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1. 发明申请

US20130253238A1 METHOD FOR PRODUCING LUBRICATING BASE OIL WITH LOW CLOUD POINT AND HIGH VISCOSITY INDEX 审中-公开
标题翻译：用于生产具有低云点和高粘度指数的润滑基础油的方法
公开(公告)号：US20130253238A1
公开(公告)日：2013-09-26
申请号：US13820839
申请日：2011-06-03
申请人： Sheng Hu , Zhijian Tian , Lijun Yan , Wenle Li , Yunpeng Xu , Kebin Chi , Xiangbin Meng , Bingchun Wang , Mingwei Tan , Lei Wang , Yanfeng Liu , Jinling Zhu , Shanbin Gao
发明人： Sheng Hu , Zhijian Tian , Lijun Yan , Wenle Li , Yunpeng Xu , Kebin Chi , Xiangbin Meng , Bingchun Wang , Mingwei Tan , Lei Wang , Yanfeng Liu , Jinling Zhu , Shanbin Gao
IPC分类号： C10G69/02
CPC分类号： C10G69/02 , B01J23/42 , B01J29/005 , B01J29/44 , B01J29/7484 , B01J29/7492 , B01J29/85 , B01J35/1019 , B01J35/1042 , B01J35/1047 , C10G45/08 , C10G45/58 , C10G47/18 , C10G65/12 , C10G2300/1022 , C10G2300/1074 , C10G2300/301 , C10G2300/302 , C10G2300/304 , C10G2300/4018 , C10G2400/02 , C10G2400/10
摘要： The present invention relates to a method for producing lubricating base oil with a low cloud point and a high viscosity index. In the method, a lubricating base oil with a low pour point, a low cloud point and a high viscosity index is produced by a hydrorefining-isomerization/asymmetrical cracking-hydrofinishing in the presence of hydrogen, wherein a highly waxy heavy fraction oil having an initial boiling point of 300° C. to 460° C., a wax content of 5% or more, a pour point of −20° C. or more and a cloud point of −5° C. or more is used as a raw material, and naphtha and middle fraction oil being co-produced. The method is characterized mainly in the high yield of heavy base oil, a low pour point and cloud point, a high viscosity and viscosity index of the base oil.
摘要翻译：本发明涉及一种具有低浊点和高粘度指数的润滑油基油的制备方法。在该方法中，通过在氢气存在下进行加氢精制 - 异构化/不对称裂化加氢精制来制备具有低倾点，低浊点和高粘度指数的润滑基础油，其中高蜡状重馏分油具有初沸点为300℃〜460℃，蜡含量为5％以上，倾点为-20℃以上，浊点为-5℃以上。原料，以及石脑油和中间馏分油共同生产。该方法的特点主要是重质油的产率高，倾点低，浊点高，基油的高粘度和粘度指数。

