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1. 发明申请

WO2007126166A1 METHOD AND APPARATUS FOR PREPARING FATTY ACID ALKYL ESTER USING FATTY ACID 审中-公开
标题翻译：使用脂肪酸制备脂肪酸亚油酸酯的方法和装置
公开(公告)号：WO2007126166A1
公开(公告)日：2007-11-08
申请号：PCT/KR2006/001620
申请日：2006-04-28
申请人： SK CHEMICALS CO., LTD. , CHUN, Shin-Ho , CHO, Hyun-Jun , ROH, Hang-Duk , LIM, Jae-Bong , LEE, Jong-In , MOON, Chan-Woo , KIM, Byung-Hui
发明人： CHUN, Shin-Ho , CHO, Hyun-Jun , ROH, Hang-Duk , LIM, Jae-Bong , LEE, Jong-In , MOON, Chan-Woo , KIM, Byung-Hui
IPC分类号： C10L1/19 , C07C67/29
CPC分类号： C10L1/026 , B01J14/00 , B01J19/006 , B01J19/1818 , B01J19/1875 , B01J2219/00006 , B01J2219/0004 , B01J2219/00768 , B01J2219/0077 , C07C67/08 , C10G2300/1014 , C10G2300/201 , C10G2300/4006 , C10G2300/4012 , C11B3/12 , C11C3/003 , Y02E50/13 , Y02P30/20 , C07C69/24 , C07C69/52
摘要： A method and an apparatus for preparing fatty acid alkyl ester for bio-diesels are disclosed, wherein fatty acid, specifically fatty acid distillate reacts with alcohol, without a catalyst. The method does not require the purification process of the catalyst and glycerin, and has the superior conversion ratio of fatty acid. The method for preparing fatty acid alkyl ester for bio-diesel fuels comprises the step of esterifying fatty acid raw material with alcohol, under a temperature of 200 to 35O0C and a pressure of atmospheric pressure to 10 bar. The apparatus for preparing fatty acid alkyl ester for bio-diesel fuels, comprises: the first reactor for esterifying fatty acid raw material with alcohol under a temperature of 2000C to 35O0C and a pressure of atmospheric pressure to 10 bar and for converting 80 to 90% of total fatty acid into fatty acid alkyl ester; and the second reactor for converting remaining fatty acid unconverted at the first reactor into fatty
摘要翻译：公开了一种制备用于生物柴油的脂肪酸烷基酯的方法和装置，其中脂肪酸特别是脂肪酸馏出物与醇反应而没有催化剂。该方法不需要催化剂和甘油的纯化过程，并且具有优异的脂肪酸转化率。制备用于生物柴油燃料的脂肪酸烷基酯的方法包括在200至350℃的温度和大气压至10巴的压力下用醇酯化脂肪酸原料的步骤。用于制备用于生物柴油燃料的脂肪酸烷基酯的设备包括：第一反应器，其用于在200℃至350℃的温度和10至10巴的压力下用醇酯化脂肪酸原料，并将80至90％的总脂肪酸转化成脂肪酸烷基酯; 以及将在第一反应器未转化的剩余脂肪酸转化为脂肪的第二反应器

2. 发明申请

WO2009123369A1 METHOD FOR PREPARING FATTY ACID ALKYL ESTER USING FATTY ACID 审中-公开
标题翻译：使用脂肪酸制备脂肪酸亚油酸酯的方法
公开(公告)号：WO2009123369A1
公开(公告)日：2009-10-08
申请号：PCT/KR2008/001831
申请日：2008-04-01
申请人： SK CHEMICALS CO., LTD. , CHO, Hyun-Jun , KIM, Byung-Hui , KIM, Soo-Hyun , SHIN, Yong-Jun , CHUN, Shin-Ho
发明人： CHO, Hyun-Jun , KIM, Byung-Hui , KIM, Soo-Hyun , SHIN, Yong-Jun , CHUN, Shin-Ho
IPC分类号： C07C67/03 , C11C3/10 , C10L1/02
CPC分类号： C11C3/003 , C07C67/08 , C10G2300/1011 , Y02E50/13 , Y02P30/20 , C07C69/24 , C07C69/52
摘要： A method for preparing fatty acid alkyl ester for bio-diesels is disclosed, wherein fatty acid, specifically fatty acid distillate reacts with alcohol in the presence of metal catalyst instead of conventional acid or solid acid catalyst. The method does not require the glycerin purification process, and has the superior conversion ratio of fatty acid. The method for preparing fatty acid alkyl ester comprises the step of carrying out an esterification reaction of fatty acid raw material with alcohol in the presence of metal catalyst. Preferably, the esterification reaction is carried out at the temperature of 200 to 35O0C and the pressure of atmospheric pressure to 10 bar, and the metal catalyst is a compound containing metal selected from the group consisting of cobalt, iron, manganese, zinc, titanium and mixture thereof.
摘要翻译：公开了一种制备用于生物柴油的脂肪酸烷基酯的方法，其中脂肪酸特别是脂肪酸馏出物在金属催化剂的存在下代替常规的酸或固体酸催化剂与醇反应。该方法不需要甘油纯化方法，具有优异的脂肪酸转化率。制备脂肪酸烷基酯的方法包括在金属催化剂存在下，进行脂肪酸原料与醇的酯化反应的步骤。优选地，酯化反应在200〜350℃的温度和大气压的压力下进行至10巴，金属催化剂是含有选自钴，铁，锰，锌，钛和钛的金属的化合物，的混合物。

