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1. 发明授权

EP0564049B1 Process for making hydroxyl functional derivatives of epoxidized diene block copolymers 失效
标题翻译：一种制备环氧化二烯嵌段共聚物的含羟基的衍生物的方法
公开(公告)号：EP0564049B1
公开(公告)日：2001-10-24
申请号：EP93200947.5
申请日：1993-04-02
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Bening, Robert Charles , St. Clair, David John , Flores, Joe Jerry , Erickson, James Robert , Gibler, Carma Joleen , Stark, Charles John
IPC分类号： C08F8/00
CPC分类号： C09D175/04 , C08C19/40 , C08F8/00 , C08G18/6208 , C08F297/00

2. 发明公开

EP0516203A3 Cross-linked epoxy functionalized polydiene block polymers, process to prepare them, adhesive compositions and starting block copolymer 失效
标题翻译：交联的环氧官能化聚酯嵌段聚合物，其制备方法，粘合组合物和起始嵌段共聚物
公开(公告)号：EP0516203A3
公开(公告)日：1993-01-07
申请号：EP92201176.2
申请日：1992-04-27
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Erickson, James Robert , St. Clair, David John
IPC分类号： C08F297/00 , C08F8/08 , C09J153/00 , C09D153/00
CPC分类号： C08G59/027 , C08F8/08 , C08F297/044 , C08F2800/20 , C08F2810/20 , C08J3/28 , C08J2353/00 , C08L63/08 , C09D153/025 , C09J153/025 , C08F297/04 , C08F8/04 , C08F297/046
摘要： A cross-linked adhesive composition is provided comprising an epoxidized diene block polymer wherein the polymer is cross-linked through at least some of the epoxy functionality. A process to prepare this polymer is also provided. The preferred polymer is partially hydrogenated and lightly epoxidized. Furthermore, there is provided a viscous block copolymer from which said epoxidized diene block polymer has been derived.

3. 发明公开

EP0008146A1 Radiation cured adhesive composition 有权
标题翻译：通过辐射可交联的粘合剂组合物。
公开(公告)号：EP0008146A1
公开(公告)日：1980-02-20
申请号：EP79200425.1
申请日：1979-07-30
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： St. Clair, David John , Hansen, David Romme
IPC分类号： C09J3/14 , C08L51/00 , C08L53/02 , C08F287/00 , C08F291/00
CPC分类号： C09J4/06 , C08F291/00 , Y10T428/31692 , Y10T428/31797 , Y10T428/31884 , C08F287/00 , C08F2/02 , C08F2/46
摘要： A radiation cured adhesive composition comprising a two block copolymer and a multiblock copolymer, each copolymer comprising at least one hydrogenated block of a conjugated diene and a monoalkenyl arene polymer block, a tackifying resin and a di-, tri- or tetra ester of acrylic or methacrylic acid and an at least dihydric aliphatic alcohol.

4. 发明授权

EP0698638B1 Crosslinkable waterborne dispersions of hydroxy functional polydiene polymers and amino resins 有权
标题翻译：羟基官能的二烯聚合物和氨基树脂的交联的，水分散体
公开(公告)号：EP0698638B1
公开(公告)日：1998-01-28
申请号：EP95201947.9
申请日：1995-07-14
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： St. Clair, David John , Erickson, James Robert
IPC分类号： C08L19/00 , C08L19/02 , C08L101/06
CPC分类号： C08J3/03 , C08J2319/00 , C08L19/006 , C08L19/02 , C08L61/28 , C08L2666/16

5. 发明公开

EP0632075A2 Liquid star polymers having terminal hydroxyl groups 失效
标题翻译： FlüssigesternförmigePolymere mitendständigenHydroxylgruppen。
公开(公告)号：EP0632075A2
公开(公告)日：1995-01-04
申请号：EP94201852.4
申请日：1994-06-28
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Handlin, Dale Lee, Jr. , Willis, Carl Lesley , Goodwin, Daniel Earl , St. Clair, David John
IPC分类号： C08F297/04 , C08F2/42 , C08F8/00
CPC分类号： C08G18/69 , C08C19/44 , C08F8/04 , C08F297/023 , C08F2800/20 , C08F2810/40 , C08G18/6208 , C08F297/02
摘要： Star polymers of isoprene or butadiene having terminal hydroxyl groups have reduced viscosity when the hydroxyl groups are located on poly-meric arms that are grown from the core of the star molecules. The polymers are useful in making coatings, sealants, and binders.
摘要翻译：当羟基位于从星形分子的核心生长的聚合物臂上时，具有末端羟基的异戊二烯或丁二烯的星形聚合物具有降低的粘度。聚合物可用于制备涂料，密封剂和粘合剂。

