , Masayuki Fujimoto
IPC分类号： C01F11/18 , C09C3/08 , C09C1/02 , C08K3/26 , C01F11/08 , C08K5/09 , B82Y30/00
CPC分类号： C08K3/26 , B82Y30/00 , C01F11/08 , C01F11/185 , C01F11/187 , C01P2004/10 , C01P2004/51 , C01P2004/52 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C08K5/09 , C09C1/02 , C09C1/021 , C09C1/024 , C09C3/08
摘要： Dispersibility of an alkaline earth metal carbonate micropowder in a polymer resin or in an organic solvent is improved by treating the surface of the alkaline earth metal micropowder with a surfactant having hydrophilic groups and hydrophobic groups and groups that form anions in water.
摘要翻译：碱土金属碳酸盐微粉在聚合物树脂或有机溶剂中的分散性通过用具有亲水基团的表面活性剂和在水中形成阴离子的疏水性基团和基团进行处理来提高碱土金属微粉的表面。

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