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1. 发明申请

WO0040331A9 APPARATUS AND METHOD FOR COMBINATORIAL RESEARCH FOR CATALYSTS AND POLYMERS 审中-公开
标题翻译：用于催化剂和聚合物的组合研究的装置和方法
公开(公告)号：WO0040331A9
公开(公告)日：2001-09-13
申请号：PCT/US0000418
申请日：2000-01-06
申请人： SYMYX TECHNOLOGIES INC , TURNER HOWARD W , VANERDEN LYNN , DALES CAMERON G , SAFIR ADAM , NIELSEN RALPH B
发明人： TURNER HOWARD W , VANERDEN LYNN , DALES CAMERON G , SAFIR ADAM , NIELSEN RALPH B
IPC分类号： B01D15/08 , B01D15/26 , B01D15/32 , B01D15/34 , B01J19/00 , B01J19/26 , C40B40/14 , C40B40/18 , G01N15/02 , G01N30/02 , G01N30/16 , G01N30/24 , G01N30/30 , G01N30/32 , G01N30/46 , G01N30/54 , G01N30/60 , G01N30/88 , G01N33/44 , G01N35/08 , B01J31/16 , C07B61/00
CPC分类号： B01J19/26 , B01D15/08 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/0046 , B01J2219/00274 , B01J2219/00283 , B01J2219/00308 , B01J2219/0031 , B01J2219/00313 , B01J2219/00335 , B01J2219/00337 , B01J2219/00344 , B01J2219/00351 , B01J2219/00452 , B01J2219/00495 , B01J2219/00585 , B01J2219/00587 , B01J2219/0059 , B01J2219/00596 , B01J2219/00689 , B01J2219/00691 , B01J2219/00704 , B01J2219/00707 , B01J2219/00722 , B01J2219/00738 , B01J2219/00745 , C40B40/14 , C40B40/18 , G01N15/0205 , G01N30/02 , G01N30/16 , G01N30/24 , G01N30/30 , G01N30/46 , G01N30/54 , G01N30/6052 , G01N30/88 , G01N33/44 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/324 , G01N2030/885
摘要： A method and system for researching and developing and/or optimizing new catalysts and polymers in a combinatorial manner is disclosed. The method begins with starting components or a ligand library and provides methods of creating catalyst or product libraries, which are then tested in a reaction of interest. The system uses methods of robotic handling for moving libraries from station to station. The method and apparatus are especially useful for synthesizing, screening, and characterizing combinatorial catalyst libraries.
摘要翻译：公开了以组合方式研究和/或优化新催化剂和聚合物的方法和系统。该方法从起始组分或配体文库开始，并提供产生催化剂或产物文库的方法，然后在感兴趣的反应中进行测试。该系统使用机器人处理方法来移动图书馆从站到站。该方法和设备对于组合催化剂文库的合成，筛选和表征特别有用。

2. 发明申请

WO0032308A3 CONTINUOUS FEED PARALLEL REACTOR 审中-公开
标题翻译：连续式并流反应器
公开(公告)号：WO0032308A3
公开(公告)日：2000-11-23
申请号：PCT/US9928741
申请日：1999-12-03
申请人： SYMYX TECHNOLOGIES INC , FREITAG J CHRISTOPHER , HAJDUK DAMIAN , NIELSEN RALPH B , SAFIR ADAM , TIEDE RICHARD
发明人： FREITAG J CHRISTOPHER , HAJDUK DAMIAN , NIELSEN RALPH B , SAFIR ADAM , TIEDE RICHARD
IPC分类号： G01N35/02 , B01J4/00 , B01J19/00 , B01J19/26 , C08F2/00 , C40B40/14 , C40B60/14 , G01N35/10
CPC分类号： B01J19/0046 , B01J2219/0029 , B01J2219/00308 , B01J2219/0031 , B01J2219/00313 , B01J2219/00315 , B01J2219/00319 , B01J2219/00351 , B01J2219/00481 , B01J2219/00484 , B01J2219/00495 , B01J2219/00585 , B01J2219/00691 , B01J2219/0072 , B01J2219/00722 , C40B40/14 , C40B60/14 , Y10S526/92 , Y10T436/11 , Y10T436/25 , Y10T436/25625 , Y10T436/2575
摘要： A method and apparatus (10) for reacting a plurality of different mixtures in parallel in a semi-batch or continuous mode is provided. Each reaction is contained within a reactor vessel (102), the reactor vessels (102) combined into a reactor block (100). Reactant(s) to be added during the reaction are kept in a header barrel (202), which has a plunger (402) to feed reactant(s) from the header barrel (202) through a transfer line (302) into the reactor vessel (102). The plunger (402) is moved using a drive system (500). The header barrels (202) are optionally combined in a header block (200). The header block (200) is sealed to a plate (300) containing the transfer lines (302), which in turn is sealed to the reactor block (100). A latch mechanism (600) is provided for easy sealing of the reactor (100) and header blocks (200) to the plate (300). The entire apparatus (10) may be placed on a rocker or rotating plate for mixture as the reaction is proceeding.
摘要翻译：提供了用于以半间歇或连续模式并行地反应多种不同混合物的方法和装置（10）。每个反应包含在反应器容器（102）内，反应器容器（102）组合成反应器块（100）。在反应过程中加入的反应物保持在具有活塞（402）的集管桶（202）中以将来自集管桶（202）的反应物通过输送管线（302）供入反应器容器（102）。柱塞（402）使用驱动系统（500）移动。标题桶（202）可选地组合在标题块（200）中。集管块（200）被密封到包含传输管线（302）的板（300），所述传输管线又被密封到反应器块（100）。提供闩锁机构（600）以便容易地将反应器（100）和集管块（200）密封到板（300）。随着反应的进行，整个装置（10）可以放置在摇摆器或旋转盘上用于混合。