6. 发明公开

EP0564049A3 Hydroxyl functional derivatives of epoxidized diene block copolymers and process for making them 失效
标题翻译：环氧化二烯嵌段共聚物的羟基官能衍生物及其制备方法
公开(公告)号：EP0564049A3
公开(公告)日：1994-03-16
申请号：EP93200947.5
申请日：1993-04-02
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Bening, Robert Charles , St. Clair, David John , Flores, Joe Jerry , Erickson, James Robert , Gibler, Carma Joleen , Stark, Charles John
IPC分类号： C08F8/00
CPC分类号： C09D175/04 , C08C19/40 , C08F8/00 , C08G18/6208 , C08F297/00
摘要： A process for making polymers of conjugated dienes containing hydroxyl groups in the diene blocks, which process comprises
(a) making a precursor polymer by polymerizing at least one conjugated diene which leaves 1,2 disubstituted, 1,1 disubstituted, 1,1,2 trisubstituted or tetrasubstituted olefinic unsaturation in the polymer, (b) epoxidizing said precursor polymer such that epoxy groups form at said substituted sites and the amount of epoxy functionality in the polymer is from 0.1 to 5 meq/g polymer, and (c) contacting the epoxidized polymer with an alcohol having one unprotected hydroxyl group and either a compound of general formula MX n , wherein M is selected from the group consisting of hydrogen, boron, aluminium, iron and tin; X is a halogen; and n is an integer corresponding with the valence of M, or an organic complex thereof. A conjugated diene block copolymer containing 0.1 to 15 meq/g polymer of hydroxyl groups, which polymer is comprised of alcohol groups of the formula

wherein P is -OH, -CI or -OR with R being selected from the group consisting of alkyl radicals containing up to 10 carbon atoms, monohydric and dihydric alcohol groups and carbonate groups; Q is -OH or Cl with the proviso that at least one of P and Q is -OH and R 1 and R 2 are hydrogen or alkyl radicals with the proviso that if P is -OR only one of R 1 and R 2 can be hydrogen.
摘要翻译：一种制备二烯嵌段中含有羟基的共轭二烯聚合物的方法，该方法包括（a）通过聚合至少一种共轭二烯制备前体聚合物，该共轭二烯使1,2-二取代的1,1-二取代的1,1,2 （b）环氧化所述前体聚合物，使得在所述取代位置形成环氧基团，并且聚合物中环氧官能团的量为0.1-5meq / g聚合物，和（c）使所述聚合物与所述前体聚合物接触环氧化聚合物与具有一个未保护的羟基的醇和通式MX n的化合物反应，其中M选自氢，硼，铝，铁和锡; X是卤素; 并且n是与M的化合价对应的整数，或其有机配合物。含有0.1至15meq / g羟基聚合物的共轭二烯嵌段共聚物，该聚合物由下式的醇基组成：其中P是-OH，-Cl或-OR，R选自含有至多10个碳原子，一元和二元醇基团和碳酸酯基团; Q是-OH或Cl，条件是P和Q中的至少一个是-OH，并且R 1和R 2是氢或烷基，条件是如果P是-OR，则只有R 1和R 2中的一个可以是氢。

7. 发明公开

EP0632074A3 Viscous conjugated diene block copolymers 失效
标题翻译：共轭二烯的粘性嵌段共聚物。
公开(公告)号：EP0632074A3
公开(公告)日：1998-04-22
申请号：EP94201829.2
申请日：1994-06-24
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Erickson, James Robert , St. Clair, David John
IPC分类号： C08F297/04
CPC分类号： C08G59/027 , C08F8/04 , C08F8/08 , C08F297/023 , C08F297/044 , C08F2800/20 , C08F2810/20 , C08J3/28 , C08J2353/00 , C08L63/08 , C09D153/005 , C09D153/025 , C09J153/005 , C09J153/025 , C08F297/046
摘要： A viscous block copolymer of the formula:
(A-B-A p ) n -Y r -(A q -B) m
wherein Y is a coupling agent or coupling monomers, and wherein A and B are polymer blocks which may be homopolymer blocks of conjugated diene monomers, copolymer blocks of conjugated diene monomers or copolymer blocks of conjugated diene monomers and monoalkenyl aromatic hydrocarbon monomers, and
wherein the A blocks have a greater number of di- and/or tetra-substituted unsaturation sites per unit of block mass than do the B blocks, wherein the number of tertiary unsaturation (TU) sites in the A blocks is lower than or equal to that number of the B blocks and
wherein the A blocks have a molecular weight from 100 to 3000 and the B blocks have a molecular weight from 1000 to 15,000, and wherein p and q are 0 or 1 and n > 0, r is 0 or 1, m ≧ 0 and n + m ranges from 1 to 100.

