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1. 发明申请

WO2004110971A3 PROCESSES FOR PREPARING BETA-DIKETONE COMPOUND, METAL COMPLEX THEREOF AND METALLIC COMPOUND 审中-公开
标题翻译：制备β-二酮酮化合物的方法，金属复合物和金属化合物
公开(公告)号：WO2004110971A3
公开(公告)日：2005-02-24
申请号：PCT/JP2004007210
申请日：2004-05-20
申请人： SHOWA DENKO KK , SAITO MAKOTO , UEDA TAKASHI , TANI TAKASHI , NAKAMURA KEIICHI
发明人： SAITO MAKOTO , UEDA TAKASHI , TANI TAKASHI , NAKAMURA KEIICHI
IPC分类号： C07C45/45 , C07C45/77 , C07C45/80 , C07C49/92 , C07C49/12
CPC分类号： C07C49/92 , C07C45/455 , C07C45/77 , C07C45/80 , C07C49/12
摘要： Disclosed is a process for preparing a beta-diketone compound such as 2,6-dimethyl-3,5-heptanedione, which comprises reacting an ester compound such as an alkyl isobutyrate with a ketone compound such as 3-methylbutanone in the presence of an alkali metal alkoxide as a catalyst. The process comprises a step 1 in which an ester compound CR R R COOQ is reacted with a ketone compound CR R R COCH2R7 using an alkali metal alkoxide catalyst to give a beta-diketone compound CR R R COCHR R R . (In the formulae, R is hydrogen or an alkyl group of 1 to 4 carbon atoms while others are each independently hydrogen or an alkyl group of 1 to 3 carbon atoms, and at least one of R to R is hydrogen.)
摘要翻译：公开了一种制备2,6-二甲基-3,5-庚二酮的β-二酮化合物的方法，该方法包括使异氰酸烷基酯等酯化合物与3-甲基丁酮等酮化合物在碱金属醇盐作为催化剂。该方法包括步骤1，其中使用碱金属醇盐催化剂将酯化合物CR 1 R 2 CO 2与酮化合物CR 4 R 5 CO 6 CH 2 R 7反应得到β-二酮化合物CR 1 R 2 R 3 COCHR 4 R 5 R 6。（式中，R 7为氢或碳原子数为1〜4的烷基，其他各自独立地为氢或碳原子数1〜3的烷基，R 1〜R 4中的至少1个为氢原子， 6>是氢。）

2. 发明专利

AU2002356437A1 PROCESS FOR PREPARING -DIKETONE COMPOUND AND PROCESS FOR PREPARING METAL COMPLEX THEREOF 未知
公开(公告)号：AU2002356437A1
公开(公告)日：2003-07-30
申请号：AU2002356437
申请日：2002-12-18
申请人： SHOWA DENKO KK
发明人： SAITO MAKOTO , UEDA TAKASHI , TANI TAKASHI
IPC分类号： C07C45/45 , C07C45/77 , C07C49/12 , C07C49/92
摘要： Disclosed is a process for preparing 2,2,6,6-tetramethyl-3,5-heptanedione, comprising reacting a pivalic acid alkyl ester with pinacolone in the presence of an alkali metal alkoxide catalyst using a pivalic acid alkyl ester as a solvent but using no other solvent or reacting them in an amide type or urea type solvent in the presence of an alkali metal alkoxide catalyst. Also disclosed is a process for preparing a 2,2,6,6-tetramethyl-3,5-heptanesione metal complex using the 2,2,6,6-tetramethyl-3,5-heptanedione obtained by the above process. The process for preparing 2,2,6,6-tetramethyl-3,5-heptanedione is an industrially advantageous process in which an alkali metal alkoxide that is easy to handle can be used as a catalyst for preparing 2,2,6,6-tetramethyl-3,5-heptanedione from a pivalic acid alkyl ester and pinacolone.

3. 发明专利

DE69934033D1 未知
公开(公告)号：DE69934033D1
公开(公告)日：2006-12-28
申请号：DE69934033
申请日：1999-09-23
申请人： SHOWA DENKO KK
发明人： YASUDA HIROSHI , ITO HARUAKI , TANI TAKASHI , OHSHIRO KIMITAKA , SAITO MAKOTO , SOYA SUMIO , MARUMO KUNIOMI
IPC分类号： C07C253/30 , C07C255/57

4. 发明专利

AT345324T 未知
公开(公告)号：AT345324T
公开(公告)日：2006-12-15
申请号：AT04022598
申请日：1999-09-23
申请人： SHOWA DENKO KK
发明人： YASUDA HIROSHI , ITO HARUAKI , TANI TAKASHI , KAWASAKI-KU , OHSHIRO KIMITAKA , SAITO MAKOTO , SOYA SUMIO , MARUMO KUNIOMI
IPC分类号： C07C253/30 , C07C255/57

