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1. 发明授权

US6069192A Low fiber-loading composites with hybridized fiber/matrix interface 有权
标题翻译：低纤维加载复合材料与杂化纤维/基质界面
公开(公告)号：US6069192A
公开(公告)日：2000-05-30
申请号：US172334
申请日：1998-10-13
申请人： Shalaby W. Shalaby , Jacqueline M. Allan , Meng Deng
发明人： Shalaby W. Shalaby , Jacqueline M. Allan , Meng Deng
IPC分类号： C04B16/06 , C08L23/06 , C08L23/10 , D06M11/55 , D06M13/288 , D06M13/332 , D06M13/368 , D06M15/263 , D06M15/65 , C08K9/00
CPC分类号： C04B16/0625 , D06M11/55 , D06M13/288 , D06M13/332 , D06M13/368 , D06M15/263 , D06M15/65 , C08F110/02 , C08L23/06 , C08L23/10
摘要： Disclosed are fiber-reinforced composites having untraditionally low fiber loading and a novel form of hybridized interface. Typical examples of fiber-matrix combinations capable of developing such interfaces include surface-phosphonylated ultrahigh molecular weight polyethylene (UHMW-PE) and polypropylene (PP) yarns (or fabric constructs) and epoxy resin, acrylic resin, and cement. For further improvement of the hybridized interface and the overall composite properties, the surface-phosphonylated fiber may be post-treated with reagents that will improve the abridging of the fibers to the matrix through physicochemically hybridized interfaces. Compared with composites having unmodified fiber, those based on modified ones, with or without post-treatment, exhibit a substantial increase in physicomechanical properties at exceptionally low fiber loading, ranging from about 0.1 to 35 percent by weight, preferably from about 0.1 to about 20 percent by weight, most preferably less than 10 percent by weight. Among these properties are maximum tensile strength, fracture toughness, and modulus.
摘要翻译：公开了具有非常低的纤维负载和新颖形式的杂化界面的纤维增强复合材料。能够开发这种界面的纤维 - 基质组合物的典型实例包括表面膦酰化的超高分子量聚乙烯（UHMW-PE）和聚丙烯（PP）纱线（或织物构造）和环氧树脂，丙烯酸树脂和水泥。为了进一步改善杂交界面和整体复合性质，可以用可以通过物理化学杂交界面改善纤维对基质的桥接的试剂对表面膦酰化的纤维进行后处理。与具有未改性纤维的复合材料相比，具有或不具有后处理的基于改性纤维的复合材料在非常低的纤维负载下显示出显着增加的物理机械性能，其范围为约0.1至35重量％，优选约0.1至约20 重量百分比，最优选小于10重量％。这些性能中的最大拉伸强度，断裂韧性和模量。

2. 发明授权

US5691062A Molecularly bonded inherently conductive polymers on substrates and shaped articles thereof 失效
标题翻译：分子结合的固有导电聚合物在基材和其成型制品上
公开(公告)号：US5691062A
公开(公告)日：1997-11-25
申请号：US390066
申请日：1995-02-16
申请人： Shalaby W. Shalaby , Richard V. Gregory , Jacqueline M. Allan
发明人： Shalaby W. Shalaby , Richard V. Gregory , Jacqueline M. Allan
IPC分类号： C08G61/12 , C08J7/04 , C08J7/12 , C23C14/20 , B32B9/04
CPC分类号： C08J7/047 , C08G61/124 , C08J7/12 , C23C14/20 , C08J2323/02 , C08J2465/00 , Y10T428/31504 , Y10T428/31533 , Y10T428/31536 , Y10T428/31551 , Y10T428/31609 , Y10T428/31678 , Y10T428/31692 , Y10T428/31725 , Y10T428/31786 , Y10T428/31935
摘要： Organic inherently conductive polymers, such as those based on polyaniline, polypyrrole and polythiophene, are formed in-situ onto polymeric surfaces that are chemically activated to bond ionically the conductive polymers to the substrates. The polymeric substrate is preferably a preshaped or preformed thermoplastic film, fabric, or tube, although other forms of thermoplastic and thermoset polymers can be used as the substrates for pretreatment using, most preferably, phosphonylation-based processes followed by exposure to an oxidatively polymerizable compound capable of forming an electrically conductive polymer. The resultant conductive surface imparts unique properties to the substrates and allows their use in antistatic clothing, surface conducting films for electronic components and the like, and electromagnetic interference shielding.
摘要翻译：有机固有导电聚合物，例如基于聚苯胺，聚吡咯和聚噻吩的聚合物原位形成在化学活化的聚合物表面上，以将导电聚合物离子地键合到基底上。聚合物基材优选为预成型或预成型的热塑性薄膜，织物或管，尽管其它形式的热塑性和热固性聚合物可用作预处理的底物，最优选基于膦酰基化的方法，随后暴露于氧化可聚合化合物能够形成导电聚合物。所得到的导电表面赋予基底独特的性能，并且允许它们用于抗静电服装，用于电子部件的表面导电膜等以及电磁干扰屏蔽。