8. 发明授权

EP0564048B1 A method of chemically cross-linking sterically hindered epoxidized polymers 失效
标题翻译：一种用于位阻环氧化聚合物的化学交联处理
公开(公告)号：EP0564048B1
公开(公告)日：1997-07-16
申请号：EP93200944.2
申请日：1993-04-01
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Bening, Robert Charles , Erickson, James Robert , St. Clair, David John
IPC分类号： C08F8/30 , C08C19/40 , C08G81/02 , C08C19/22
CPC分类号： C08G59/027 , C08C19/40 , C08F8/30 , C08L63/08 , C08L61/20

9. 发明公开

EP0564049A2 Hydroxyl functional derivatives of epoxidized diene block copolymers and process for making them 失效
标题翻译：含羟基的环氧化二烯嵌段共聚物和它们的制备方法的衍生物。
公开(公告)号：EP0564049A2
公开(公告)日：1993-10-06
申请号：EP93200947.5
申请日：1993-04-02
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Bening, Robert Charles , St. Clair, David John , Flores, Joe Jerry , Erickson, James Robert , Gibler, Carma Joleen , Stark, Charles John
IPC分类号： C08F8/00
CPC分类号： C09D175/04 , C08C19/40 , C08F8/00 , C08G18/6208 , C08F297/00
摘要： A process for making polymers of conjugated dienes containing hydroxyl groups in the diene blocks, which process comprises

(a) making a precursor polymer by polymerizing at least one conjugated diene which leaves 1,2 disubstituted, 1,1 disubstituted, 1,1,2 trisubstituted or tetrasubstituted olefinic unsaturation in the polymer,
(b) epoxidizing said precursor polymer such that epoxy groups form at said substituted sites and the amount of epoxy functionality in the polymer is from 0.1 to 5 meq/g polymer, and
(c) contacting the epoxidized polymer with an alcohol having one unprotected hydroxyl group and either a compound of general formula MX n , wherein M is selected from the group consisting of hydrogen, boron, aluminium, iron and tin; X is a halogen; and n is an integer corresponding with the valence of M, or an organic complex thereof.

A conjugated diene block copolymer containing 0.1 to 15 meq/g polymer of hydroxyl groups, which polymer is comprised of alcohol groups of the formula

wherein P is -OH, -CI or -OR with R being selected from the group consisting of alkyl radicals containing up to 10 carbon atoms, monohydric and dihydric alcohol groups and carbonate groups; Q is -OH or Cl with the proviso that at least one of P and Q is -OH and R 1 and R 2 are hydrogen or alkyl radicals with the proviso that if P is -OR only one of R 1 and R 2 can be hydrogen.
摘要翻译：一种用于制造共轭二烯的含羟基基团中的块的服务聚合物的方法，该方法包括方法（a）通过聚合至少一种共轭服务哪个叶1.2二取代，二取代的1,1，1,1,2制作的前体聚合物三取代的或在聚合物中的四取代的烯属不饱和，（b）中环氧化所述的前体聚合物的搜索没有环氧基团形成在所述substituiertem位点和环氧官能团对所述聚合物为0.1〜5毫克当量/克聚合物，和（c）的量联系的与醇有一个未保护羟基和任一个通式为MX n的化合物的环氧化的聚合物中，M选自worin氢，硼，铝，铁和锡中选择的; X是卤素; 并且n是一个整数与M的价数相应的，或它们的有机络合物。的共轭用作嵌段共聚物含有羟基基团的0.1至15毫克当量/克聚合物，该聚合物是由下式的醇基团的 worin P为-OH，-Cl或-OR，其中R为选自的选择烷基含至多10个碳原子，一元和二元醇基团和碳酸酯基团; Q是OH或Cl，其条件没有P的至少一种，且Q是OH和R1和R2是氢或烷基，条件做如果P为-OR仅R 1和R 2可以是氢。

10. 发明公开

EP0564048A2 A method of chemically cross-linking sterically hindered epoxidized polymers 失效
标题翻译： Verfahren zur chemischen Vernetzung von sterisch gehinderten epoxydierten Polymeren。
公开(公告)号：EP0564048A2
公开(公告)日：1993-10-06
申请号：EP93200944.2
申请日：1993-04-01
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Bening, Robert Charles , Erickson, James Robert , St. Clair, David John
IPC分类号： C08F8/30 , C08C19/40 , C08G81/02 , C08C19/22
CPC分类号： C08G59/027 , C08C19/40 , C08F8/30 , C08L63/08 , C08L61/20
摘要： This invention is a method of curing epoxidized diene polymers which do not have a significant amount of functional groups which undergo a cross-linking reaction with amino resins and which have at least 50 olefinic epoxy groups which are predominately sterically hindered and which comprise at least one conjugated diolefin monomer, said method comprising mixing said polymer with an amino resin in the presence of a proton-donating acid catalyst.
摘要翻译：本发明是一种固化环氧化二烯聚合物的方法，其不具有与氨基树脂进行交联反应的显着量的官能团，并且具有至少50个主要由空间位阻的烯属环氧基组成，并且包含至少一个共轭二烯单体，所述方法包括在质子递送酸催化剂存在下将所述聚合物与氨基树脂混合。

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