5. 发明专利

DE69934034D1 未知
公开(公告)号：DE69934034D1
公开(公告)日：2006-12-28
申请号：DE69934034
申请日：1999-09-23
申请人： SHOWA DENKO KK
发明人： YASUDA HIROSHI , ITO HARUAKI , TANI TAKASHI , OHSHIRO KIMITAKA , SAITO MAKOTO , SOYA SUMIO , MARUMO KUNIOMI
IPC分类号： C07C253/30 , C07C255/57

6. 发明专利

DE69934034T2 未知
公开(公告)号：DE69934034T2
公开(公告)日：2007-06-21
申请号：DE69934034
申请日：1999-09-23
申请人： SHOWA DENKO KK
发明人： YASUDA HIROSHI , ITO HARUAKI , TANI TAKASHI , OHSHIRO KIMITAKA , SAITO MAKOTO , SOYA SUMIO , MARUMO KUNIOMI
IPC分类号： C07C253/30 , C07C255/57

7. 发明专利

DE69934033T2 未知
公开(公告)号：DE69934033T2
公开(公告)日：2007-06-21
申请号：DE69934033
申请日：1999-09-23
申请人： SHOWA DENKO KK
发明人： YASUDA HIROSHI , ITO HARUAKI , TANI TAKASHI , OHSHIRO KIMITAKA , SAITO MAKOTO , SOYA SUMIO , MARUMO KUNIOMI
IPC分类号： C07C253/30 , C07C255/57

8. 发明专利

AT345325T 未知
公开(公告)号：AT345325T
公开(公告)日：2006-12-15
申请号：AT04022599
申请日：1999-09-23
申请人： SHOWA DENKO KK
发明人： YASUDA HIROSHI , ITO HARUAKI , TANI TAKASHI , KAWASAKI-KU , OHSHIRO KIMITAKA , SAITO MAKOTO , SOYA SUMIO , MARUMO KUNIOMI
IPC分类号： C07C253/30 , C07C255/57

9. 发明专利

JP2004300575A Metal oxide film deposition method 审中-公开
标题翻译：金属氧化物膜沉积方法
公开(公告)号：JP2004300575A
公开(公告)日：2004-10-28
申请号：JP2004073176
申请日：2004-03-15
申请人： Showa Denko Kk , 昭和電工株式会社
发明人： UEDA TAKASHI , TANI TAKASHI , SAITO MAKOTO
IPC分类号： C01G23/04 , B01J21/06 , B01J35/02 , B01J37/02 , C03C17/245 , C23C16/40
摘要： PROBLEM TO BE SOLVED: To provide a metal oxide film deposition method in which an inexpensive raw material is used, and less vaporization residue is left in an obtained film in a spray thermal decomposition method which is unnecessary for vacuum and easily handled.
SOLUTION: In a method for depositing a metal oxide film on a substrate by the chemical vapor deposition method, aqueous suspension of metal complex compound expressed by a general formula (1) : MX
n Y
(m-n) (where, M denotes metal of valence of 3-5, X denotes β-diketonate ligand, Y denotes alkoxy group, m denotes a positive integer of 3-5, and n denotes a positive integer of 1-4) is sprayed on the heated substrate.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：为了提供一种使用廉价的原料的金属氧化物膜沉积方法，并且对于真空不需要并且容易处理的喷雾热分解方法，在获得的膜中留下较少的汽化残留物。解决方案：在通过化学气相沉积法在基板上沉积金属氧化物膜的方法中，由通式（1）表示的金属络合物的水性悬浮液：MX＆lt; SB＆gt; SB>（mn）（其中，M表示3-5价的金属，X表示β-二酮配体，Y表示烷氧基，m表示正整数3-5，n表示正整数 1-4）喷涂在加热的基底上。版权所有（C）2005，JPO＆NCIPI

10. 发明专利

JP2000119237A PRODUCTION OF CYANOBENZOIC ACID 失效
公开(公告)号：JP2000119237A
公开(公告)日：2000-04-25
申请号：JP28779698
申请日：1998-10-09
申请人： SHOWA DENKO KK
发明人： TANI TAKASHI , SAITO MAKOTO , OSHIRO KIMITAKA
IPC分类号： C07C253/30 , C07C255/57
摘要： PROBLEM TO BE SOLVED: To obtain the subject compound useful as a raw material or an intermediate material of an intermediate of a medicine and an agrochemical, and various fine chemicals under a moderate condition in a high purity by using an easily available and relatively inexpensive phthalonitrile as a raw material. SOLUTION: This method for producing cyanobenzoic acid is to subject a phthalonitrile (preferably terephthalonitrile) of formula I [two nitrile groups are in the meta or para position; X is Cl or F; and (n) is 0-4] under a hydration reaction in an alcoholic solvent in the presence of a base to obtain (A) cyanobenzoic acid amide by converting one of nitriles to an amide, then convert only the amide group of the compound A to carboxyl group by adding (B) an alkaline hypohalogenous acid and/or an alkaline halogenous acid to obtain a cyanobenzoic acid of formula II. Further, as the cyanobenzoic acid amide of the component A, the acid amide prepared by another method is allowed to be used, and the amount of use of the component B is preferably 0.1-12.5 mole based on 1 mole of the component A.

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