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1. 发明授权

US4604326A Porous regenerated cellulose hollow fiber and process for preparation thereof 失效
标题翻译：多孔再生纤维素中空纤维及其制备方法
公开(公告)号：US4604326A
公开(公告)日：1986-08-05
申请号：US604512
申请日：1984-04-27
申请人： Seiichi Manabe , Michitaka Iwata , Mamoru Inoue
发明人： Seiichi Manabe , Michitaka Iwata , Mamoru Inoue
IPC分类号： B01D71/10 , D01D5/24 , D01F1/08 , D01F2/04 , D02G3/00
CPC分类号： B01D71/10 , B01D69/08 , B01D69/087 , D01F2/04 , Y10T428/2935 , Y10T428/2975
摘要： A porous regenerated cellulose hollow fiber obtained by a micro-phase-separation method is described. The hollow fiber is characterized in that the viscosity average molecular weight is at least 5.times.10.sup.4, each of the average pore diameter D.sub.1 on the inner wall surface of the hollow fiber and the average pore diameter D.sub.2 on the outer wall surface is 0.02 to 10 .mu.m, the in-plane porosity Pr on the outer wall surface is at least 10%, and the hollow fiber comprises a wall thickness portion having pores piercing therethrough between the inner wall surface and outer wall surface and a hollow portion extending continuously over the entire fiber length. The hollow fiber is prepared by a process characterized in that at the steps of extruding a cuprammonium solution of a cellulose from an annular spinning orifice and coagulating, regenerating and water-washing the extrudate, the spinning solution is extruded from an outer annular spinning orifice and a liquid having a coagulating action to the spinning solution is extruded from a central spinning orifice, and micro-phase-separation is caused to occur before the coagulation.
摘要翻译：描述通过微相分离方法获得的多孔再生纤维素中空纤维。中空纤维的特征在于，中空纤维的内壁面上的平均孔径D1和外壁面的平均孔径D2的粘均分子量为至少5×10 4，为0.02〜10μm 外壁表面上的面内孔隙率Pr至少为10％，中空纤维包括在内壁表面和外壁表面之间具有穿孔的壁厚部分和在整个纤维上连续延伸的中空部分长度。中空纤维是通过以下方法制备的，其特征在于在从环形纺丝口挤出纤维素的铜铵溶液并使挤出物凝结，再生和水洗的步骤中，纺丝溶液从外环形纺丝孔挤出，从中心纺丝口挤出对纺丝溶液具有凝结作用的液体，在凝固前发生微相分离。

2. 发明授权

US4822540A Process for the preparation of a porous regenerated cellulose hollow fiber 失效
标题翻译：制备多孔再生纤维素中空纤维的方法
公开(公告)号：US4822540A
公开(公告)日：1989-04-18
申请号：US867228
申请日：1986-05-27
申请人： Seiichi Manabe , Michitaka Iwata , Mamoru Inoue
发明人： Seiichi Manabe , Michitaka Iwata , Mamoru Inoue
IPC分类号： B01D71/10 , D01D5/24 , D01F1/08 , D01F2/04 , D01D5/247
CPC分类号： B01D71/10 , B01D69/08 , B01D69/087 , D01F2/04 , Y10T428/2935 , Y10T428/2975
摘要： A porous regenerated cellulose hollow fiber is obtained by a micro-phase-separation method. The hollow fiber is characterized in that the viscosity average molecular weight is at least 5.times.10.sup.4, each of the average pore diameter D.sub.1 on the inner wall surface of the hollow fiber and the average pore diameter D.sub.2 on the outer wall surface is 0.02 to 10 .mu.m, the in-plane porosity Pr on the outer wall surface is at least 10%, and the hollow fiber comprises a wall thickness portion having pores piercing therethrough between the inner wall surface and outer wall surface and a hollow portion extending continuously over the entire fiber length. The hollow fiber is prepared by a process characterized in that at the steps of extruding a cuprammonium solution of a cellulose from an annular spinning orifice and coagulating, regenerating and water-washing the extrudate, the spinning solution is extruded from an outer annular spinning orifice and a liquid having a coagulating action to the spinning solution is extruded from a central spinning orifice, and micro-phase-separation is caused to occur before the coagulation.