3. 发明授权

US5849415A Molecularly bonded inherently conductive polymers on substrates and shaped articles thereof 失效
标题翻译：分子结合的固有导电聚合物在基材和其成型制品上
公开(公告)号：US5849415A
公开(公告)日：1998-12-15
申请号：US687641
申请日：1996-07-26
申请人： Shalaby W. Shalaby , Richard V. Gregory , Jacqueline M. Allan
发明人： Shalaby W. Shalaby , Richard V. Gregory , Jacqueline M. Allan
IPC分类号： C08G61/12 , C08J7/04 , C08J7/12 , C23C14/20 , B32B27/06
CPC分类号： C08J7/047 , C08G61/124 , C08J7/12 , C23C14/20 , C08J2323/02 , C08J2465/00 , Y10T428/31504 , Y10T428/31533 , Y10T428/31536 , Y10T428/31551 , Y10T428/31609 , Y10T428/31678 , Y10T428/31692 , Y10T428/31725 , Y10T428/31786 , Y10T428/31935
摘要： Organic inherently conductive polymers, such as those based on polyaniline, polypyrrole and polythiophene, are formed in-situ onto polymeric surfaces that are chemically activated to bond ionically the conductive polymers to the substrates. The polymeric substrate is preferably a preshaped or preformed thermoplastic film, fabric, or tube, although other forms of thermoplastic and thermoset polymers can be used as the substrates for pretreatment using, most preferably, phosphonylation-based processes followed by exposure to an oxidatively polymerizable compound capable of forming an electrically conductive polymer. The resultant conductive surface imparts unique properties to the substrates and allows their use in antistatic clothing, surface conducting films for electronic components and the like, and electromagnetic interference shielding. In an alternative embodiment, metals such as gold or platinum are bonded to the chemically interactive surface of a preshaped thermoplastic or thermoset article.
摘要翻译：有机固有导电聚合物，例如基于聚苯胺，聚吡咯和聚噻吩的聚合物原位形成在化学活化的聚合物表面上，以将导电聚合物离子地键合到基底上。聚合物基材优选为预成型或预成型的热塑性薄膜，织物或管，尽管其它形式的热塑性和热固性聚合物可用作预处理的底物，最优选基于膦酰基化的方法，随后暴露于氧化可聚合化合物能够形成导电聚合物。所得到的导电表面赋予基底独特的性能，并且允许它们用于抗静电服装，用于电子部件的表面导电膜等以及电磁干扰屏蔽。在替代实施例中，诸如金或铂的金属结合到预成型的热塑性塑料或热固性制品的化学相互作用的表面上。

4. 发明授权

US6117554A Modulated molecularly bonded inherently conductive polymers on substrates with conjugated multiple lamellae and shaped articles thereof 失效
标题翻译：在具有共轭多层片及其成型制品的基底上调制分子结合的固有导电聚合物
公开(公告)号：US6117554A
公开(公告)日：2000-09-12
申请号：US862945
申请日：1997-05-30
申请人： Shalaby W. Shalaby , Jacqueline M. Allan
发明人： Shalaby W. Shalaby , Jacqueline M. Allan
IPC分类号： C08G61/12 , C08J7/12 , C08J7/16 , C23C28/00 , B32B31/06 , B05D3/00 , B05D3/04 , B32B15/04
CPC分类号： C23C28/00 , C08G61/122 , C08G61/124 , C08J7/12 , C08J7/16
摘要： Organic inherently conductive polymers, such as those based on polyaniline, polypyrrole and polythiophene, are sequentially formed in-situ onto polymeric surfaces that are chemically functionalized to molecularly bond the conductive polymers to the substrates. The polymeric substrate is preferably a preshaped or preformed thermoplastic film, fabric, or tube, although other forms of thermoplastic and thermoset polymers can be used as the substrates for functionalization using, most preferably, phosphonylation-based processes followed by exposure to an oxidatively polymerizable compound capable of forming an electrically conductive polymer. It has been found that the degree of electrical conductivity may be modulated by bonding further electrically conductive layers to the article. That is, each underlying conductive layer is functionalized prior to bonding of a subsequent conductive layer thereto until the degree of conductivity is achieved. In an alternative embodiment, metals such as gold or platinum may be bonded to one of the functionalized surfaces.
摘要翻译：有机固有导电聚合物，例如基于聚苯胺，聚吡咯和聚噻吩的固体导电聚合物，原位地依次形成在化学官能化以将导电聚合物分子结合到基底上的聚合物表面上。聚合物基材优选为预成型或预成型的热塑性薄膜，织物或管，尽管其它形式的热塑性和热固性聚合物可用作官能化底物，最优选使用基于膦酰基化的方法，随后暴露于氧化可聚合化合物能够形成导电聚合物。已经发现，可以通过将另外的导电层粘合到制品上来调节导电性的程度。也就是说，每个下面的导电层在其后面的导电层结合之前被功能化，直到达到导电度。在替代实施例中，诸如金或铂的金属可以结合到功能化表面之一。