3. 发明公开

EP2348009A2 METHOD AND APPARATUS FOR PREPARING ALKYL ESTER FATTY ACID USING FATTY ACID 审中-公开
标题翻译：方法和设备用于生产ALKYLESTERFETTSÄURE使用脂肪酸链
公开(公告)号：EP2348009A2
公开(公告)日：2011-07-27
申请号：EP09824941.0
申请日：2009-09-22
申请人： SK Chemicals, Co., Ltd. , Cho, Hyun-Jun
发明人： KIM, Soo-Hyun , MOON, Chan-Woo , HAM, Byoung-Kyung , LIM, Jae-Bong , CHO, Hyun-Jun
IPC分类号： C07C67/08
CPC分类号： C07C67/08 , B01J8/0492 , C11C1/08 , C11C3/003 , Y02E50/13 , C07C69/52 , C07C69/24
摘要： A method for preparing fatty acid alkyl ester for bio-diesel fuel is disclosed, wherein fatty acid, specifically fatty acid distillate reacts with alcohol. The method does not require the glycerin purification process, and has the superior conversion ratio of fatty acid. The method for preparing fatty acid alkyl ester for bio-diesel fuel comprises the step of carrying out a counter current type esterification reaction of fatty acid and alcohol in each tray of a counter current column reactor at a temperature of 200 to 350°C and a pressure of 1 to 35 bar. Here the raw material of the fatty acid is fed to an upper part of the counter current column reactor and the alcohol is fed to a lower part of the counter current column reactor. The counter current column reactor has a number of trays which are installed horizontally to have a number of vertical compartments. Each of the number of trays has an opening part at one end thereof to communicate one compartment with an adjoining compartment. The opening parts of two adjoining trays are alternately installed with each other.
摘要翻译：一种用于制备脂肪酸烷基酯的生物柴油燃料的方法是游离缺失盘，worin脂肪酸，特别是脂肪酸馏出物与醇发生反应。该方法不需要甘油纯化过程，具有和脂肪酸的优良转化率，用于制备脂肪酸烷基酯的生物柴油燃料的方法，包括在200〜350℃，的温度下进行以逆流塔式反应器的每个塔板的脂肪酸和醇的逆流型酯化反应的步骤 1至35巴的压力。这里所述的脂肪酸的原料进料至在所述逆流塔式反应器的上部和所述醇进料到逆流塔式反应器的下部。逆流塔式反应器具有许多哪些是水平安装以具有多个垂直的隔室的托盘。每个托盘的数量的具有在一端开口部其与一个隔室到隔室邻接的通信。两个邻接塔板的敞开部分安装或者海誓山盟。

4. 发明授权

EP2013319B1 METHOD FOR PREPARING FATTY ACID ALKYL ESTER USING FATTY ACID DISTILLATE 有权转让
公开(公告)号：EP2013319B1
公开(公告)日：2019-01-23
申请号：EP06757588.6
申请日：2006-04-28
申请人： SK CHEMICALS CO., LTD.
发明人： CHUN, Shin-Ho , CHO, Hyun-Jun , ROH, Hang-Duk , LIM, Jae-Bong , LEE, Jong-In , MOON, Chan-Woo , KIM, Byung-Hui
IPC分类号： C10L1/02 , C07C67/29 , C07C67/08 , C11B3/12 , C11C3/00 , B01J14/00 , B01J19/00 , B01J19/18