2. 发明授权

US09334405B2 Chromium-free insulation coating material for non-oriented silicon steel 有权
标题翻译：无取向硅钢的无铬绝缘涂料
公开(公告)号：US09334405B2
公开(公告)日：2016-05-10
申请号：US13818258
申请日：2011-04-13
申请人： Yunpeng Xu , Yongjie Yang , Dengfeng Li , Yaming Ji , Zipeng Zhao , Lingyun Chen , Xiao Chen , Jie Huang
发明人： Yunpeng Xu , Yongjie Yang , Dengfeng Li , Yaming Ji , Zipeng Zhao , Lingyun Chen , Xiao Chen , Jie Huang
IPC分类号： C09D5/00 , C09D5/08 , C09D7/12 , C09D163/00 , H01B3/40
CPC分类号： C09D5/00 , C09D5/084 , C09D7/61 , C09D163/00 , H01B3/40
摘要： The present invention refers to a chromium-free insulation coating material for non-oriented silicon steel, comprising, in parts by weight, the following components: metal dihydrogen phosphate salt of 100 parts, epoxy resin of 10˜60 parts, naphthenate drier or isooctanoate metal salt drier of 0.001˜10 parts, organic solvent of 0.001˜100 parts and pure water of 60˜2000 parts. The metal dihydrogen phosphate salt is Al(H2PO4)3, Mg(H2PO4)2, Ca(H2PO4)2 or Zn(H2PO4)2; the epoxy resin is water-soluble epoxy resin or epoxy resin emulsion. Chromium-free insulation coating material of the present invention, after being coated on non-oriented silicon steel, renders highly transparent appearance, and has excellent insulativity, corrosion resistance, adhesiveness, weldability and manufacturability, so as to eliminate defects of the existing chromium-free coating, such as sticky and un-wear-resistant and to meet environment protection requirements.
摘要翻译：本发明涉及一种用于非取向硅钢的无铬绝缘涂层材料，其包含以重量份计的以下成分：100份的金属二氢磷酸盐，10〜60份的环氧树脂，环烷酸酯干燥剂或异辛酸酯金属盐干燥剂为0.001〜10份，有机溶剂为0.001〜100份，纯水为60〜2000份。磷酸金属盐为Al（H 2 PO 4）3，Mg（H 2 PO 4）2，Ca（H 2 PO 4）2或Zn（H 2 PO 4）2; 环氧树脂是水溶性环氧树脂或环氧树脂乳液。本发明的无铬绝缘涂层材料涂覆在非取向硅钢上后，外观高透明，绝缘性，耐腐蚀性，粘合性，焊接性和可制造性优异，从而消除了现有的铬 - 自由涂层，如粘性和不耐磨损，符合环保要求。

3. 发明申请

US20130292005A1 ANNUALING SEPARATION AGENT FOR PRODUCING GRAIN-ORIENTED SILICON STEEL WITH SMOOTH SURFACE AND GOOD MAGNETIC PROPERTY 审中-公开
标题翻译：用于生产具有平滑表面和良好磁性性能的面向导向的硅钢的年度分离剂
公开(公告)号：US20130292005A1
公开(公告)日：2013-11-07
申请号：US13880278
申请日：2011-04-14
申请人： Zipeng Zhao , Yaming Ji , Yongjie Yang , Guobao Li , Dengfeng Li , Yunpeng Xu
发明人： Zipeng Zhao , Yaming Ji , Yongjie Yang , Guobao Li , Dengfeng Li , Yunpeng Xu
IPC分类号： C21D1/70
CPC分类号： C21D1/70 , C21D1/26 , C21D1/68 , C21D3/04 , C21D8/12 , C21D9/46 , C22C38/02 , C22C38/04 , C22C38/06 , C22C38/16 , H01F1/16
摘要： An annealing separator for manufacturing grain-oriented silicon steel with mirror-like surface having good magnetic performance consists of the composition of which is 77˜98 by wt % of Al2O3 powder, 1˜8 by wt % of alkaline earth powder, 1˜15 by wt % of alkali metal chloride and/or alkaline earth metal chloride. The annealing separator of the invention can avoid forming a glass-film undercoating on the surface of the steel sheet during high-temperature annealing, and at the same time, the oxide embedded at near-surface of the sheet is removed by means of corrosive reaction of the chloride, so that a produce with smooth surface and stable magnetic performance is obtained.
摘要翻译：用于制造具有良好磁性能的镜面状的晶粒取向硅钢的退火分离剂组成为Al2O3粉末的77〜98重量％，碱土金属粉末1〜8重量％，碱土金属粉末1〜的碱金属氯化物和/或碱土金属氯化物。本发明的退火分离装置可以避免在高温退火时在钢板的表面上形成玻璃膜底涂层，同时通过腐蚀反应除去嵌入片材近表面的氧化物的氯化物，从而获得具有光滑表面和稳定磁性能的产品。

