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1. 发明申请

WO2012150253A1 METHOD FOR MANUFACTURING FLUOROELASTOMERS 审中-公开
标题翻译：制造荧光体的方法
公开(公告)号：WO2012150253A1
公开(公告)日：2012-11-08
申请号：PCT/EP2012/058011
申请日：2012-05-02
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.p.A. , KENT, Bradley Lane , APOSTOLO, Marco , CHERNYSHEVA, Liubov , COMINO, Giovanni
发明人： KENT, Bradley Lane , APOSTOLO, Marco , CHERNYSHEVA, Liubov , COMINO, Giovanni
IPC分类号： C08F214/22
CPC分类号： C08F214/28 , C08F214/22 , C08F214/222 , C08F214/225
摘要： The invention pertains to a process for manufacturing a fluoroelastomer [fluoroelastomer (A)] having a heat of fusion of less than 5 J/g as measured by ASTM D-3418-08, said method comprising emulsion polymerizing vinylidene fluoride (VDF) in the presence of at least one additional fluorinated monomer, in an aqueous polymerization medium, said method comprising polymerizing VDF and said additional fluorinated monomer(s) in the presence of a redox radical initiator system comprising: - at least one organic oxidizing agent [agent (O)]; - at least one organic reducing agent [agent (R)]; and - at least one transition metal catalyst [agent (P)]; wherein agent (O) is fed to said polymerization medium separately from agent (R) and agent (P), so that agent (O) comes in contact with agent (R) and agent (P) exclusively in said polymerization medium comprising VDF and optional additional monomer(s), to fluoroelastomers having low amount of chain defects and low amount of polar end groups, notably obtainable from said process, and to curable compositions therefrom.
摘要翻译：本发明涉及通过ASTM D-3418-08测定的具有小于5J / g的熔化热的含氟弹性体（含氟弹性体（A）]的制造方法，所述方法包括：将聚偏二氟乙烯在水性聚合介质中存在至少一种另外的氟化单体，所述方法包括在氧化还原自由基引发剂体系存在下聚合VDF和所述另外的氟化单体，其包含： - 至少一种有机氧化剂）]; - 至少一种有机还原剂[agent（R）]; 和 - 至少一种过渡金属催化剂[试剂（P）]; 其中将试剂（O）与试剂（R）和试剂（P）分开地进料到所述聚合介质中，使得试剂（O）仅在包含VDF的聚合介质中与试剂（R）和试剂（P））接触，具有少量链缺陷和少量极性端基的含氟弹性体，特别是可从所述方法得到的含氟弹性体及其可固化组合物。

2. 发明申请

WO2012150256A1 METHOD FOR MANUFACTURING FLUOROELASTOMERS 审中-公开
标题翻译：制造荧光体的方法
公开(公告)号：WO2012150256A1
公开(公告)日：2012-11-08
申请号：PCT/EP2012/058018
申请日：2012-05-02
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.p.A. , CHERNYSHEVA, Liubov , KENT, Bradley Lane , COMINO, Giovanni , KAPELYUSHKO, Valeriy
发明人： CHERNYSHEVA, Liubov , KENT, Bradley Lane , COMINO, Giovanni , KAPELYUSHKO, Valeriy
IPC分类号： C08F214/22
CPC分类号： C08F214/28 , C08F214/22 , C08F214/222 , C08F214/225
摘要： The invention pertains to a process for manufacturing a fluoroelastomer [fluoroelastomer (A)] having a heat of fusion of less than 5 J/g as measured by ASTM D-3418-08, said method comprising emulsion polymerizing vinylidene fluoride (VDF) in the presence of at least one additional fluorinated monomer, in an aqueous polymerization medium, said method comprising polymerizing VDF and said additional fluorinated monomer(s) in the presence of a redox radical initiator system comprising: - at least one organic oxidizing agent [agent (O)]; - at least one organic reducing agent [agent (R)]; wherein agent (O) is fed to said polymerization medium separately from agent (R), so that agent (O) comes in contact with agent (R) exclusively in said polymerization medium comprising VDF and optional additional monomer(s), to fluoroelastomers having low amount of chain defects and low amount of polar end groups, notably obtainable from said process, and to curable compositions therefrom.
摘要翻译：本发明涉及通过ASTM D-3418-08测定的具有小于5J / g的熔化热的含氟弹性体（含氟弹性体（A）]的制造方法，所述方法包括：将聚偏二氟乙烯在水性聚合介质中存在至少一种另外的氟化单体，所述方法包括在氧化还原自由基引发剂体系存在下聚合VDF和所述另外的氟化单体，其包含： - 至少一种有机氧化剂）]; - 至少一种有机还原剂[agent（R）]; 其中将试剂（O）与试剂（R）分开地加入到所述聚合介质中，使得试剂（O）仅在包含VDF和任选的另外的单体的所述聚合介质中与试剂（R）接触，具有含氟弹性体少量的链缺陷和少量极性端基，特别可从所述方法获得，以及可固化组合物。