5. 发明授权

US5986050A Peracylated proteins and synthetic polypeptides and process for making the same 失效
标题翻译：过酰化蛋白质和合成多肽及其制备方法
公开(公告)号：US5986050A
公开(公告)日：1999-11-16
申请号：US996366
申请日：1997-12-22
申请人： Shalaby W. Shalaby , Jacqueline M. Allan , Joel T. Corbett
发明人： Shalaby W. Shalaby , Jacqueline M. Allan , Joel T. Corbett
IPC分类号： C07K1/113 , C07K14/415 , C07K1/00 , A61K35/78
CPC分类号： C07K14/415 , C07K1/113 , Y10T428/29 , Y10T428/2913 , Y10T428/2915
摘要： A method for modifying a protein or polypeptide is disclosed which includes the steps of dispersing a protein or polypeptide in an essentially non-aqueous medium and peracylating the protein or polypeptide with a cyclic anhydride having a carbon chain substituent selected from the group consisting of alkyl and alkenyl groups. Most preferably, the cyclic anhydride is succinic anhydride, although glutaric anhydride may also be employed. Preferably, the step of peracylating the protein or polypeptide is performed in the presence of an acid catalyst, most preferably .rho.-toluene sulfonic acid. The resultant modified protein or polypeptide may be employed in numerous applications including drug delivery, absorbable sutures, and thermoplastic films and molded articles.
摘要翻译：公开了一种修饰蛋白质或多肽的方法，其包括以下步骤：将蛋白质或多肽分散在基本上非水性的培养基中，并将所述蛋白质或多肽与具有选自以下的碳链取代基的环酸酐进行过酰化：烷基和烯基。最优选地，环状酸酐是琥珀酸酐，尽管也可以使用戊二酸酐。优选地，在酰基化蛋白质或多肽的步骤在酸催化剂，最优选Rho-甲苯磺酸的存在下进行。所得到的修饰的蛋白质或多肽可用于许多应用，包括药物递送，可吸收缝合线，以及热塑性薄膜和模塑制品。

6. 发明授权

US6162895A Peracylated insulin compositions and process for making the same 有权
标题翻译：过酰基化胰岛素组合物及其制备方法
公开(公告)号：US6162895A
公开(公告)日：2000-12-19
申请号：US392416
申请日：1999-09-09
申请人： Shalaby W. Shalaby , Jacqueline M. Allan , Joel T. Corbett
发明人： Shalaby W. Shalaby , Jacqueline M. Allan , Joel T. Corbett
IPC分类号： C07K1/113 , C07K14/415 , C07K1/00 , A61K35/78
CPC分类号： C07K14/415 , C07K1/113 , Y10T428/29 , Y10T428/2913 , Y10T428/2915
摘要： A method for modifying a protein or polypeptide is disclosed which includes the steps of dispersing a protein or polypeptide in an essentially non-aqueous medium and peracylating the protein or polypeptide with a cyclic anhydride having a carbon chain substituent selected from the group consisting of alkyl and alkenyl groups. Most preferably, the cyclic anhydride is succinic anhydride, although glutaric anhydride may also be employed. Preferably, the step of peracylating the protein or polypeptide is performed in the presence of an acid catalyst, most preferably .rho.-toluene sulfonic acid. The resultant modified protein or polypeptide may be employed in numerous applications including drug delivery, absorbable sutures, and thermoplastic films and molded articles.
摘要翻译：公开了一种修饰蛋白质或多肽的方法，其包括以下步骤：将蛋白质或多肽分散在基本上非水性的培养基中，并将所述蛋白质或多肽与具有选自以下的碳链取代基的环酸酐进行过酰化：烷基和烯基。最优选地，环状酸酐是琥珀酸酐，尽管也可以使用戊二酸酐。优选地，在酰基化蛋白质或多肽的步骤在酸催化剂，最优选Rho-甲苯磺酸的存在下进行。所得到的修饰的蛋白质或多肽可用于许多应用，包括药物递送，可吸收缝合线，以及热塑性薄膜和模塑制品。

