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1. 发明授权

US08877381B2 Production process for composite oxide, positive-electrode active material for lithium-ion secondary battery and lithium-ion secondary battery 有权
标题翻译：复合氧化物，锂离子二次电池正极活性物质和锂离子二次电池的生产工艺
公开(公告)号：US08877381B2
公开(公告)日：2014-11-04
申请号：US13580613
申请日：2011-03-07
申请人： Naoto Yasuda , Hitotoshi Murase , Ryota Isomura
发明人： Naoto Yasuda , Hitotoshi Murase , Ryota Isomura
IPC分类号： H01M4/13 , H01M4/50 , H01M4/505 , C01G45/12 , B82Y30/00
CPC分类号： H01M4/505 , B82Y30/00 , C01G45/1257 , C01P2002/72 , C01P2004/62 , C01P2004/64 , Y02E60/122 , Y02P70/54 , Y10S977/773
摘要： A composite oxide is produced via the following: a raw-material mixture preparation step of preparing a raw-material mixture by mixing a metallic-compound raw material and a molten-salt raw material with each other, the metallic-compound raw material at least including one or more kinds of Mn-containing metallic compounds being selected from the group consisting of oxides, hydroxides and metallic salts that include one or more kinds of metallic elements in which Mn is essential, the molten-salt raw material including lithium hydroxide and lithium nitrate, and exhibiting a proportion of the lithium hydroxide with respect to the lithium nitrate (i.e., (Lithium Hydroxide)/(Lithium Nitrate)) that falls in a range of from 0.05 or more to less than 1 by molar ratio; a molten reaction step of reacting said raw-material mixture at from 300° C. or more to 550° C. or less by melting it: and a recovery step of recovering said composite oxide being generated from said raw-material mixture that has undergone the reaction.
摘要翻译：复合氧化物通过以下方式制造：原料混合物制备步骤，通过将金属化合物原料和熔融盐原料彼此混合来制备原料混合物，至少金属化合物原料包括一种或多种选自包括Mn为必需的一种或多种金属元素的氧化物，氢氧化物和金属盐的含Mn金属化合物，包括氢氧化锂和锂的熔融盐原料并且相对于以摩尔比在0.05以上且小于1的范围内的硝酸锂（即，（氢氧化锂）/（硝酸锂））表现出一定比例的氢氧化锂。将原料混合物在300℃以上550℃以下的熔融反应的熔融反应工序进行熔融反应的工序;回收上述复合氧化物的回收工序，反应。

2. 发明授权

US09039926B2 Production process for composite oxide, positive-electrode active material for lithium-ion secondary battery and lithium-ion secondary battery 有权
标题翻译：复合氧化物，锂离子二次电池正极活性物质和锂离子二次电池的生产工艺
公开(公告)号：US09039926B2
公开(公告)日：2015-05-26
申请号：US13577523
申请日：2011-02-07
申请人： Ryota Isomura , Hitotoshi Murase , Naoto Yasuda
发明人： Ryota Isomura , Hitotoshi Murase , Naoto Yasuda
IPC分类号： H01M4/88 , H01M4/505 , C01G45/12 , B82Y30/00 , H01M10/0525
CPC分类号： H01M4/505 , B82Y30/00 , C01G45/1228 , C01P2002/54 , C01P2002/72 , C01P2002/76 , C01P2004/61 , C01P2004/64 , C01P2006/40 , H01M10/0525 , H01M2220/20 , Y02E60/122 , Y02P70/54 , Y02T10/7011
摘要： A production process for composite oxide expressed by a compositional formula: LiMn1-xAxO2, where “A” is one or more kinds of metallic elements other than Mn; and 0≦“x”
摘要翻译：由组成式LiMn1-xAxO2表示的复合氧化物的制造方法，其中“A”是除Mn以外的一种以上的金属元素; 并且通过将金属化合物原料和熔融盐原料混合而制备原料混合物而获得的0＆lt; nlE;“x”<1，所述金属化合物原料至少含有含Mn的硝酸盐其中包括其中Mn是必需的一种或多种金属元素，包括氢氧化锂和硝酸锂的熔融盐原料，并且显示相对于氢氧化锂（硝酸锂/氢氧化锂）的一部分硝酸锂，其中以摩尔比为1以上3以下的范围; 通过熔化使原料混合物在500℃以下反应; 并回收由经历反应的原料混合物产生的复合氧化物。