3. 发明授权

US4581140A Porous regenerated cellulose membrane and process for the preparation thereof 失效
标题翻译：多孔再生纤维素膜及其制备方法
公开(公告)号：US4581140A
公开(公告)日：1986-04-08
申请号：US443074
申请日：1982-11-19
申请人： Seiichi Manabe , Michitaka Iwata , Mamoru Inoue
发明人： Seiichi Manabe , Michitaka Iwata , Mamoru Inoue
IPC分类号： B01D71/10 , C08L1/06 , B01D13/00
CPC分类号： B01D71/10 , C08L1/06
摘要： A porous regenerated cellulose membrane consisting essentially of cellulose molecules having a viscosity average molecular weight of at least about 5.times.10.sup.4, the crystalline region of the cellulose molecules being substantially cellulose II crystal, cellulose III-2 crystal or the mixture thereof and having a degree of crystal orientation at a face of (101) in the crystalline region in the direction of the surface of the membrane of at most about 40%, the membrane having a dynamic modulus at 30.degree. C. measured with a frequency of 110 Hz of at least about 1.5.times.10.sup.8 (100-pr.rho.) dyn/cm.sup.2 wherein Pr.rho. is a porosity by percentage, a mean pore size represented by D(.mu.m) of about 0.01 .mu.m to about 20 .mu.m and at the same time a porosity in a plane of at least one plane of at least about 30% or a number of pores in a plane per 1 cm.sup.2 of about 6.times.10.sup.5 /D to about 3.times.10.sup.7 /D; and a process for preparing the same.
摘要翻译：基本上由粘均分子量为至少约5×10 4的纤维素分子组成的多孔再生纤维素膜，纤维素分子的结晶区域基本上是纤维素II晶体，纤维素III-2晶体或其混合物，并且具有一定程度的结晶在膜表面方向的结晶区域的（101）面的取向至多约为40％，膜的动态模量在30℃下以110Hz的频率测量为至少约 1.5×10 8（100-pr rho）dyn / cm 2，其中Pr rho是以百分比表示的孔隙率，由D（μm）表示的平均孔径为约0.01μm至约20μm，同时在至少一个平面的平面为至少约30％或每平方厘米约1×10 5 / D至约3×10 7 / D的平面中的孔数; 及其制备方法。

4. 发明授权

US4426516A Polyester fiber dyeable under normal pressure 失效
标题翻译：聚酯纤维在常压下可染色
公开(公告)号：US4426516A
公开(公告)日：1984-01-17
申请号：US363628
申请日：1982-03-30
申请人： Tomio Kuriki , Seiichi Manabe
发明人： Tomio Kuriki , Seiichi Manabe
IPC分类号： D01F6/62 , D01D5/098 , C08G63/70
CPC分类号： D01F6/62 , D01D5/098
摘要： A fiber consisting essentially of polyethylene terephthalate capable of being dyed under normal pressure and having an initial modulus at 30.degree. C. of about 55 g/d to about 130 g/d, a relationship between a peak temperature ]T.sub.max (.degree.C.)] at the peak of a dynamic mechanical loss tangent (tan .delta.) measured with a frequency of 110 Hz and a peak value of the dynamic mechanical loss tangent [(tan .delta.).sub.max ] represented by the formula:(tan .delta.).sub.max .ltoreq.1.times.10.sup.-2 (T.sub.max -105)and a (tan .delta.).sub.max of about 0.14 to about 0.30 and a dynamic mechanical loss tangent at 220.degree. C. (tan .delta..sub.220) of at most about 0.055. The fiber is produced by subjecting a polyethylene terephthalate fiber obtained at a spinning speed of at least about 4000 m/min. to heat treatment at a temperature ranging from a temperature at which a dynamic modulus (E') of the fiber deviates from a tangent line at 180.degree. C. of a logarithm of the E' of the fiber-temperature curve (T.sub.min) plus 10.degree. C. to a temperature of completion of melting (T.sub.m.sbsb.3) at a melting curve of the fiber measured by a differential scanning calorimeter (DSC) plus 10.degree. C.
摘要翻译：基本上由聚对苯二甲酸乙二醇酯组成的纤维，其能够在常压下染色，在30℃下的初始模量为约55g / d至约130g / d，峰值温度Tmax（℃） ]在以110Hz的频率测量的动态机械损耗角正切（tanδ）的峰值处，以及由下式表示的动态机械损耗角正切[（tanδ）max]的峰值：（tanδ）max < = 1×10 -2（T max-105）和（tanδ）max为约0.14至约0.30，并且在220℃下的动态机械损耗角正切（tanδ220）为至多约0.055。该纤维是通过以至少约4000m /分钟的纺丝速度获得的聚对苯二甲酸乙二醇酯纤维进行生产的。在从纤维的动态弹性模量（E'）与180℃的切线偏离的温度相对于纤维 - 温度曲线的E'的对数（Tmin）加上10的温度下进行热处理通过差示扫描量热计（DSC）加10℃在纤维的熔解曲线下达到熔融完成温度（Tm3）。