7. 发明授权

US06254986B1 Peracylated protein-based sutures and fabrics and process for making the same 有权
标题翻译：过基因蛋白质的缝合线和织物以及制造相同的方法
公开(公告)号：US06254986B1
公开(公告)日：2001-07-03
申请号：US09593859
申请日：2000-06-14
申请人： Shalaby W. Shalaby , Jacqueline M. Allan , Joel T. Corbett
发明人： Shalaby W. Shalaby , Jacqueline M. Allan , Joel T. Corbett
IPC分类号： D02G300
CPC分类号： C07K14/415 , C07K1/113 , Y10T428/29 , Y10T428/2913 , Y10T428/2915
摘要： A method for modifying a protein or polypeptide is disclosed which includes the steps of dispersing a protein or polypeptide in an essentially non-aqueous medium and peracylating the protein or polypeptide with a cyclic anhydride having a carbon chain substituent selected from the group consisting of alkyl and alkenyl groups. Most preferably, the cyclic anhydride is succinic anhydride, although glutaric anhydride may also be employed. Preferably, the step of peracylating the protein or polypeptide is performed in the presence of an acid catalyst, most preferably &rgr;-toluene sulfonic acid. The resultant modified protein or polypeptide may be employed in numerous applications including drug delivery, absorbable sutures, and thermoplastic films and molded articles.
摘要翻译：公开了一种修饰蛋白质或多肽的方法，其包括以下步骤：将蛋白质或多肽分散在基本上非水性的培养基中，并将所述蛋白质或多肽与具有选自以下的碳链取代基的环酸酐进行过酰化：烷基和烯基。最优选地，环状酸酐是琥珀酸酐，尽管也可以使用戊二酸酐。优选地，在酰基化蛋白质或多肽的步骤在酸催化剂，最优选的是对甲苯磺酸的存在下进行。所得到的修饰的蛋白质或多肽可用于许多应用，包括药物递送，可吸收缝合线，以及热塑性薄膜和模塑制品。

8. 发明授权

US5529736A Process of making a bone healing device 失效
标题翻译：制造骨愈合装置的过程
公开(公告)号：US5529736A
公开(公告)日：1996-06-25
申请号：US288343
申请日：1994-08-10
申请人： Shalaby W. Shalaby , Russell A. Johnson , Meng Deng
发明人： Shalaby W. Shalaby , Russell A. Johnson , Meng Deng
IPC分类号： A61B17/00 , A61B17/68 , B29C43/00 , B29C43/02 , B29C43/16 , B29C70/04 , B29C70/06 , B29C43/36
CPC分类号： B29C43/02 , A61B17/68 , B29C43/003 , B29C43/16 , B29C70/04 , B29C70/06 , A61B2017/00004 , B29C2791/001 , B29K2067/00 , B29K2067/04 , B29K2067/043 , B29K2067/046 , B29K2101/12 , B29K2995/0041 , B29K2995/0051 , B29K2995/006 , B29L2031/753 , B29L2031/7546
摘要： The present invention is directed to polymeric bone fixation devices and processes for making the devices. In making the bone fixation devices, a polymeric material having a crystalline portion is deformed by a compressive force along a particular direction which causes molecular chains contained within the polymer to orient. The resulting polymer has increased mechanical properties including increased tensile strength and modulus. The polymeric material used to make the bone fixation device can be a bioabsorbable polymer which, once implanted, is broken down and absorbed by the patient's body, eliminating the need for removal.
摘要翻译：本发明涉及聚合物骨固定装置及其制造方法。在制造骨固定装置时，具有结晶部分的聚合材料通过沿着特定方向的压缩力而变形，这导致包含在聚合物内的分子链取向。所得聚合物具有增加的机械性能，包括增加的拉伸强度和模量。用于制造骨固定装置的聚合物材料可以是生物可吸收的聚合物，其一旦被植入就被细胞分解并被患者的身体吸收，就不需要去除。

