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1. 发明授权

US07998320B2 Coated article with high visible transmission and low emissivity 有权
公开(公告)号：US07998320B2
公开(公告)日：2011-08-16
申请号：US11086327
申请日：2005-03-23
申请人： Ronald E. Laird , Carole Laird, legal representative , Uwe Kriltz
发明人： Ronald E. Laird , Uwe Kriltz
IPC分类号： C23C14/34
CPC分类号： C03C17/3636 , C03C17/36 , C03C17/3618 , C03C17/3626 , C03C17/3639 , C03C17/3644 , C03C17/366 , C03C2217/78 , Y10T428/12896
摘要： A coated article that can be used in applications such as insulating glass (IG) units, so that resulting IG units can achieve high visible transmission of at least 70% (e.g., when using clear glass substrates from 1.0 to 3.5 mm thick), combined with at least one of: (a) SHGC no greater than about 0.45, more preferably no greater than about 0.40; (b) SC no greater than about 0.49, more preferably no greater than about 0.46; (c) chemical and/or mechanical durability; (d) neutral transmissive color such that transmissive a* is from −5.0 to 0 (more preferably from −3.5 to −1.5), and transmissive b* is from −2.0 to 4.0 (more preferably from 1.0 to 3.0); and (e) neutral reflective color from the exterior of the IG unit (i.e., Rg/Rout) such that reflective a* is from −3.0 to 2.0 (more preferably from −2.0 to 0.5), and reflective b* is from −5.0 to 1.0 (more preferably from −4.0 to −1.0). In certain example non-limiting embodiments, coated articles herein comprise: substrate/TiOx/ZnOx/Ag/NiCrOx/SnOx/ZnOx/Ag/NiCrOx/SnOx/SixNy.

2. 发明授权

US08101278B2 Coated article with absorbing layer 有权
标题翻译：涂层制品与吸收层
公开(公告)号：US08101278B2
公开(公告)日：2012-01-24
申请号：US11898557
申请日：2007-09-13
申请人： Ronald E. Laird , Carole Laird, legal representative
发明人： Ronald E. Laird
IPC分类号： B32B17/06
CPC分类号： C03C17/36 , C03C17/3626 , C03C17/3639 , C03C17/3652 , C03C17/366 , C03C17/3681 , Y10T428/12576 , Y10T428/261 , Y10T428/265
摘要： A coated article is provided with an absorbing layer(s). The coating is, in certain example embodiments, designed so that significant changes in visible transmission can be made by adjusting thickness of the absorbing layer without significantly affecting certain other characteristics such as certain color values. Such coated articles may be used monolithically or in the context of insulating glass (IG) units in different embodiments of this invention, and may or may not be heat treated.
摘要翻译：涂覆制品设置有吸收层。在某些示例性实施例中，涂层被设计成使得可以通过调节吸收层的厚度而不显着影响某些其他特性（例如某些颜色值）来进行可见透射的显着变化。这种涂覆制品可以在本发明的不同实施方案中一体地使用或在绝缘玻璃（IG）单元的上下文中使用，并且可以或可以不进行热处理。

3. 发明授权

US08226803B2 Heat treatable coated article with zinc oxide inclusive contact layer(s) 有权
标题翻译：具有含氧化锌的接触层的可热处理涂层制品
公开(公告)号：US08226803B2
公开(公告)日：2012-07-24
申请号：US12801850
申请日：2010-06-29
申请人： George Neuman , Philip J. Lingle , Ronald E. Laird , Thomas A Seder , Grzegorz Stachowiak
发明人： George Neuman , Philip J. Lingle , Ronald E. Laird , Thomas A Seder , Grzegorz Stachowiak
IPC分类号： C23C14/34
CPC分类号： C03C17/3618 , B32B17/10174 , C03C17/36 , C03C17/3626 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C2217/78 , C03C2218/154
摘要： A coated article is provided so as to have a fairly high visible transmission (TY or Tvis) to sheet resistance (Rs) ratio (i.e., a ratio Tvis/Rs). The higher this ratio, the better the coated article's combined functionality of providing for both good solar performance (e.g., ability to reflect and/or absorb IR radiation) and high visible transmission. In certain example embodiments, coated articles herein may be heat treatable. Coated articles herein may be used in the context of insulating glass (IG) window units, architectural or residential monolithic window units, vehicle window units, and/or the like.
摘要翻译：提供涂层制品以具有相当高的可见透射率（TY或Tvis）至薄层电阻（Rs）比（即比率Tvis / Rs）。该比例越高，涂层制品提供良好的太阳能性能（例如，反射和/或吸收IR辐射的能力）和高可见透射率的组合功能越好。在某些示例性实施方案中，本文的涂覆制品可以是可热处理的。本文中的涂层制品可用于中空玻璃（IG）窗单元，建筑或住宅单片窗单元，车窗单元等的上下文中。

