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1. 发明授权

US06232027B1 Toner having negative triboelectric chargeability and image forming method 有权
标题翻译：具有负摩擦带电性和图像形成方法的调色剂
公开(公告)号：US06232027B1
公开(公告)日：2001-05-15
申请号：US09318776
申请日：1999-05-26
申请人： Satoshi Matsunaga , Toshiaki Nakahara , Yuichi Mizoh , Hirohide Tanikawa , Minekazu Endo , Tadashi Doujo , Nene Shibayama
发明人： Satoshi Matsunaga , Toshiaki Nakahara , Yuichi Mizoh , Hirohide Tanikawa , Minekazu Endo , Tadashi Doujo , Nene Shibayama
IPC分类号： G03G9087
CPC分类号： G03G9/09783 , G03G9/08755 , G03G9/08782 , G03G9/08793 , G03G9/09741 , G03G9/0975
摘要： A toner having a negative triboelectric chargeability is constituted by at least a binder resin, a colorant and an organic metal compound. The toner is characterized by: (a) the organic metal compound is an organic zirconium compound comprising a coordination or/and a bonding of zirconium and an aromatic compound as a ligand or/and an acid source selected from the group consisting of aromatic diols, aromatic hydroxycarboxylic acids, aromatic monocarboxylic acids, and aromatic polycarboxylic acids, (b) the binder resin is a resin selected from the group consisting of (i) a polyester resin and (ii) a hybrid resin component comprising a polyester unit and a vinyl polymer unit, (c) the binder resin has an acid value of 2-50 mgKOH/g, and (d) the toner contains a TFT (tetrahydrofuran)-soluble content providing a GPC (gel permeation chromatography) chromatogram exhibiting a main peak in a molecular weight range of 3,000-20,000 and including 3-25% of a component having molecular weights of at least 5×105.
摘要翻译：具有负摩擦带电性的调色剂至少由粘合剂树脂，着色剂和有机金属化合物构成。调色剂的特征在于：（a）有机金属化合物是一种有机锆化合物，其包含锆和作为配体的芳族化合物的配位或/和键合，和/或选自芳族二醇，（b）粘合剂树脂是选自（i）聚酯树脂和（ii）包含聚酯单元和乙烯基聚合物的杂化树脂组分的树脂中的一种树脂单元，（c）粘合剂树脂的酸值为2-50mgKOH / g，（d）调色剂含有提供GPC（凝胶渗透色谱）色谱的TFT（四氢呋喃） - 可溶性含量，分子量范围为3,000-20,000，并且包括3-25％的分子量至少为5×10 5的成分。

2. 发明授权

US5976752A Toner and image forming method 有权
标题翻译：调色剂和成像方法
公开(公告)号：US5976752A
公开(公告)日：1999-11-02
申请号：US135167
申请日：1998-08-18
申请人： Satoshi Matsunaga , Koichi Tomiyama , Yuichi Mizoh , Keita Nozawa , Minekazu Endo , Tadashi Doujo , Yoshihiro Ogawa , Nene Shibayama
发明人： Satoshi Matsunaga , Koichi Tomiyama , Yuichi Mizoh , Keita Nozawa , Minekazu Endo , Tadashi Doujo , Yoshihiro Ogawa , Nene Shibayama
IPC分类号： G03G9/087 , G03G9/097 , G03G13/22
CPC分类号： G03G9/08755 , G03G9/087 , G03G9/08702 , G03G9/08711 , G03G9/08728 , G03G9/08797
摘要： An electrophotographic toner is composed of at least a binder resin, a colorant, and a wax. The binder resin (a) comprises a polyester resin, a vinyl resin and a hybrid resin component comprising a polyester unit and a vinyl polymer unit, (b) has a THF (tetrahydrofuran)-soluble content (W1) of 50-85 wt. % and a THF-insoluble content (W2) of 5-50 wt. %, an ethyl acetate-soluble content (W3) of 40-98 wt. % and an ethyl acetate-insoluble content (W4) of 2-60 wt. %, a chloroform-soluble content (W5) of 55-90 wt. % and a chloroform-insoluble content (W6) of 10-45 wt. %, respectively after 10 hours of Soxhlet extraction with respective solvents, giving a ratio W4/S6 of 1.1-4.0, and contains a THF-soluble content providing a GPC (gel permeation chromatography) chromatogram exhibiting a main peak in a molecular weight range of 4000-9000, including 35.0-65.0% (A1) of a component haing molecular weights in a range of 500 to below 1.times.10.sup.4, 25.0-45.0% (A2) of a component having molecular weights in a range of 1.times.10.sup.4 to below 1.times.10.sup.5 and 10.0-30.0% (A3) of a component having molecular weights of at least 1.times.10.sup.5 giving a ratio A1/A2 of 1.05-2.00. The binder resin shows good dispersibility of wax and colorant.
摘要翻译：电子照相调色剂由至少粘合剂树脂，着色剂和蜡组成。粘合剂树脂（a）包括聚酯树脂，乙烯基树脂和包含聚酯单元和乙烯基聚合物单元的混合树脂组分，（b）具有50-85重量％的THF（四氢呋喃） - 可溶成分（W1）％和THF不溶物含量（W2）为5-50wt。％，40-98重量％的乙酸乙酯可溶物含量（W3）％，乙酸乙酯不溶物含量（W4）为2-60wt。％，55-90重量％的氯仿可溶物含量（W5）％，氯仿不溶物含量（W6）为10-45wt。％，分别用各自的溶剂提取索氏提取10小时后，得到比例W4 / S6为1.1-4.0，并含有THF可溶性成分，提供在分子量范围内显示主峰的GPC（凝胶渗透色谱）色谱图 4000-9000，包括分子量在500至低于1×10 4范围内的分子量为35.0-65.0％（A1），分子量为1×104至低于1×10 5的组分的25.0-45.0％（A2）和10.0 -30.0％（A3）的分子量为至少1×10 5的组分，其A1 / A2比为1.05-2.00。粘合剂树脂表现出良好的蜡和着色剂的分散性。