9. 发明授权

US5834113A Self-reinforced ultra-high molecular weight polyethylene composite medical implants 失效
标题翻译：自增强超高分子量聚乙烯复合医用植入物
公开(公告)号：US5834113A
公开(公告)日：1998-11-10
申请号：US472404
申请日：1995-06-07
申请人： Shalaby W. Shalaby , Meng Deng
发明人： Shalaby W. Shalaby , Meng Deng
IPC分类号： A61L27/48 , A61L31/12 , B29C67/24 , B29C70/04 , B29C70/06 , B29C70/46 , B29C70/50 , C08L23/06 , D02G3/00 , A61F2/30
CPC分类号： C08L23/06 , A61L27/48 , A61L31/129 , B29C67/24 , B29C70/04 , B29C70/06 , B29C70/465 , B29C70/50 , B29K2023/0683 , B29K2105/101 , B29K2105/24 , B29L2031/7532 , C08L2203/02 , C08L2205/02 , C08L2205/16 , Y10S428/902 , Y10T428/2913 , Y10T428/2929 , Y10T428/2973 , Y10T428/31855
摘要： The invention provides composites of ultra-high molecular weight polyethylene reinforced with ultra-high molecular weight polyethylene anisotropic reinforcement of high strength and modulus. The composites have superior mechanical properties relative to non-filled ultra-high molecular weight polyethylene, including higher strength, impact strength, increased creep resistance, and improved modulus. The composites may be sterilized for biomedical use, using gamma radiation and other techniques. Further, the composites are resistant to the effect of body fluids and have lower creep rates so that they will provide implant life. The composites may be cross-linked by exposure to an acetylene environment. Also, the composites find use in other high strength, high impact applications such as sports equipment.
摘要翻译：本发明提供了具有高强度和模量的超高分子量聚乙烯各向异性增强材料的超高分子量聚乙烯复合材料。复合材料相对于未填充的超高分子量聚乙烯具有优异的机械性能，包括较高的强度，冲击强度，增加的抗蠕变性和改善的模量。可以使用γ辐射和其他技术将复合材料灭菌用于生物医学应用。此外，复合材料抵抗体液的作用，具有较低的蠕变速率，因此它们将提供植入寿命。复合材料可能通过暴露于乙炔环境而交联。此外，复合材料可用于其他高强度，高冲击应用，如运动器材。

10. 发明授权

US5824411A Self-reinforced ultra-high molecular weight polyethylene composites 失效
标题翻译：自增强超高分子量聚乙烯复合材料
公开(公告)号：US5824411A
公开(公告)日：1998-10-20
申请号：US480848
申请日：1995-06-07
申请人： Shalaby W. Shalaby , Meng Deng
发明人： Shalaby W. Shalaby , Meng Deng
IPC分类号： A61L27/48 , A61L31/12 , B29C67/24 , B29C70/04 , B29C70/06 , B29C70/46 , B29C70/50 , C08L23/06 , D02G3/32
CPC分类号： C08L23/06 , A61L27/48 , A61L31/129 , B29C67/24 , B29C70/04 , B29C70/06 , B29C70/465 , B29C70/50 , B29K2023/0683 , B29K2105/101 , B29K2105/24 , B29L2031/7532 , C08L2203/02 , C08L2205/02 , C08L2205/16 , Y10S428/902 , Y10T428/2913 , Y10T428/2929 , Y10T428/2973 , Y10T428/31855
摘要： The invention provides composites of ultra-high molecular weight polyethylene reinforced with ultra-high molecular weight polyethylene anisotropic reinforcement of high strength and modulus. The composites have superior mechanical properties relative to non-filled ultra-high molecular weight polyethylene, including higher strength, impact strength, increased creep resistance, and improved modulus. The composites may be sterilized for biomedical use, using gamma radiation and other techniques. Further, the composites are resistant to the effect of body fluids and have lower creep rates so that they will provide implant life. The composites may be cross-linked by exposure to an acetylene environment. Also, the composites find use in other high strength, high impact applications such as sports equipment.
摘要翻译：本发明提供了具有高强度和模量的超高分子量聚乙烯各向异性增强材料的超高分子量聚乙烯复合材料。复合材料相对于未填充的超高分子量聚乙烯具有优异的机械性能，包括较高的强度，冲击强度，增加的抗蠕变性和改善的模量。可以使用γ辐射和其他技术将复合材料灭菌用于生物医学应用。此外，复合材料抵抗体液的作用，具有较低的蠕变速率，因此它们将提供植入寿命。复合材料可能通过暴露于乙炔环境而交联。此外，复合材料可用于其他高强度，高冲击应用，如运动器材。

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