3. 发明申请

WO2013037707A1 POLYMERIZATION PROCESS 审中-公开
标题翻译：聚合工艺
公开(公告)号：WO2013037707A1
公开(公告)日：2013-03-21
申请号：PCT/EP2012/067495
申请日：2012-09-07
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.p.A. , KENT, Bradley Lane , VENERONI, Alessandro , KAPELYUSHKO, Valeriy
发明人： KENT, Bradley Lane , VENERONI, Alessandro , KAPELYUSHKO, Valeriy
IPC分类号： C08F14/22 , C09D127/16 , C08K5/5313 , C08F2/26
CPC分类号： C08F14/22 , C08K5/5313 , C09D127/16 , C08F2/16 , C08F2/26 , C08L27/16
摘要： The invention pertains to a process for manufacturing a dispersion of a vinylidene fluoride (VDF) thermoplastic polymer [polymer (F)], said process comprising polymerizing VDF in an aqueous phase comprising at least one bisfluorocarbonphosphinic surfactant of formula R F 1 R F 2 P(0)O - X a + wherein R F 1 and R F 2 , equal to or different from each other, is independently a fluorinated or perfluorinated C 1 -C 20 group, and X a is H, a alkali metal or a NR H 4 group, with R H being H or a C 1 -C 6 hydrocarbon group [surfactant (P)], and to a vinylidene fluoride thermoplastic polymer dispersion therefrom.
摘要翻译：本发明涉及一种制备偏二氟乙烯（VDF）热塑性聚合物[聚合物（F）]的分散体的方法，所述方法包括在包含至少一种式RF 1 RF 2P（0）的二氟碳化膦表面活性剂的水相中聚合VDF， O-Xa +其中RF 1和RF 2彼此相同或不同，独立地为氟化或全氟化的C1-C20基团，Xa为H，碱金属或NRH4基团，其中RH为H或 C1-C6烃基[表面活性剂（P）]，和偏二氟乙烯热塑性聚合物分散体。