3. 发明申请

US20130017449A1 POSITIVE-ELECTRODE ACTIVE MATERIAL FOR LITHIUM-ION SECONDARY BATTERY AND LITHIUM-ION SECONDARY BATTERY 审中-公开
标题翻译：用于锂离子二次电池和锂离子二次电池的正极电极活性材料
公开(公告)号：US20130017449A1
公开(公告)日：2013-01-17
申请号：US13637868
申请日：2011-04-04
申请人： Naoto Yasuda , Hitotoshi Murase , Ryota Isomura , Toru Abe
发明人： Naoto Yasuda , Hitotoshi Murase , Ryota Isomura , Toru Abe
IPC分类号： H01M4/36 , H01M4/583 , H01B1/00 , H01M4/525 , H01M4/505 , H01M4/485 , H01M4/02 , H01M4/38
CPC分类号： H01M4/362 , H01M4/505 , H01M4/525 , H01M10/052
摘要： The present invention is characterized in that it is a positive-electrode active material for lithium-ion secondary battery, the positive-electrode active material being capable of absorbing and releasing lithium; it includes the following at least: a first compound exhibiting an irreversible capacity; and a second compound being capable of absorbing more lithium than an amount of lithium that has been released at the time of first-round charging; and it exhibits an irreversible capacity decreasing as a whole of active material.An irreversible capacity of the resulting positive-electrode active material can be reduced by combining the specific compounds to use.
摘要翻译：本发明的特征在于它是用于锂离子二次电池的正极活性材料，正极活性材料能够吸收和释放锂; 它至少包括：呈现不可逆容量的第一化合物; 以及能够吸收比在第一次充电时释放的锂量多的锂的第二化合物; 并且其表现出作为整体活性材料的不可逆容量的降低。可以通过组合使用的具体化合物来降低所得正极活性物质的不可逆容量。

4. 发明申请

US20120321954A1 PRODUCTION PROCESS FOR COMPOSITE OXIDE, POSITIVE-ELECTRODE ACTIVE MATERIAL FOR LITHIUM-ION SECONDARY BATTERY AND LITHIUM-ION SECONDARY BATTERY 有权
标题翻译：用于锂离子二次电池和锂离子二次电池的复合氧化物，正电极活性材料的生产工艺
公开(公告)号：US20120321954A1
公开(公告)日：2012-12-20
申请号：US13577523
申请日：2011-02-07
申请人： Ryota Isomura , Hitotoshi Murase , Naoto Yasuda
发明人： Ryota Isomura , Hitotoshi Murase , Naoto Yasuda
IPC分类号： H01M4/505 , H01M4/54 , H01M4/525
CPC分类号： H01M4/505 , B82Y30/00 , C01G45/1228 , C01P2002/54 , C01P2002/72 , C01P2002/76 , C01P2004/61 , C01P2004/64 , C01P2006/40 , H01M10/0525 , H01M2220/20 , Y02E60/122 , Y02P70/54 , Y02T10/7011
摘要： The present invention is a production process for composite oxide being expressed by a compositional formula: LiMn1-xAxO2 (where “A” is one or more kinds of metallic elements other than Mn; and 0≦“x”
摘要翻译：本发明是由组成式LiMn1-xAxO2（其中A是除Mn以外的一种或多种金属元素，0＆lt; NlE; x <1）表示的复合氧化物的制造方法，并且通过以下：通过将金属化合物原料和熔融盐原料混合而制备原料混合物的原料混合物制备工序，所述金属化合物原料至少含有含Mn的硝酸盐其包括其中Mn是必需的一种或多种金属元素，包括氢氧化锂和硝酸锂的熔融盐原料，并且显示相对于氢氧化锂的硝酸锂的比例（即，（硝酸锂）/ （氢氧化锂）），其摩尔比为1以上3以下的范围; 将原料混合物在500℃以下进行熔融反应的熔融反应工序和回收从经历反应的原料混合物生成的复合氧化物的回收工序。