3. 发明授权

US06953646B2 Toner particles including a sulfur-containing resin 有权
标题翻译：包含含硫树脂的调色剂颗粒
公开(公告)号：US06953646B2
公开(公告)日：2005-10-11
申请号：US10437021
申请日：2003-05-14
申请人： Tadashi Doujo , Yuichi Mizoh , Nene Shibayama , Yusuke Hasegawa
发明人： Tadashi Doujo , Yuichi Mizoh , Nene Shibayama , Yusuke Hasegawa
IPC分类号： G03G9/083 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08726 , G03G9/0833 , G03G9/08711 , G03G9/08733 , G03G9/08771 , G03G9/08773 , G03G9/08791 , G03G9/08795 , G03G9/08797 , G03G9/0902
摘要： A toner comprises toner particles comprising at least a binder resin, a colorant, and a sulfur-containing resin, in which the toner particles comprise the sulfur-containing resin so as to satisfy a relation of; 0.50≦IS/TS≦0.95 where TS denotes a content of sulfur in the toner particles, and IS denotes a content of sulfur in isopropyl alcohol insoluble components of the toner particles, whereby it is possible to obtain a high quality image having an excellent developing resistance regardless of the surrounding conditions and a uniform charge amount distribution regardless of processing speed.
摘要翻译：调色剂包括至少包含粘合剂树脂，着色剂和含硫树脂的调色剂颗粒，其中调色剂颗粒包含含硫树脂以满足以下关系： 0.50 其中T S表示调色剂颗粒中的硫含量，而I < S表示调色剂颗粒的异丙醇不溶性组分中的硫含量，由此无论处理速度如何，都可以获得具有优异显影阻力的高品质图像，而不管周围条件和均匀的电荷量分布。

4. 发明授权

US5858597A Toner for developing electrostatic image containing specified double oxide particles 失效
标题翻译：用于显影含有特定双氧化物颗粒的静电图像的调色剂
公开(公告)号：US5858597A
公开(公告)日：1999-01-12
申请号：US697877
申请日：1996-08-30
申请人： Yuichi Mizoh , Takaaki Kohtaki , Yushi Mikuriya , Tadashi Doujo
发明人： Yuichi Mizoh , Takaaki Kohtaki , Yushi Mikuriya , Tadashi Doujo
IPC分类号： G03G9/093 , G03G9/097
CPC分类号： G03G9/09385 , G03G9/09708
摘要： A toner for developing an electrostatic image is constituted by toner particles containing at least a binder resin and a colorant, and particles containing at least one double oxide. The double oxide includes a double oxide (A) represented by the following formula (1):M.sub.a Si.sub.b O.sub.c (1),wherein M denotes a metallic element selected from the group consisting of Sr, Mg, Zn, Co, Mn and Ce; a is an integer of 1-9; b is an integer of 1-9; and c is an integer of 3-9. The above particles including a double oxide (A) are effective in improving flowability and triboelectric chargeability of the toner and providing a resultant image with excellent image qualities.
摘要翻译：用于显影静电图像的调色剂由至少含有粘合剂树脂和着色剂的调色剂颗粒以及含有至少一种双氧化物的颗粒构成。双氧化物包括由下式（1）表示的双氧化物（A）：MaSibOc（1），其中M表示选自Sr，Mg，Zn，Co，Mn和Ce的金属元素; a是1-9的整数; b是1-9的整数; 且c为3-9的整数。包括双氧化物（A）的上述颗粒在改善调色剂的流动性和摩擦带电性方面是有效的，并提供具有优异图像质量的所得图像。