4. 发明申请

WO2013010936A1 AQUEOUS VINYLIDENE FLUORIDE POLYMER LATEX 审中-公开
标题翻译：水性乙烯基氟化物聚合物
公开(公告)号：WO2013010936A1
公开(公告)日：2013-01-24
申请号：PCT/EP2012/063778
申请日：2012-07-13
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A. , STANGA, Milena , PIERI, Riccardo , BERTASA, Anna Maria , KENT, Bradley Lane , BRINATI, Giulio
发明人： STANGA, Milena , PIERI, Riccardo , BERTASA, Anna Maria , KENT, Bradley Lane , BRINATI, Giulio
IPC分类号： C08L27/16 , C09D127/16 , C08K3/04 , H01M4/04 , H01M10/0525
CPC分类号： H01M4/623 , C08L27/16 , C09D127/16 , H01M4/0402 , H01M4/0404 , H01M4/133 , H01M4/1393 , H01M4/622 , H01M10/0525
摘要： The present invention pertains to an aqueous composition comprising: (A) an aqueous latex comprising at least one vinylidene fluoride (VDF) polymer [polymer (F)] comprising recurring units derived from vinylidene fluoride (VDF) and at least one (meth)acrylic monomer (MA) having formula (I) here below: wherein: - R 1 , R 2 and R 3 , equal to or different from each other, are independently selected from a hydrogen atom and a C 1 -C 3 hydrocarbon group, and - R OH is a hydrogen atom or a C 1 -C 5 hydrocarbon moiety comprising at least one hydroxyl group, (B) at least one powdery electrode material, and (C) optionally, less than 10% by weight, based on the total weight of the aqueous composition, of at least one organic solvent (S), wherein the polymer (F) in the aqueous latex is under the form of primary particles having an average primary particle size of less than 1 μm, as measured according to ISO 13321. The present invention also pertains to a process for manufacturing an electrode using said aqueous composition, to an electrode comprising a metal substrate coated on at least one surface with said aqueous composition and to use of said electrode for manufacturing a non-aqueous-type electrochemical device.
摘要翻译：本发明涉及一种水性组合物，其包含：（A）包含至少一种含偏二氯乙烯（VDF）的重复单元和至少一种（甲基）丙烯酸酯的偏二氟乙烯（VDF）聚合物[聚合物（F）具有式（I）的单体（MA）如下：其中：-R 1，R 2和R 3彼此相同或不同，独立地选自氢原子和C1-C3烃基，和-ROH是氢原子或包含至少一个羟基的C 1 -C 5烃部分，（B）至少一种粉末状电极材料，和（C）任选地，基于水性组合物的总重量，小于10重量％至少一种有机溶剂（S），其中根据ISO 13321测量，水性胶乳中的聚合物（F）是平均一次粒径小于1μm的初级颗粒的形式。本发明还涉及一种使用所述水溶液制造电极的方法涉及包含涂覆在至少一个表面上的金属基材与所述水性组合物的电极，并且使用所述电极来制造非水型电化学装置。

5. 发明申请

WO2012175414A1 METHOD FOR POLYMERIZING VINYLIDENE FLUORIDE 审中-公开
标题翻译：聚乙烯基氟化物的方法
公开(公告)号：WO2012175414A1
公开(公告)日：2012-12-27
申请号：PCT/EP2012/061409
申请日：2012-06-15
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A. , KENT, Bradley Lane , KAPELYUSHKO, Valeriy , BRINATI, Giulio , VENERONI, Alessandro
发明人： KENT, Bradley Lane , KAPELYUSHKO, Valeriy , BRINATI, Giulio , VENERONI, Alessandro
IPC分类号： C08F14/22 , C08F214/22
CPC分类号： C08K5/42 , C08F14/22 , C08F214/22 , C08F2/16
摘要： A process for manufacturing a dispersion of a vinylidene fluoride (VDF) thermoplastic polymer [polymer (F)], said process comprising polymerizing VDF in an aqueous phase comprising from 0.5 to 1.5 g/l of at least one surfactant of formula F-(CF 2 CF 2 ) 3 -CH 2 CH 2 -SO 3 X a , wherein X a is H, a alkali metal or a NR H 4 group, with R H being H or a C 1 -C 6 hydrocarbon group [surfactant (T)] and an organic oxidizing agent [agent (O)] as polymerization initiator.
摘要翻译：一种制备偏二氟乙烯（VDF）热塑性聚合物[聚合物（F）]的分散体的方法，所述方法包括在包含0.5至1.5g / l的至少一种式F-（CF 2 CF 2）的表面活性剂的水相中聚合VDF ）3-CH 2 CH 2 -SO 3 Xa，其中Xa为H，碱金属或NRH 4基，RH为H或C1-C6烃基[表面活性剂（T）]和有机氧化剂[试剂（O）]为聚合引发剂。

