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1. 发明申请

WO2012104365A3 METHOD FOR MANUFACTURING PERFLUOROVINYLETHERS 审中-公开
标题翻译：制备全氟尿嘧啶的方法
公开(公告)号：WO2012104365A3
公开(公告)日：2012-10-04
申请号：PCT/EP2012051730
申请日：2012-02-02
申请人： SOLVAY SPECIALTY POLYMERS IT , MILLEFANTI STEFANO , TORTELLI VITO , MARCHIONNI GIUSEPPE , ALBONETTI STEFANIA , GREGORI MANUEL , FORNASARI GIUSEPPE
发明人： MILLEFANTI STEFANO , TORTELLI VITO , MARCHIONNI GIUSEPPE , ALBONETTI STEFANIA , GREGORI MANUEL , FORNASARI GIUSEPPE
IPC分类号： C07C41/24 , C07C43/17
CPC分类号： C07C41/24 , C07C43/17
摘要： The invention pertains to a process for the manufacture of a perfluorovinylether by hydrodehalogenation of a halofluoroether (HFE) having general formula (l-A) or (l-B): RfO-CRf'X-CRf"Rf"'X' (l-A) wherein Rf represents a C1-C6 perfluoro(oxy)alkyl group; Rf', Rf" and Rf'", equal or different from each other, independently represent fluorine atoms or C1-C5 perfluoro(oxy)alkyl groups; X and X', equal or different from each other, are independently chosen among CI, Br or I; formula (I-B) wherein Rf* and Rf*', equal or different from each other, independently represent fluorine atoms or C1-C3 perfluoro(oxy)alkyl groups; Y1 and Y2, equal or different from each other, independently represent fluorine atoms or C1-C3 perfluoroalkyl groups; X and X' are as above defined; said process comprising contacting said halofluoroether (HFE) with hydrogen in the presence of a catalyst comprising palladium and at least one transition metal (M) selected from the group consisting of the metals of group VIIIB, other than palladium, and of group IB.
摘要翻译：本发明涉及通过具有通式（1A）或（1B）的卤代氟醚（HFE）的加氢脱卤制备全氟乙烯基醚的方法：RfO-CRf'X-CRf“Rf”'X'（1A）其中Rf代表 C1-C6全氟（氧）烷基; Rf'，Rf“和Rf”“彼此相同或不同，独立地表示氟原子或C1-C5全氟（氧）烷基; X和X'彼此相同或不同，独立地选自CI，Br或I; 式（I-B）其中Rf *和Rf *'彼此相同或不同，独立地表示氟原子或C1-C3全氟（氧）烷基; Y1和Y2彼此相同或不同，独立地表示氟原子或C1-C3全氟烷基; X和X'如上所定义; 所述方法包括在催化剂存在下使所述卤代氟醚（HFE）与氢气接触，所述催化剂包含钯和至少一种选自除钯以外的第VIIIB族金属和IB族的过渡金属（M）。

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