5. 发明授权

US5695902A Toner for developing electrostatic image, image forming method and process-cartridge 失效
标题翻译：用于显影静电图像，成像方法和处理盒的调色剂
公开(公告)号：US5695902A
公开(公告)日：1997-12-09
申请号：US749635
申请日：1996-11-15
申请人： Yushi Mikuriya , Yuichi Mizoh , Tadashi Doujo
发明人： Yushi Mikuriya , Yuichi Mizoh , Tadashi Doujo
IPC分类号： G03G9/097 , G03G13/22
CPC分类号： G03G9/09716 , G03G9/09708
摘要： A toner for developing an electrostatic image is formed as a mixture of toner particles containing at least a binder resin and a colorant, and inorganic fine powder. The inorganic fine powder includes: (A) inorganic fine powder (A) treated at least with silicone oil, and (B) inorganic fine powder (B) comprising a composite metal oxide including at least Si as a constituent element and having a weight-average particle size of 0.3-5 .mu.m. Because of the inclusion of the two types of inorganic fine powders (A) and (B), the toner is stably provided with a high flowability and a high triboelectric charge under various environmental conditions including low-humidity to high-humidity conditions. The toner is suitably used in an image forming system including a contact-charging means, a contact-transfer means and a film (or surf)-fixing system.
摘要翻译：作为静电图像显影用调色剂形成为至少含有粘合剂树脂和着色剂的调色剂颗粒和无机细粉末的混合物。无机细粉末包括：（A）至少用硅油处理的无机细粉末（A）和（B）无机细粉末（B），其包含至少包含Si作为构成元素的复合金属氧化物，平均粒径0.3-5μm。由于包含两种类型的无机细粉（A）和（B），调色剂在包括低湿度至高湿条件的各种环境条件下稳定地具有高流动性和高摩擦电荷。调色剂适用于包括接触充电装置，接触转移装置和膜（或冲洗） - 混合系统的图像形成系统。

6. 发明授权

US6040103A Toner for developing electrostatic image and image forming method 失效
标题翻译：用于显影静电图像和图像形成方法的调色剂
公开(公告)号：US6040103A
公开(公告)日：2000-03-21
申请号：US921565
申请日：1997-09-02
申请人： Manabu Ohno , Takeshi Ohtake , Satoshi Matsunaga , Tadashi Doujo
发明人： Manabu Ohno , Takeshi Ohtake , Satoshi Matsunaga , Tadashi Doujo
IPC分类号： G03G9/087 , G03G9/097 , G03G13/22
CPC分类号： G03G9/08782
摘要： A toner for developing an electrostatic image is composed of toner particles each containing at least a binder resin, a colorant, and a wax. The wax satisfies conditions of:(a) showing a maximum heat-absorption peak in a region of 50-130.degree. C. on temperature increase on a DSC (differential scanning calorimeter) curve, and(b) giving a .sup.13 C-NMR (nuclear magnetic resonance) spectrum showing a total peak area S in a range of 0-50 ppm, a total peak area S1 in a range of 36-42 ppm and a total peak area S2 in a range of 10-17 ppm satisfying:1.0.ltoreq.(S1/S).times.100.ltoreq.10, 1.5.ltoreq.(S2/S).times.100.ltoreq.15, and S1
摘要翻译：用于显影静电图像的调色剂由至少包含粘合剂树脂，着色剂和蜡的调色剂颗粒组成。蜡满足以下条件：（a）在DSC（差示扫描量热计）曲线上升温时，在50-130℃区域显示最大吸热峰，（b）给出13 C-NMR（核磁共振）光谱，其总峰面积S在0-50ppm的范围内，总峰面积S1在36-42ppm范围内，总峰面积S2在10-17ppm的范围内满足：1.0 < 满足上述条件的蜡具有适当分支的长链结构，并且提供了（S1 / S）×100