6. 发明申请

WO2012084578A1 VINYLIDENE FLUORIDE COPOLYMERS 审中-公开
标题翻译：乙烯基氟化物共聚物
公开(公告)号：WO2012084578A1
公开(公告)日：2012-06-28
申请号：PCT/EP2011/072506
申请日：2011-12-13
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A. , STANGA, Milena , KENT, Bradley Lane , MARRANI, Alessio , BRINATI, Giulio
发明人： STANGA, Milena , KENT, Bradley Lane , MARRANI, Alessio , BRINATI, Giulio
IPC分类号： C08F14/22 , C08F214/22 , C08L27/16 , C08J5/22 , H01M4/00 , C08F2/16
CPC分类号： C08F14/22 , C08F214/22 , C08F214/225 , C08J5/2237 , C08J2327/16 , C08K5/06 , C08L27/16 , C08L33/02 , C08L2205/02 , C08L2205/025 , H01M4/02 , H01M4/8605 , H01M8/0289 , H01M8/1023 , H01M10/0565 , Y02E60/521 , Y02P70/56 , C08F2/16 , C08F220/06 , C08F214/182 , C08F214/24
摘要： The present invention pertains to a fluoropolymer [polymer (F)] comprising: - recurring units derived from vinylidene fluoride (VDF), and - from 0.01 % to 5% by moles of recurring units derived from at least one (meth)acrylic monomer [monomer (MA)] having formula (I), wherein: - R 1 , R 2 and R 3 , equal to or different from each other, are independently selected from a hydrogen atom and a C 1 -C 3 hydrocarbon group, and - R OH represents a hydrogen atom or a C 1 -C 5 hydrocarbon moiety comprising at least one hydroxyl group, said polymer (F) comprising end groups having formula -CF 2 H and/or -CF 2 CH 3 in an amount of at least 30 mmoles per Kg of vinylidene fluoride (VDF) recurring units. The invention also pertains to a process for the manufacture of said polymer (F) and to use of said polymer (F) as binders for the manufacture of electrodes or for the manufacture of membranes.
摘要翻译：本发明涉及含氟聚合物[聚合物（F）]，其包含： - 衍生自偏二氟乙烯（VDF）的重复单元，和 - 0.01％至5％（摩尔）来自至少一种（甲基）丙烯酸单体的重复单元[ 具有式（I）的单体（MA）]，其中：-R 1，R 2和R 3彼此相同或不同，独立地选自氢原子和C1-C3烃基，-ROH表示氢原子或包含至少一个羟基的C 1 -C 5烃部分，所述聚合物（F）包含具有式-CF 2 H和/或-CF 2 CH 3的端基，其量为至少30mmol / Kg偏二氟乙烯（VDF）重复单元。本发明还涉及制备所述聚合物（F）的方法和所述聚合物（F）用作制备电极或制造膜的粘合剂。

7. 发明申请

WO2012160135A1 HYDRO-FLUOROCOMPOUNDS 审中-公开
标题翻译： HYDRO氟化合物
公开(公告)号：WO2012160135A1
公开(公告)日：2012-11-29
申请号：PCT/EP2012/059702
申请日：2012-05-24
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.p.A. , TORTELLI, Vito , WLASSICS, Ivan , MONZANI, Cristiano , KENT, Bradley Lane , VENERONI, Alessandro
发明人： TORTELLI, Vito , WLASSICS, Ivan , MONZANI, Cristiano , KENT, Bradley Lane , VENERONI, Alessandro
IPC分类号： C07C51/00 , C07C51/41 , C07C59/115
CPC分类号： C07C59/135 , C07C51/00 , C07C51/377 , C07C51/41 , C07C59/115 , C08K3/20
摘要： The invention pertains to certain hydro-fluorocompounds of the following formula (I): R f O-R H -O-(CH2) m -[CF(X)] n -COOX a wherein: - X a is H, a monovalent metal (preferably an alkaline metal) or an ammonium group of formula -N(R' n ) 4 , wherein each of R' n , equal to or different from each other, independently represents a hydrogen atom or a C 1-6 hydrocarbon group (preferably an alkyl group); - R f is a C 1 -C 6 (per)fluoroalkyl optionally comprising one or more catenary oxygen atoms, preferably R f is a group of formula R 'f -CH 2 -, wherein R' f is a C 1 -C 5 perfluorinated group, possibly comprising one or more ethereal oxygens, preferably a C 1 -C 3 perfluorinated group, possibly comprising one or more ethereal oxygens; - R H is a fluorine-free hydrocarbon group optionally comprising one or more catenary oxygen atoms; - X is F or CF 3 , preferably X is F; - m is 0 or 1; - n is 1 to 3, to a process for the manufacture of said hydro-fluorocompounds, to a method of making fluoropolymers in the presence of said hydro-fluorocompounds, and to fluoropolymer dispersions comprising said hydro-fluorocompound.
摘要翻译：本发明涉及以下式（I）的某些含氟化合物：RfO-RH-O-（CH2）m- [CF（X）] n-COOXa其中：-Xa为H，一价金属（优选碱金属）或式-N（R'n）4的铵基，其中R'n彼此相同或不同，各自独立地表示氢原子或C1-6烃基（优选烷基） ; -R f是任选地包含一个或多个链状氧原子的C 1 -C 6（全）氟烷基，优选地，Rf是式R'f-CH 2 - 的基团，其中R'f是C1-C5全氟化基团，可能包含一个或多个更多的醚氧，优选C1-C3全氟化基团，可能包含一个或多个醚类氧; - RH是任选地包含一个或多个链状氧原子的无氟烃基; - X是F或CF 3，优选X是F; - m为0或1; n为1至3，涉及制备所述含氟化合物的方法，涉及在所述含氟化合物存在下制备含氟聚合物的方法，以及包含所述氢氟化合物的含氟聚合物分散体。