5. 发明授权

EP2257518B1 METHOD FOR PREPARING FATTY ACID ALKYL ESTER USING FATTY ACID 有权转让
标题翻译：用于生产使用脂肪的脂肪酸烷基酯
公开(公告)号：EP2257518B1
公开(公告)日：2016-03-09
申请号：EP08741082.5
申请日：2008-04-01
申请人： SK Chemicals Co., Ltd.
发明人： CHO, Hyun-Jun , KIM, Byung-Hui , KIM, Soo-Hyun , SHIN, Yong-Jun , CHUN, Shin-Ho
IPC分类号： C07C67/08 , C11C3/10 , C10L1/02 , C11C3/00
CPC分类号： C11C3/003 , C07C67/08 , C10G2300/1011 , Y02E50/13 , Y02P30/20 , C07C69/24 , C07C69/52

6. 发明公开

EP2257518A1 METHOD FOR PREPARING FATTY ACID ALKYL ESTER USING FATTY ACID 有权转让
标题翻译：用于生产使用脂肪的脂肪酸烷基酯
公开(公告)号：EP2257518A1
公开(公告)日：2010-12-08
申请号：EP08741082.5
申请日：2008-04-01
申请人： SK Chemicals, Co., Ltd.
发明人： CHO, Hyun-Jun , KIM, Byung-Hui , KIM, Soo-Hyun , SHIN, Yong-Jun , CHUN, Shin-Ho
IPC分类号： C07C67/03 , C11C3/10 , C10L1/02
CPC分类号： C11C3/003 , C07C67/08 , C10G2300/1011 , Y02E50/13 , Y02P30/20 , C07C69/24 , C07C69/52
摘要： A method for preparing fatty acid alkyl ester for bio-diesels is disclosed, wherein fatty acid, specifically fatty acid distillate reacts with alcohol in the presence of metal catalyst instead of conventional acid or solid acid catalyst. The method does not require the glycerin purification process, and has the superior conversion ratio of fatty acid. The method for preparing fatty acid alkyl ester comprises the step of carrying out an esterification reaction of fatty acid raw material with alcohol in the presence of metal catalyst. Preferably, the esterification reaction is carried out at the temperature of 200 to 35O0C and the pressure of atmospheric pressure to 10 bar, and the metal catalyst is a compound containing metal selected from the group consisting of cobalt, iron, manganese, zinc, titanium and mixture thereof.

7. 发明公开

EP2013319A1 METHOD AND APPARATUS FOR PREPARING FATTY ACID ALKYL ESTER USING FATTY ACID 有权转让
标题翻译：方法和装置脂肪酸脂肪酸的生产中使用
公开(公告)号：EP2013319A1
公开(公告)日：2009-01-14
申请号：EP06757588.6
申请日：2006-04-28
申请人： SK CHEMICALS CO., LTD.
发明人： CHUN, Shin-Ho , CHO, Hyun-Jun , ROH, Hang-Duk , LIM, Jae-Bong , LEE, Jong-In , MOON, Chan-Woo , KIM, Byung-Hui
IPC分类号： C10L1/19 , C07C67/29
CPC分类号： C10L1/026 , B01J14/00 , B01J19/006 , B01J19/1818 , B01J19/1875 , B01J2219/00006 , B01J2219/0004 , B01J2219/00768 , B01J2219/0077 , C07C67/08 , C10G2300/1014 , C10G2300/201 , C10G2300/4006 , C10G2300/4012 , C11B3/12 , C11C3/003 , Y02E50/13 , Y02P30/20 , C07C69/24 , C07C69/52
摘要： A method and an apparatus for preparing fatty acid alkyl ester for bio-diesels are disclosed, wherein fatty acid, specifically fatty acid distillate reacts with alcohol, without a catalyst. The method does not require the purification process of the catalyst and glycerin, and has the superior conversion ratio of fatty acid. The method for preparing fatty acid alkyl ester for bio-diesel fuels comprises the step of esterifying fatty acid raw material with alcohol, under a temperature of 200 to 350° C. and a pressure of atmospheric pressure to 10 bar. The apparatus for preparing fatty acid alkyl ester for bio-diesel fuels, comprises: the first reactor for esterifying fatty acid raw material with alcohol under a temperature of 200° C. to 350° C. and a pressure of atmospheric pressure to 10 bar and for converting 80 to 90% of total fatty acid into fatty acid alkyl ester; and the second reactor for converting remaining fatty acid unconverted at the first reactor into fatty acid alkyl ester.

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