7. 发明授权

US5955234A Toner for developing electrostatic image, and image forming method 失效
标题翻译：用于显影静电图像的调色剂和图像形成方法
公开(公告)号：US5955234A
公开(公告)日：1999-09-21
申请号：US947273
申请日：1997-10-08
申请人： Satoshi Matsunaga , Manabu Ohno , Tadashi Doujo
发明人： Satoshi Matsunaga , Manabu Ohno , Tadashi Doujo
IPC分类号： C08F257/00 , C08F265/06 , G03G9/08 , G03G9/087
CPC分类号： C08F257/00 , C08F265/06 , G03G9/081 , G03G9/08711 , G03G9/08782 , G03G9/08788 , G03G9/08795 , G03G9/08797
摘要： A toner for developing an electrostatic image is comprised of a binder resin, a colorant and a wax. The toner has the following rheological characteristics: (a) a temperature at which the ratio of a loss elastic modulus to a storage elastic modulus (G"/G'=tan .delta.) comes to be 1.0 is present in a temperature range of from 55.degree. C. to 70.degree. C., with an elastic modulus being 1.5.times.10.sup.8 Pa or below; (b) the ratio of the storage elastic modulus at a temperature of 40.degree. C. (G'.sub.40) to the storage elastic modulus at a temperature of 50.degree. C. (G'.sub.50), G'.sub.40 /G'.sub.50, is from 1.5 to 5.0; (c) the ratio of the storage elastic modulus at a temperature of 50.degree. C. (G'.sub.50) to the storage elastic modulus at a temperature of 60.degree. C. (G'.sub.60), G'.sub.50 /G'.sub.60, is from 3 to 20; (d) the ratio of the storage elastic modulus at a temperature of 70.degree. C. (G'.sub.70) to the storage elastic modulus at a temperature of 100.degree. C. (G'.sub.100), G'.sub.70 /G'.sub.100, is from 50 to 250; and (e) the ratio of the storage elastic modulus at a temperature of 110.degree. C. (G'.sub.110) to the storage elastic modulus at a temperature of 140.degree. C. (G'.sub.140), G'.sub.110 /G'.sub.140, is from 2 to 20.
摘要翻译：用于显影静电图像的调色剂由粘合剂树脂，着色剂和蜡组成。调色剂具有以下流变特性：（a）在下述的温度范围内存在损耗弹性模量与储能弹性模量（G“/ G'=tanδ）的比率为1.0的温度 55℃至70℃，弹性模量为1.5×10 8 Pa或更低; （b）在温度为40℃（G'40）下的储能弹性模量与50℃温度（G'50），G'40 / G'50，为1.5〜5.0; （c）温度为50℃（G'50）的储能弹性模量与60℃温度（G'60），G'50 / G'60，从3到20; （d）温度为70℃（G'70）时的储能弹性模量与100℃（G'100），G'70 / G'100的储能弹性模量的比率，从50到250; 和（e）温度为110℃（G'110）时的储能弹性模量与140℃温度下的储能弹性模量（G'140），G'110 / G'140 是从2到20。

8. 发明授权

US06623901B1 Toner for developing electrostatic image 失效
标题翻译：用于显影静电图像的调色剂
公开(公告)号：US06623901B1
公开(公告)日：2003-09-23
申请号：US08992427
申请日：1997-12-18
申请人： Takaaki Kohtaki , Makoto Unno , Yushi Mikuriya , Tadashi Doujo
发明人： Takaaki Kohtaki , Makoto Unno , Yushi Mikuriya , Tadashi Doujo
IPC分类号： G03G9083
CPC分类号： G03G9/08795 , G03G9/08755 , G03G9/09733
摘要： A toner for developing an electrostatic image is constituted by a binder resin and a long-chain compound. The binder resin is a polyester resin or vinyl resin respectively having an acid value of preferably 25-70 mgKOH/g. The long-chain compound is a long-chain alkyl alcohol having an OH value of 10-120 mgKOH/g or a long-chain alkyl carboxylic acid having an acid value of 5-120 mgKOH/g and is contained so as to satisfy a condition of the following formula (1) or formula (2): Formula (1) acid value of binder resin +OH value of long-chain alkyl alcohol >(¼)×OH value of binder resin, or Formula (2) acid value of binder resin +acid value of long-chain alkyl carboxylic acid >(¼)×OH value of binder resin. The toner is characterized by a good balance between fixing performances and developing performances suitable for a variety of models of image forming apparatus and in wide ranges of environmental conditions.
摘要翻译：用于显影静电图像的调色剂由粘合剂树脂和长链化合物构成。粘合剂树脂是分别具有优选25-70mgKOH / g的酸值的聚酯树脂或乙烯基树脂。长链化合物是OH值为10〜120mgKOH / g的长链烷基醇或酸值为5-120mgKOH / g的长链烷基羧酸，其含有以满足下式（1）或式（2）的条件：式（1）粘合剂树脂的酸值+长链烷基醇的OH值>（¼）粘合剂树脂的xOH值，或式（2）粘合剂的酸值树脂+长链烷基羧酸的酸值>（¼）xOH值的粘合剂树脂。调色剂的特征在于适用于多种型号的图像形成装置的定影性能和显影性能之间的良好平衡以及广泛的环境条件。