8. 发明申请

WO2019076901A1 METHOD FOR THE SYNTHESIS OF FLUOROPOLYMERS 审中-公开
公开(公告)号：WO2019076901A1
公开(公告)日：2019-04-25
申请号：PCT/EP2018/078254
申请日：2018-10-16
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A.
发明人： D'APRILE, Fiorenza , KAPELYUSHKO, Valeriy , KENT, Bradley Lane , BRINATI, Giulio , PONTA, Laura
IPC分类号： C08F14/22 , C08F2/16
CPC分类号： C08F14/22 , C08F214/225 , C08F228/02 , C08F2/16 , C08F2/001
摘要： The present invention relates to a fluorosurfactant-free emulsion polymerization method for the synthesis of a fluoropolymer, more in particular of a VDF-based polymer.

9. 发明申请

WO2018050688A1 FLUORINATED THERMOPLASTIC ELASTOMER 审中-公开
标题翻译：氟化热塑性弹性体
公开(公告)号：WO2018050688A1
公开(公告)日：2018-03-22
申请号：PCT/EP2017/073008
申请日：2017-09-13
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A.
发明人： DOSSI, Marco , AVATANEO, Marco , FANTONI, Matteo , KENT, Bradley Lane , CORASANITI, Martina , SRINIVASAN, Satchit
IPC分类号： C08F293/00 , C08F2/38 , C08L53/00
CPC分类号： C08F293/00 , C08F2/30 , C08F2/38 , C08L53/00
摘要： The present invention pertains to a fluorinated thermoplastic elastomer, to a process for the manufacture of said fluorinated thermoplastic elastomer and to uses of said fluorinated thermoplastic elastomer in various applications, especially in low temperature applications.
摘要翻译：本发明涉及氟化热塑性弹性体，制造所述氟化热塑性弹性体的方法以及所述氟化热塑性弹性体在各种应用中的用途，尤其是在低温应用中。 >

10. 发明申请

WO2022200345A1 COMPOSITION FOR ELECTRODES 审中-公开
公开(公告)号：WO2022200345A1
公开(公告)日：2022-09-29
申请号：PCT/EP2022/057481
申请日：2022-03-22
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A.
发明人： AGOSTINI, Azzurra , PENA CABRERA, Rosita Lissette , MAZZOLA, Mirko , BRINATI, Giulio , KENT, Bradley Lane , DOSSI, Marco
IPC分类号： H01M4/62 , H01M4/04 , H01M4/131 , H01M4/136 , H01M4/1391 , H01M4/1397 , H01M4/505 , H01M4/525 , H01M4/58
摘要： The present invention pertains to electrode-forming compositions, comprising an electro-active material and a VDF based polymer comprising at least 70% by moles of recurring units derived from VDF, less than 0.9% by moles of recurring units derived from monomers comprising a functional group selected from carbonylic, carboxylic, sulfonic, sulfinic, phosphonic, hydroxy, -SH, ester or mixtures thereof, having a TM between 130°C and 180°C and comprising less than 700 mmoles/kg of chain ends -CF2H and -CF2CH3. The composition has good adhesion and is physically stable over time. The invention also relates to the use of said electrode-forming compositions in a process for the manufacture of electrodes, to said electrodes and to electrochemical devices such as secondary batteries comprising said electrodes.

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