3. 发明申请

WO2007022110A3 EVENT-BASED LIBRARY PROCESS DESIGN 审中-公开
标题翻译：基于事件的图书馆流程设计
公开(公告)号：WO2007022110A3
公开(公告)日：2007-09-27
申请号：PCT/US2006031695
申请日：2006-08-14
申请人： SYMYX TECHNOLOGIES INC , KENYON KIRK , LOW ERIC , SAFIR ADAM
发明人： KENYON KIRK , LOW ERIC , SAFIR ADAM
IPC分类号： G06F19/00 , G01N37/00
CPC分类号： C40B50/02 , C40B30/02 , G06F19/702
摘要： Systems, methods and apparatus for designing a process to be performed at regions of an experiment library, the process involving the application of components at the library regions. Components are associated with regions of the experiment library. Each of the components represents a material or process parameter to be applied at the regions (100). A plurality o experiment stages are defined, each having one or more associated event types that are selected from predetermined eve types and define a start condition for the corresponding stage. For each of the library regions, the components are associated with one or more of the experiment stages. A plurality of component profiles are generated, which represent processes to be performed at the various regions, and which describe the application over time of one or more of the components associated with a corresponding region or regions according to the associated experiment stages (120).
摘要翻译：用于设计在实验库区域执行的过程的系统，方法和设备，涉及在库区域应用组件的过程。组件与实验库的区域相关联。每个部件表示要在区域（100）处施加的材料或工艺参数。定义多个o实验阶段，每个实验阶段具有从预定前夕类型中选择的一个或多个相关联的事件类型并且定义相应阶段的起始条件。对于每个库区域，组件与一个或多个实验阶段相关联。生成多个组件简档，其表示将在各个区域执行的处理，并且根据相关联的实验阶段（120）描述与相应区域相关联的一个或多个组件随着时间的应用。

4. 发明专利

CA2351336C CONTINUOUS FEED PARALLEL REACTOR 未知
公开(公告)号：CA2351336C
公开(公告)日：2005-05-17
申请号：CA2351336
申请日：1999-12-03
申请人： SYMYX TECHNOLOGIES INC
发明人： NIELSEN RALPH B , SAFIR ADAM , TIEDE RICHARD , HAJDUK DAMIAN , FREITAG J CHRISTOPHER
IPC分类号： G01N35/02 , B01J4/00 , B01J19/00 , B01J19/26 , C08F2/00 , C40B40/14 , C40B60/14 , G01N35/10
摘要： A method and apparatus (10) for reacting a plurality of different mixtures in parallel in a semi-batch or continuous mode is provided. Each reaction is contained within a reactor vessel (102), the reactor vessels (102) combined into a reactor block (100). Reactant(s) to be added during the reaction are kept in a header barrel (202), which has a plunger (402) to feed reactant(s) from the header barrel (202) through a transfer line (302) into the reactor vessel (102). The plunger (402) is moved using a drive system (500). The header barrels (202) are optionally combined in a header block (200). The header block (200) is seated to a plate (300) containing the transfer lines (302), which in turn is sealed to the reactor block (100). A latch mechanism (600) is provided for easy sealing of the reactor (100) and header blocks (200) to the plate (300). The entire apparatus (10) may be placed on a rocker or rotating plate for mixture as the reaction is proceeding.

5. 发明专利

AU2041200A Continuous feed parallel reactor 未知
公开(公告)号：AU2041200A
公开(公告)日：2000-06-19
申请号：AU2041200
申请日：1999-12-03
申请人： SYMYX TECHNOLOGIES INC
发明人： FREITAG CHRISTOPHER J , HAJDUK DAMIAN , NIELSEN RALPH B , SAFIR ADAM , TIEDE RICHARD
IPC分类号： G01N35/02 , B01J4/00 , B01J19/00 , B01J19/26 , C08F2/00 , C40B40/14 , C40B60/14 , G01N35/10