4. 发明申请

US20150203425A1 METHOD FOR PRODUCING CRESOL FROM PHENOL AND METHANOL VIA GAS PHASE ALKYLATION 有权
标题翻译：通过气相烷基化生产酚和甲醇的方法
公开(公告)号：US20150203425A1
公开(公告)日：2015-07-23
申请号：US14416209
申请日：2012-07-24
申请人： Kunyuan Wang , Yunpeng Xu , Zhongmin Liu
发明人： Kunyuan Wang , Yunpeng Xu , Zhongmin Liu
IPC分类号： C07C37/11
CPC分类号： C07C37/11 , B01J29/00 , B01J29/40 , B01J29/46 , B01J29/7007 , B01J29/7038 , B01J29/7615 , B01J29/7676 , B01J37/28 , B01J2229/186 , B01J2229/32 , B01J2229/36 , B01J2229/37 , B01J2229/42 , C07C37/16 , Y02P20/52 , C07C39/07
摘要： The present invention relates to a method for producing cresol from phenol and methanol via gas phase alkylation, in which phenol and methanol are preheated and mixed with diluent gas, then the mixture continuously go through a catalyst bed comprising the catalyst for alkylation of phenol with methanol, to produce cresol by gas phase reaction at the reaction temperature of 200-500° C. and the weight hourly space velocity of 0.5˜20 h−1. The catalyst for alkylation of phenol with methanol is obtained by modification steps and using ZSM-5 zeolite, MCM-22 zeolite or Beta zeolite as an active composition. Using phenol and methanol as feedstock, the cresol selectivity can reach to 90%, and the p-cresol selectivity can reach to 58%. The catalyst is environmental friendly and non-corrosive to the equipment with a good stability and a broad prospect in industrial application.
摘要翻译：本发明涉及一种通过气相烷基化从苯酚和甲醇生产甲酚的方法，其中苯酚和甲醇被预热并与稀释气体混合，然后将混合物连续地通过催化剂床，该催化剂床包含用甲醇烷基化苯酚的催化剂在200-500℃的反应温度下通过气相反应生产甲酚，重时空速为0.5〜20h-1。用甲醇烷基化苯酚的催化剂是通过改性步骤和使用ZSM-5沸石，MCM-22沸石或β沸石作为活性组合物得到的。使用苯酚和甲醇作为原料，甲酚选择性可以达到90％，对甲酚的选择性可以达到58％。催化剂环保，无腐蚀性，稳定性好，工业应用前景广阔。

5. 发明申请

US20110180187A1 METHOD FOR PRODUCING GRAIN-ORIENTED SILICON STEEL CONTAINING COPPER 有权
标题翻译：生产含有铜的含晶硅钢的方法
公开(公告)号：US20110180187A1
公开(公告)日：2011-07-28
申请号：US13058073
申请日：2009-04-24
申请人： Yaming JI , Huande Sun , Guohua Yang , Yongjie Yang , Yunpeng Xu , Changguo Huang , Guobao Li
发明人： Yaming JI , Huande Sun , Guohua Yang , Yongjie Yang , Yunpeng Xu , Changguo Huang , Guobao Li
IPC分类号： C21D8/00 , B22D11/00
CPC分类号： C22C38/04 , C21D1/26 , C21D6/008 , C21D8/02 , C21D8/12 , C21D8/1233 , C21D8/1255 , C21D8/1266 , C21D8/1283 , C21D10/005 , C22C38/001 , C22C38/02 , C22C38/06 , C22C38/16
摘要： A method of manufacturing oriented Si steel containing Cu with high electric-magnetic property comprises: hot rolling slab; after first cold rolling, heating it to 800° C. or higher temperature and performing intermediate decarburization annealing in a protective atmosphere with PH2O/PH2 of 0.50˜0.88 for 3-8 minutes, to decrease carbon content of the steel plate to less than 30 ppm; then peening and acid-pickling to remove oxide of Fe on surface and to control oxygen content to lower than 500 ppm; secondary cold rolling to final thickness and coating separation agent in water-slurry form; drying to decrease water content to lower than 1.5%; high-temperature annealing in a protective atmosphere containing hydrogen with oxidation degree (PH2O/PH2) of 0.0001-0.2; finally applying a tension coating and leveling tension annealing.
摘要翻译：含有具有高电磁性能的Cu的取向Si钢的方法包括：热轧板; 在第一次冷轧后，加热到800℃或更高的温度，并在保护气氛中进行中间脱碳退火，PH2O / PH2为0.50〜0.88，3-8分钟，将钢板的碳含量降低到30 ppm; 然后进行喷丸和酸洗以除去表面上的Fe的氧化物，并控制氧含量低于500ppm; 二次冷轧至最终厚度，涂层分离剂为水浆形式; 干燥以减少含水量低于1.5％; 在含氢氧化程度（PH2O / PH2）为0.0001-0.2的保护气氛中进行高温退火; 最后施加张力涂层和流平张力退火。