5. 发明授权

US4419317A Process for the preparation of fibers of poly-p-phenylene-terephthalamide 失效
标题翻译：制备聚对苯二甲酰对苯二胺纤维的方法
公开(公告)号：US4419317A
公开(公告)日：1983-12-06
申请号：US380781
申请日：1982-05-21
申请人： Takashi Fujiwara , Shuji Kajita , Tetsuo Matsushita , Seiichi Manabe
发明人： Takashi Fujiwara , Shuji Kajita , Tetsuo Matsushita , Seiichi Manabe
IPC分类号： B60C9/00 , D01F6/60 , D02G3/02 , D02G3/48 , D01D5/12
CPC分类号： B60C9/0042 , D01F6/605 , D02G3/02 , D02G3/48 , D10B2331/021
摘要： A poly-p-phenylene-terephthalamide fiber with excellent fatigue resistance resulting from a unique combination of properties. The fibers are prepared by extruding an anisotropic polymer dope in a non-coagulating layer, passing the extrudate through a coagulating layer, depositing the resulting coagulated fibers on a net conveyor, and in the absence of substantial tension sequentially washing the fibers, holding the fibers in saturated steam, and drying the fibers under specified conditions.
摘要翻译：聚对苯二甲酰对苯二胺纤维具有优异的耐疲劳性，由特性组合而成。纤维通过在非凝固层中挤出各向异性聚合物涂料，使挤出物通过凝结层，将所得凝结纤维沉积在网状输送机上，并且在没有显着张力的情况下依次洗涤纤维，保持纤维在饱和蒸汽中，并在特定条件下干燥纤维。

6. 发明授权

US4374977A Poly-p-phenylene-terephthalamide fibers excellent in fatigue resistance and process for preparation thereof 失效
标题翻译：耐疲劳性优异的聚对苯二甲酰对苯二胺纤维及其制备方法
公开(公告)号：US4374977A
公开(公告)日：1983-02-22
申请号：US129403
申请日：1980-03-11
申请人： Takashi Fujiwara , Shuji Kajita , Tetsuo Matsushita , Seiichi Manabe
发明人： Takashi Fujiwara , Shuji Kajita , Tetsuo Matsushita , Seiichi Manabe
IPC分类号： B60C9/00 , D01F6/60 , D02G3/02 , D02G3/48 , C08G69/46
CPC分类号： B60C9/0042 , D01F6/605 , D02G3/02 , D02G3/48 , D10B2331/021
摘要： A poly-p-phenylene-terephthalamide fiber with excellent fatigue resistance resulting from a unique combination of properties. The fibers are prepared by extruding an anisotropic polymer dope in a non-coagulating layer, passing the extrudate through a coagulating layer, depositing the resulting coagulated fibers on a net conveyor, and in the absence of substantial tension sequentially washing the fibers, holding the fibers in saturated steam, and drying the fibers under specified conditions.
摘要翻译：聚对苯二甲酰对苯二胺纤维具有优异的耐疲劳性，由特性组合而成。纤维通过在非凝固层中挤出各向异性聚合物涂料，使挤出物通过凝结层，将所得凝结纤维沉积在网状输送机上，并且在没有显着张力的情况下依次洗涤纤维，保持纤维在饱和蒸汽中，并在特定条件下干燥纤维。

7. 发明授权

US5185082A Method for evaluating the virus-removing capability of a porous polymeric membrane module for removing viruses 失效
标题翻译：评估用于去除病毒的多孔聚合物膜模块的病毒去除能力的方法
公开(公告)号：US5185082A
公开(公告)日：1993-02-09
申请号：US894544
申请日：1992-06-05
申请人： Hiroo Nakano , Seiichi Manabe
发明人： Hiroo Nakano , Seiichi Manabe
IPC分类号： A61L2/02 , B01D65/10
CPC分类号： B01D65/102 , A61L2/022 , B01D65/104
摘要： Disclosed is a method for the evaluation of the virus-removing capability of a porous polymeric membrane module for removing viruses by filtration, which comprises testing I in which a transmembrane pressure lowering from predetermined value Ph a predetermined period of time after the termination of the supply of a gas is measured with respect to the porous polymeric membrane module, wherein the value Ph satisfies the formula: d