5. 发明申请

US20120315544A1 PRODUCTION PROCESS FOR COMPOSITE OXIDE, POSITIVE-ELECTRODE ACTIVE MATERIAL FOR LITHIUM-ION SECONDARY BATTERY AND LITHIUM-ION SECONDARY BATTERY 有权
标题翻译：用于锂离子二次电池和锂离子二次电池的复合氧化物，正电极活性材料的生产工艺
公开(公告)号：US20120315544A1
公开(公告)日：2012-12-13
申请号：US13580613
申请日：2011-03-07
申请人： Naoto Yasuda , Hitotoshi Murase , Ryota Isomura
发明人： Naoto Yasuda , Hitotoshi Murase , Ryota Isomura
IPC分类号： H01M4/505 , C01G45/02 , B82Y30/00
CPC分类号： H01M4/505 , B82Y30/00 , C01G45/1257 , C01P2002/72 , C01P2004/62 , C01P2004/64 , Y02E60/122 , Y02P70/54 , Y10S977/773
摘要： A composite oxide is produced via the following: a raw-material mixture preparation step of preparing a raw-material mixture by mixing a metallic-compound raw material and a molten-salt raw material with each other, the metallic-compound raw material at least including one or more kinds of Mn-containing metallic compounds being selected from the group consisting of oxides, hydroxides and metallic salts that include one or more kinds of metallic elements in which Mn is essential, the molten-salt raw material including lithium hydroxide and lithium nitrate, and exhibiting a proportion of the lithium hydroxide with respect to the lithium nitrate (i.e., (Lithium Hydroxide)/(Lithium Nitrate)) that falls in a range of from 0.05 or more to less than 1 by molar ratio; a molten reaction step of reacting said raw-material mixture at from 300° C. or more to 550° C. or less by melting it: and a recovery step of recovering said composite oxide being generated from said raw-material mixture that has undergone the reaction.
摘要翻译：复合氧化物通过以下方式制造：原料混合物制备步骤，通过将金属化合物原料和熔融盐原料彼此混合来制备原料混合物，至少金属化合物原料包括一种或多种选自包括Mn为必需的一种或多种金属元素的氧化物，氢氧化物和金属盐的含Mn金属化合物，包括氢氧化锂和锂的熔融盐原料并且相对于以摩尔比在0.05以上且小于1的范围内的硝酸锂（即，（氢氧化锂）/（硝酸锂））表现出一定比例的氢氧化锂。将原料混合物在300℃以上550℃以下的熔融反应的熔融反应工序进行熔融反应的工序;回收上述复合氧化物的回收工序，反应。

6. 发明申请

US20130171525A1 PRODUCTION PROCESS FOR COMPOSITE OXIDE, POSITIVE-ELECTRODE ACTIVE MATERIAL FOR SECONDARY BATTERY AND SECONDARY BATTERY 审中-公开
标题翻译：复合氧化物的生产工艺，二次电池和二次电池的正极电极活性材料
公开(公告)号：US20130171525A1
公开(公告)日：2013-07-04
申请号：US13820961
申请日：2011-08-06
申请人： Naoto Yasuda , Toru Abe , Ryota Isomura
发明人： Naoto Yasuda , Toru Abe , Ryota Isomura
IPC分类号： H01M4/1391 , H01M4/131 , H01M4/04 , C30B9/00
CPC分类号： H01M4/1391 , B82Y30/00 , C01G45/12 , C01G45/1228 , C01G45/125 , C01G51/56 , C01G53/50 , C01P2002/72 , C01P2004/64 , C01P2006/40 , C30B9/00 , H01M4/0471 , H01M4/0497 , H01M4/131 , H01M4/505 , H01M10/052
摘要： A production process according to the present invention is a novel production process for composite oxide, production process whose a major product is a lithium-manganese-based oxide that includes at least the following: a lithium (Li) element; and a tetravalent manganese (Mn) element, and lithium-manganese-based oxide whose crystal structure belongs to a layered rock-salt structure; said composite oxide is obtained via the following: a molten reaction step of reacting at least the following one another: a metal-containing raw material; and a molten-salt raw material at a melting point of the molten-salt raw material or more, the metal-containing raw material including one or more kinds of metallic elements in which Mn is essential, the molten-salt raw material including lithium hydroxide but not including any other compound virtually, and the molten-salt raw material including Li in an amount that exceeds a theoretical composition of Li being included in said composite oxide to be targeted; and a recovery step of recovering said composite oxide being generated at said molten reaction step.
摘要翻译：本发明的制造方法是一种新型的复合氧化物的制造方法，其制造方法主要是至少包括以下的锂锰系氧化物：锂（Li）元素，和四价锰（Mn）元素和晶体结构属于层状岩盐结构的锂锰氧化物; 所述复合氧化物通过以下方式获得：使至少彼此反应的熔融反应步骤：含金属的原料; 以及熔融盐原料的熔点以上的熔融盐原料，含有金属的原料含有Mn为必需的一种或多种金属元素，熔融盐原料包括氢氧化锂但实际上不包括任何其他化合物，并且包含Li的熔融盐原料的量超过所述待复制氧化物中的Li的理论组成，以及回收在所述熔融反应步骤中产生的所述复合氧化物的回收步骤。