6. 发明授权

US08231739B2 Method for producing grain-oriented silicon steel containing copper 有权
标题翻译：含铜的晶粒取向硅钢的制造方法
公开(公告)号：US08231739B2
公开(公告)日：2012-07-31
申请号：US13058073
申请日：2009-04-24
申请人： Yaming Ji , Huande Sun , Guohua Yang , Yongjie Yang , Yunpeng Xu , Changguo Huang , Guobao Li
发明人： Yaming Ji , Huande Sun , Guohua Yang , Yongjie Yang , Yunpeng Xu , Changguo Huang , Guobao Li
IPC分类号： H01F1/147
CPC分类号： C22C38/04 , C21D1/26 , C21D6/008 , C21D8/02 , C21D8/12 , C21D8/1233 , C21D8/1255 , C21D8/1266 , C21D8/1283 , C21D10/005 , C22C38/001 , C22C38/02 , C22C38/06 , C22C38/16
摘要： A method of manufacturing oriented Si steel containing Cu with high electric-magnetic property comprises: hot rolling slab; after first cold rolling, heating it to 800° C. or higher temperature and performing intermediate decarburization annealing in a protective atmosphere with PH2O/PH2 of 0.50˜0.88 for 3-8 minutes, to decrease carbon content of the steel plate to less than 30 ppm; then peening and acid-pickling to remove oxide of Fe on surface and to control oxygen content to lower than 500 ppm; secondary cold rolling to final thickness and coating separation agent in water-slurry form; drying to decrease water content to lower than 1.5%; high-temperature annealing in a protective atmosphere containing hydrogen with oxidation degree (PH2O/PH2) of 0.0001-0.2; finally applying a tension coating and leveling tension annealing.
摘要翻译：含有具有高电磁性能的Cu的取向Si钢的方法包括：热轧板; 在第一次冷轧后，加热到800℃或更高的温度，并在保护气氛中进行中间脱碳退火，PH2O / PH2为0.50〜0.88，3-8分钟，将钢板的碳含量降低到30 ppm; 然后进行喷丸和酸洗以除去表面上的Fe的氧化物，并控制氧含量低于500ppm; 二次冷轧至最终厚度，涂层分离剂为水浆形式; 干燥以减少含水量低于1.5％; 在含氢氧化程度（PH2O / PH2）为0.0001-0.2的保护气氛中进行高温退火; 最后施加张力涂层和流平张力退火。