8. 发明授权

US4717480A Method for separation of liquid mixture 失效
标题翻译：液体混合物分离方法
公开(公告)号：US4717480A
公开(公告)日：1988-01-05
申请号：US842838
申请日：1986-03-24
申请人： Takaharu Akedo , Seiichi Manabe
发明人： Takaharu Akedo , Seiichi Manabe
IPC分类号： B01D11/04 , B01D17/00 , B01D19/00 , B01D61/16 , B01D61/42 , C07C29/76
CPC分类号： B01D61/425 , B01D11/0415 , B01D11/0419 , B01D17/00 , B01D19/0031 , B01D19/0073 , C07C29/76
摘要： A method for separation of a liquid mixture wherein a component, intended to be separated, in the liquid mixture is concentrated in the interiors of particles having an average size of 0.1 to 10 .mu.m; the particles are then transported to the surface of a polymeric porous membrane having an average pore size 0.1 to 50 times the average size of the particles under an electrostatic field; and the particles are then separated by a pressure difference loaded on the membrane.
摘要翻译：一种液体混合物的分离方法，其中待分离的组分在液体混合物中浓缩在平均尺寸为0.1至10μm的颗粒的内部; 然后将颗粒输送到在静电场下具有颗粒平均尺寸的平均孔径0.1至50倍的聚合物多孔膜的表面; 然后通过加载在膜上的压差来分离颗粒。

9. 发明授权

US4440710A Process for the preparation of high Young's modulus poly-p-phenylene-terephthalamide 失效
标题翻译：制备高杨氏模量聚对苯二甲酰对苯二胺的方法
公开(公告)号：US4440710A
公开(公告)日：1984-04-03
申请号：US406043
申请日：1982-08-06
申请人： Takashi Fujiwara , Shuji Kajita , Tetsuo Matsushita , Seiichi Manabe
发明人： Takashi Fujiwara , Shuji Kajita , Tetsuo Matsushita , Seiichi Manabe
IPC分类号： B29C70/04 , D01F6/60 , D01D5/12
CPC分类号： D01F6/605
摘要： A high Young's modulus poly-p-phenylene-terephthalamide fiber having a unique fine-structure and excellent properties, including excellent resistance to lateral stress and to friction. The fiber is made by extruding an anisotropic dope in a non-coagulating layer, passing the extrudate through a coagulating layer, washing and drying the resulting coagulated fibers in the absence of substantial tension, and heating the fibers under tension.
摘要翻译：具有独特精细结构和优异性能的高杨氏模量聚对苯二甲酰亚胺纤维，包括优异的抗横向应力和摩擦性。纤维通过在非凝固层中挤出各向异性涂料而制成，使挤出物通过凝固层，在没有显着张力的情况下洗涤和干燥所得到的凝固纤维，并在张力下加热纤维。

10. 发明授权

US4374978A High Young's modulus poly-p-phenylene terephthalamide fiber 失效
标题翻译：高杨氏模量聚对苯二甲酰对苯二胺纤维
公开(公告)号：US4374978A
公开(公告)日：1983-02-22
申请号：US129404
申请日：1980-03-11
申请人： Takashi Fujiwara , Shuji Kajita , Tetsuo Matsushita , Seiichi Manabe
发明人： Takashi Fujiwara , Shuji Kajita , Tetsuo Matsushita , Seiichi Manabe
IPC分类号： B29C70/04 , D01F6/60 , C08G69/46
CPC分类号： D01F6/605
摘要： A high Young's modulus poly-p-phenylene-terephthalamide fiber having a unique fine-structure and excellent properties, including excellent resistance to lateral stress and to friction. The fiber is made by extruding an anisotropic dope in a non-coagulating layer, passing the extrudate through a coagulating layer, washing and drying the resulting coagulated fibers in the absence of substantial tension, and heating the fibers under tension.
摘要翻译：具有独特精细结构和优异性能的高杨氏模量聚对苯二甲酰亚胺纤维，包括优异的抗横向应力和摩擦性。纤维通过在非凝固层中挤出各向异性涂料而制成，使挤出物通过凝固层，在没有显着张力的情况下洗涤和干燥所得到的凝固纤维，并在张力下加热纤维。

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