7. 发明申请

US20120282526A1 PRODUCTION PROCESS FOR COMPOSITE OXIDE, POSITIVE-ELECTRODE ACTIVE MATERIAL FOR LITHIUM-ION SECONDARY BATTERY AND LITHIUM-ION SECONDARY BATTERY 审中-公开
标题翻译：用于锂离子二次电池和锂离子二次电池的复合氧化物，正电极活性材料的生产工艺
公开(公告)号：US20120282526A1
公开(公告)日：2012-11-08
申请号：US13519077
申请日：2010-12-20
申请人： Naoto Yasuda , Ryota Isomura
发明人： Naoto Yasuda , Ryota Isomura
IPC分类号： H01M4/505
CPC分类号： H01M4/505 , B82Y30/00 , C01G45/1228 , C01G45/1257 , C01G51/42 , C01G51/50 , C01G53/50 , C01P2002/52 , C01P2002/72 , C01P2002/77 , C01P2004/64 , C01P2004/80 , C01P2006/40 , H01M10/052 , H01M10/0568 , Y02E60/122 , Y02P70/54
摘要： A composite oxide, whose major component is a lithium-manganese-system oxide including Li and tetravalent Mn at least and having a crystal structure that belongs to a layered rock-salt structure, is produced via the following: a raw-material mixture preparation step of preparing a raw-material mixture by mixing a metallic-compound raw material and a molten-salt raw material with each other, the metallic-compound raw material at least including one or more kinds of metallic compounds being selected from the group consisting of oxides, hydroxides and metallic salts that include one or more kinds of metallic elements in which Mn is essential, the molten-salt raw material including lithium hydroxide and lithium nitrate, and exhibiting a proportion of the lithium hydroxide with respect to the lithium nitrate (i.e., (Lithium Hydroxide)/(Lithium Nitrate)) that falls in a range of from 1 or more to 10 or less by molar ratio; a molten reaction step of reacting said raw-material mixture at a melting point of said molten-salt raw material or more by melting it: and a recovery step of recovering said composite oxide being generated from said raw-material mixture that has undergone the reaction.
摘要翻译：通过以下方式制造其主要成分是包含Li和至少具有属于层状岩盐结构的晶体结构的四价Mn的锂 - 锰系氧化物的复合氧化物，原料混合物制备工序通过将金属化合物原料和熔融盐原料混合而制备原料混合物，所述金属化合物原料至少包含一种或多种选自氧化物的金属化合物包括其中Mn为必需的一种或多种金属元素的氢氧化物和金属盐，包括氢氧化锂和硝酸锂的熔融盐原料，并且显示相对于硝酸锂的一部分氢氧化锂（即，（氢氧化锂）/（硝酸锂）），其摩尔比为1以上10以下的范围; 熔融反应步骤，使所述原料混合物在所述熔融盐原料的熔点以上进行熔融反应;和从所述原料混合物中反应生成的复合氧化物的回收步骤，。