9. 发明授权

US5773183A Toner for developing electrostatic images 失效
标题翻译：用于显影静电图像的调色剂
公开(公告)号：US5773183A
公开(公告)日：1998-06-30
申请号：US749640
申请日：1996-11-15
申请人： Tadashi Doujo , Yuichi Mizoo , Takaaki Kotaki , Yushi Mikuriya
发明人： Tadashi Doujo , Yuichi Mizoo , Takaaki Kotaki , Yushi Mikuriya
IPC分类号： G03G9/083 , G03G9/087 , G03G9/09
CPC分类号： G03G9/091 , G03G9/08755 , G03G9/08795 , G03G9/0833 , G03G9/08782
摘要： A toner for developing an electrostatic image has a binder resin, a colorant and a charge control agent. The binder resin has a polyester resin having an acid value of from 15 to 40 and a hydroxyl value of 45 or less. The toner has, in its molecular weight distribution as measured by gel permeation chromatography, tetrahydrofuran-soluble matter having a weight average molecular weight Mw of 100,000 or more, having a ratio of weight average molecular weight Mw to number average molecular weight Mn, Mw/Mn, of not less than 35, containing from 70% to 94% of a low-molecular weight region component having a molecular weight of less than 150,000, containing from 1% to 10% of a medium-molecular weight region component having a molecular weight of from 150,000 to 500,000, and containing from 5% to 25% of a high-molecular weight region component having a molecular weight of more than 500,000. The high-molecular weight region component is more than the medium-molecular weight region component.
摘要翻译：用于显影静电图像的调色剂具有粘合剂树脂，着色剂和电荷控制剂。粘合剂树脂具有酸值为15〜40，羟值为45以下的聚酯树脂。调色剂在通过凝胶渗透色谱法测定的分子量分布中，具有重均分子量Mw为100,000以上的四氢呋喃可溶性物质，重均分子量Mw与数均分子量Mn的比，Mw / Mn不低于35，含有70％至94％的分子量小于150,000的低分子量成分，含有1％至10％的具有分子量重量为15万至500,000，并含有5％至25％的分子量大于500,000的高分子量成分。高分子量区域成分大于中等分子量区域成分。

10. 发明授权

US06365314B1 Toner for developing electrostatic image, image forming method and process cartridge 失效
标题翻译：用于显影静电图像，成像方法和处理盒的调色剂
公开(公告)号：US06365314B1
公开(公告)日：2002-04-02
申请号：US09457138
申请日：1999-12-09
申请人： Koichi Tomiyama , Takaaki Kohtaki , Manabu Ohno , Makoto Unno , Yushi Mikuriya , Nobuyuki Okubo , Tadashi Doujo , Shunji Suzuki
发明人： Koichi Tomiyama , Takaaki Kohtaki , Manabu Ohno , Makoto Unno , Yushi Mikuriya , Nobuyuki Okubo , Tadashi Doujo , Shunji Suzuki
IPC分类号： G03G9097
CPC分类号： G03G9/0819 , G03G9/0975 , G03G9/09783 , G03G15/08
摘要： A toner for developing electrostatic images. having a uniform composition and uniform performances over varying sizes of toner particles is constituted by (a) a binder resin, (b) a long-chain alkyl compound and (c) a specific azo-type iron complex. The long-chain alkyl compound is represented by the following formula (1), (2) or (3): CH3&Parenopenst;CH2&Parenclosest;xCH2OH (1), CH3&Parenopenst;CH2&Parenclosest;yCH2COOH (3), wherein x and y independently denote an average value in the range of 35-150.
摘要翻译：用于静电图像显影的调色剂。具有均匀的组成和不同尺寸的调色剂颗粒的均匀性能由（a）粘合剂树脂，（b）长链烷基化合物和（c）特定的偶氮型铁络合物构成。长链烷基化合物由下式（1），（2）或（3）表示：其中x和y独立地表示在35-150范围内的平均值。

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