7. 发明授权

US09212116B2 Method for producing cresol from phenol and methanol via gas phase alkylation 有权
标题翻译：通过气相烷基化从苯酚和甲醇生产甲酚的方法
公开(公告)号：US09212116B2
公开(公告)日：2015-12-15
申请号：US14416209
申请日：2012-07-24
申请人： Kunyuan Wang , Yunpeng Xu , Zhongmin Liu
发明人： Kunyuan Wang , Yunpeng Xu , Zhongmin Liu
IPC分类号： C07C37/11 , C07C37/16 , B01J29/00 , B01J29/40 , B01J29/70
CPC分类号： C07C37/11 , B01J29/00 , B01J29/40 , B01J29/46 , B01J29/7007 , B01J29/7038 , B01J29/7615 , B01J29/7676 , B01J37/28 , B01J2229/186 , B01J2229/32 , B01J2229/36 , B01J2229/37 , B01J2229/42 , C07C37/16 , Y02P20/52 , C07C39/07
摘要： The present invention relates to a method for producing cresol from phenol and methanol via gas phase alkylation, in which phenol and methanol are preheated and mixed with diluent gas, then the mixture continuously go through a catalyst bed comprising the catalyst for alkylation of phenol with methanol, to produce cresol by gas phase reaction at the reaction temperature of 200˜500° C. and the weight hourly space velocity of 0.5˜20 h−1. The catalyst for alkylation of phenol with methanol is obtained by modification steps and using ZSM-5 zeolite, MCM-22 zeolite or Beta zeolite as an active composition. Using phenol and methanol as feedstock, the cresol selectivity can reach to 90%, and the p-cresol selectivity can reach to 58%. The catalyst is environmental friendly and non-corrosive to the equipment with a good stability and a broad prospect in industrial application.
摘要翻译：本发明涉及一种通过气相烷基化从苯酚和甲醇生产甲酚的方法，其中苯酚和甲醇被预热并与稀释气体混合，然后将混合物连续地通过催化剂床，该催化剂床包含用甲醇烷基化苯酚的催化剂在200〜500℃的反应温度下通过气相反应生产甲酚，重时空速为0.5〜20h-1。用甲醇烷基化苯酚的催化剂是通过改性步骤和使用ZSM-5沸石，MCM-22沸石或β沸石作为活性组合物得到的。使用苯酚和甲醇作为原料，甲酚选择性可以达到90％，对甲酚的选择性可以达到58％。催化剂环保，无腐蚀性，稳定性好，工业应用前景广阔。

8. 发明申请

US20130203896A1 Chromium-Free Insulation Coating Material for Non-Oriented Silicon Steel 有权
标题翻译：用于非定向硅钢的无铬绝缘涂层材料
公开(公告)号：US20130203896A1
公开(公告)日：2013-08-08
申请号：US13818258
申请日：2011-04-13
申请人： Yunpeng Xu , Yongjie Yang , Dengfeng Li , Yaming Ji , Zipeng Zhao , Lingyun Chen , Xiao Chen , Jie Huang
发明人： Yunpeng Xu , Yongjie Yang , Dengfeng Li , Yaming Ji , Zipeng Zhao , Lingyun Chen , Xiao Chen , Jie Huang
IPC分类号： C09D5/00
CPC分类号： C09D5/00 , C09D5/084 , C09D7/61 , C09D163/00 , H01B3/40
摘要： The present invention refers to a chromium-free insulation coating material for non-oriented silicon steel, comprising, in parts by weight, the following components: metal dihydrogen phosphate salt of 100 parts, epoxy resin of 10˜60 parts, naphthenate drier or isooctanoate metal salt drier of 0.001˜10 parts, organic solvent of 0.001˜100 parts and pure water of 60˜2000 parts. The metal dihydrogen phosphate salt is Al(H2PO4)3, Mg(H2PO4)2, Ca(H2PO4)2 or Zn(H2PO4)2; the epoxy resin is water-soluble epoxy resin or epoxy resin emulsion. Chromium-free insulation coating material of the present invention, after being coated on non-oriented silicon steel, renders highly transparent appearance, and has excellent insulativity, corrosion resistance, adhesiveness, weldability and manufacturability, so as to eliminate defects of the existing chromium-free coating, such as sticky and un-wear-resistant and to meet environment protection requirements.
摘要翻译：本发明涉及一种用于非取向硅钢的无铬绝缘涂层材料，其包含以重量份计的以下组分：100份的金属二氢磷酸盐，10〜60份的环氧树脂，环烷酸盐干燥剂或异辛酸酯金属盐干燥剂为0.001〜10份，有机溶剂为0.001〜100份，纯水为60〜2000份。磷酸金属盐为Al（H 2 PO 4）3，Mg（H 2 PO 4）2，Ca（H 2 PO 4）2或Zn（H 2 PO 4）2; 环氧树脂是水溶性环氧树脂或环氧树脂乳液。本发明的无铬绝缘涂层材料涂覆在非取向硅钢上后，外观高透明，绝缘性，耐腐蚀性，粘合性，焊接性和可制造性优异，从而消除了现有的铬 - 自由涂层，如粘性和不耐磨损，符合环保要求。

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