8. 发明申请

US20140134491A1 LITHIUM CONTAINING COMPOSITE OXIDE POWDER AND MANUFACTURING PROCESS FOR THE SAME 审中-公开
标题翻译：含锂复合氧化物粉末及其制造方法
公开(公告)号：US20140134491A1
公开(公告)日：2014-05-15
申请号：US14128744
申请日：2012-06-22
申请人： Yuki Sugimoto , Naoto Yasuda , Fumiya Kanetake , Hideaki Shinoda , Manabu Miyoshi , Kyoichi Kinoshita , Toru Abe
发明人： Yuki Sugimoto , Naoto Yasuda , Fumiya Kanetake , Hideaki Shinoda , Manabu Miyoshi , Kyoichi Kinoshita , Toru Abe
IPC分类号： H01M4/505 , C30B9/06
CPC分类号： H01M4/505 , C01G45/125 , C01G51/42 , C01G53/42 , C01G53/50 , C01P2002/52 , C01P2002/72 , C01P2002/88 , C01P2004/03 , C01P2004/04 , C01P2004/61 , C01P2006/12 , C30B9/06 , H01M4/525
摘要： Provided is a lithium containing composite oxide powder suitable for the positive electrode active material of the non-aqueous electrolysis solution secondary battery such as the lithium ion secondary battery, and a manufacturing process for the same. A lithium containing composite oxide powder includes a single crystal particle containing a lithium containing composite oxide that is manufactured by a molten salt method and that includes at least lithium and another one or more metal elements and in which a crystal structure belongs to a lamellar rock salt structure, wherein an average primary particle diameter is greater than or equal to 200 nm and smaller than or equal to 30 μm. The lithium containing composite oxide powder is grown by reacting the metal containing ingredient in the molten salt of the lithium hydroxide at a reaction temperature of higher than or equal to 650° C. and lower than or equal to 900° C.
摘要翻译：本发明提供适用于锂离子二次电池等非水电解液二次电池的正极活性物质的锂复合氧化物粉末及其制造方法。含锂复合氧化物粉末包括含有通过熔融盐法制造的含锂复合氧化物的单晶颗粒，其至少包含锂和另一种一种或多种金属元素，并且其中晶体结构属于层状岩盐结构，其中平均一次粒径大于或等于200nm且小于或等于30μm。含锂复合氧化物粉末通过使氢氧化锂的熔融盐中的金属成分在高于或等于650℃且低于或等于900℃的反应温度下反应而生长。

9. 发明申请

US20120321955A1 LITHIUM-ION SECONDARY BATTERY 审中-公开
标题翻译：锂离子二次电池
公开(公告)号：US20120321955A1
公开(公告)日：2012-12-20
申请号：US13581355
申请日：2011-04-01
申请人： Naoto Yasuda , Toru Abe , Junichi Niwa
发明人： Naoto Yasuda , Toru Abe , Junichi Niwa
IPC分类号： H01M4/505 , H01M4/485 , H01M4/52 , H01M4/54
CPC分类号： H01M4/505 , H01M4/131 , H01M4/386 , H01M4/387 , H01M4/525 , H01M4/587 , H01M10/052 , Y02T10/7011
摘要： A lithium-ion secondary battery is characterized in that it is equipped with: a positive electrode comprising a positive-electrode active material that includes a lithium-transition metal composite oxide including at least lithium and manganese and possessing a layered rock-salt structure; a negative electrode comprising a negative-electrode active material that includes at least one kind of carbon-based materials, silicon-based materials, and tin-based materials; and a non-aqueous electrolytic solution, wherein: said lithium-transition metal composite oxide exhibits an irreversible capacity; and an actual capacity of said negative electrode at the time of first-round charging up to 0 V with respect to metallic lithium is smaller than an actual capacity of said positive electrode at the time of first-round charging up to 4.7 V with respect to metallic lithium. Even when an employment amount of the active materials is reduced less than those conventional amounts, the resulting battery capacity hardly declines.
摘要翻译：锂离子二次电池的特征在于，其具备：包含正极活性物质的正极，所述正极活性物质包括至少包含锂和锰的锂 - 过渡金属复合氧化物，并具有层状岩盐结构; 包含负极活性物质的负极，所述负极活性物质包含至少一种碳类材料，硅类材料和锡类材料; 和非水电解液，其中：所述锂 - 过渡金属复合氧化物具有不可逆容量; 并且相对于金属锂在第一次充电至0V时的所述负极的实际容量小于相对于第一次充电高达4.7V时的所述正极的实际容量金属锂。即使活性物质的使用量比常规量减少，所得电池容量几乎不下降。

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