6. 发明专利

AU3742599A Rapid characterization of polymers 未知
公开(公告)号：AU3742599A
公开(公告)日：1999-10-25
申请号：AU3742599
申请日：1999-04-03
申请人： SYMYX TECHNOLOGIES INC
发明人： CARLSON ERIC , SAFIR ADAM , PETRO MIROSLAV , NIELSEN RALPH B , LEE THOMAS S , FRECHET JEAN M J , DALES G CAMERON , KUEBLER SIGRID C , BENNETT JAMES
IPC分类号： G01N37/00 , B01D15/08 , B01D15/26 , B01D15/32 , B01D15/34 , B01J19/00 , B01J19/26 , C40B40/14 , C40B40/18 , G01N1/00 , G01N15/02 , G01N30/02 , G01N30/16 , G01N30/24 , G01N30/30 , G01N30/32 , G01N30/46 , G01N30/54 , G01N30/60 , G01N30/88 , G01N30/90 , G01N33/44 , G01N35/08
摘要： A method and system for researching and developing and/or optimizing new catalysts and products in a combinatorial manner is disclosed. The method begins with starting components or a ligand library and provides methods of creating catalyst or product libraries, which are then tested in a reaction of interest. The system uses methods of robotic handling for moving libraries from station to station. The method and apparatus are especially useful for synthesizing, screening, and characterizing combinatorial catalyst libraries, but also offer significant advantages over conventional experimental methods as well.

7. 发明专利

CA2527935A1 RAPID CHARACTERIZATION OF POLYMERS 未知
公开(公告)号：CA2527935A1
公开(公告)日：1999-10-14
申请号：CA2527935
申请日：1999-04-02
申请人： SYMYX TECHNOLOGIES INC
发明人： LEE THOMAS S , FRECHET JEAN M J , DALES G CAMERON , KUEBLER SIGRID C , SAFIR ADAM , CARLSON ERIC , PETRO MIROSLAV , BENNETT JAMES , NIELSEN RALPH B
IPC分类号： G01N30/54 , G01N30/24 , G01N30/30 , G01N30/36 , G01N30/74 , G01N35/10
摘要： A method for characterizing a polymer sample that includes the steps of withdrawing a polymer sample from a sample container into an injection probe of an auto- sampler where the probe is heated to maintain the withdrawn sample at a temperature of not less than about 75 degrees Celsius while resident in the probe. The heated injection probe resides in a first environment maintained at about ambient temperature while withdrawing the polymer sample. The method further includes loading at least a portion of the withdrawn sample into an injection port or a loading port of a liquid chromatography system where the injection port or loading port is adaptable for fluid communication with a chromatographic column. The chromatographic column resides in a heated second environment maintained at a temperature of not less than about 75 degrees Celsius. The loaded sample is injected into a mobile phase of the liquid chromatography system. The sample is maintained at a temperature but not les s than about 75 degrees Celsius during a period of time including from when the sample is withdrawn from the sample container to when the sample is within the heated second environment. The injected sample is chromatographically separated and a property of the sample or a composition thereof is detected.

8. 发明专利

AU3733800A Controlled free radical emulsion and water-based polymerizations and seeded methodologies 未知
公开(公告)号：AU3733800A
公开(公告)日：2000-09-28
申请号：AU3733800
申请日：2000-03-08
申请人： SYMYX TECHNOLOGIES INC
发明人： KLAERNER GERRIT , SAFIR ADAM , NIELSEN RALPH B , JANDELEIT BERND , HUEFNER PETER , LI YUNXIAO
IPC分类号： C08F2/22 , C08F2/28 , C08F2/38 , C08F4/00 , C08F220/58 , G01N33/543
摘要： Nitroxides having an alpha-carbon atom with a destabilizing moiety are effective control agents for emulsion and water-based polymerizations, including the formation of block copolymers from a wide range of monomers. The nitroxide radicals may be used as a free radical or as an adduct with a residue from the initiator. The emulsions have living characteristics, including the re-initiation of polymer chains. Also, a seeded process for emulsions, which includes the step-wise addition of monomer is disclosed, providing access to a wide range of initiator types.

10. 发明专利

CA2290394C RAPID CHARACTERIZATION OF POLYMERS 未知
公开(公告)号：CA2290394C
公开(公告)日：2006-02-28
申请号：CA2290394
申请日：1999-04-02
申请人： SYMYX TECHNOLOGIES INC
发明人： LEE THOMAS S , NIELSEN RALPH B , FRECHET JEAN M J , SAFIR ADAM , BENNETT JAMES , CARLSON ERIC , DALES G CAMERON , KUEBLER SIGRID C , PETRO MIROSLAV
IPC分类号： G01N30/02 , G01N37/00 , B01D15/08 , B01D15/26 , B01D15/32 , B01D15/34 , B01J19/00 , B01J19/26 , C40B40/14 , C40B40/18 , G01N1/00 , G01N1/14 , G01N15/02 , G01N21/53 , G01N30/16 , G01N30/24 , G01N30/30 , G01N30/32 , G01N30/46 , G01N30/54 , G01N30/60 , G01N30/74 , G01N30/88 , G01N30/90 , G01N33/44 , G01N35/08
摘要： Rapid characterization and screening of polymer samples to determine average molecular weight, molecular weight distribution and other properties is disclosed. Rapid flow characterization systems and methods, including liquid chromatography and flow-injection analysis systems and methods are preferably employed. High throughput, automated sampling systems and methods, high-temperature characterization systems and methods, and rapid, indirect calibration compositions and methods are also disclosed. The described methods, systems, and devices have primary applications in combinatorial polymer research and in industrial process control.

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