4. 发明授权

US07005190B2 Heat treatable coated article with reduced color shift at high viewing angles 有权
标题翻译：在高视角下减少颜色偏移的可热处理涂层制品
公开(公告)号：US07005190B2
公开(公告)日：2006-02-28
申请号：US10324093
申请日：2002-12-20
申请人： Ronald E. Laird
发明人： Ronald E. Laird
IPC分类号： B32B9/00
CPC分类号： C03C17/3618 , C03C17/36 , C03C17/3626 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C17/3694
摘要： A coated article is provided so as to have fairly neutral a* and/or b* color values at high viewing angles such as 45 and/or 60 degrees off-axis. In certain example embodiments, the neutral a* and/or b* values at high viewing angles (VA) are caused by lessening the thickness of a bottom titanium oxide layer. Coated articles herein may be used in the context of insulating glass (IG) window units, or in other suitable applications.
摘要翻译：提供涂层制品，以便在高视角（例如离轴45度和/或60度）处具有相当中性的*和/或b *颜色值。在某些示例性实施例中，在高视角（VA）下的中性a *和/或b *值是通过减小底部氧化钛层的厚度引起的。本文中的涂层制品可用于中空玻璃（IG）窗单元或其它合适应用中。

5. 发明授权

US06787005B2 Methods of making coated articles by sputtering silver in oxygen inclusive atmosphere 有权
标题翻译：通过在包含氧气的气氛中溅射银制造涂层制品的方法
公开(公告)号：US06787005B2
公开(公告)日：2004-09-07
申请号：US10243952
申请日：2002-09-16
申请人： Ronald E. Laird , George Neuman , Philip J. Lingle , Jean-Marc Lemmer , Keith H. Schillinger
发明人： Ronald E. Laird , George Neuman , Philip J. Lingle , Jean-Marc Lemmer , Keith H. Schillinger
IPC分类号： C23C1434
CPC分类号： C03C17/3423 , B32B17/10036 , B32B17/10174 , B32B17/10761 , B32B27/34 , C03C17/36 , C03C17/3618 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C2217/78 , C23C14/0063 , C23C14/0084 , C23C14/08 , C23C14/185
摘要： A sputter coated article is provided with improved mechanical durability (e.g., pre-HT scratch resistance) and/or thermal stability by sputtering at least one Ag inclusive layer in an atmosphere including at least O2 gas. For instance, in certain example embodiments an Ag inclusive target may be sputtered in an atmosphere including a combination of Ar and O2 gas. In certain embodiments, this enables the resulting AgOx infrared (IR) reflecting layer to better adhere to adjacent contact layer(s).
摘要翻译：通过在至少包括O 2气体的气氛中溅射至少一种含Ag的层，提供具有改进的机械耐久性（例如，预HT耐刮擦性）和/或热稳定性的溅射涂覆制品。例如，在某些示例性实施方案中，包含Ag的靶标可以在包括Ar和O 2气体的组合的气氛中溅射。在某些实施例中，这使得所得到的AgOx红外（IR）反射层更好地粘附到相邻的接触层。

6. 发明申请

US20100276274A1 Heat treatable coated article with zinc oxide inclusive contact layer(s) 有权
标题翻译：具有含氧化锌的接触层的可热处理涂层制品
公开(公告)号：US20100276274A1
公开(公告)日：2010-11-04
申请号：US12801850
申请日：2010-06-29
申请人： George Neuman , Philip J. Lingle , Ronald E. Laird , Thomas A. Seder , Grzegorz Stachowiak
发明人： George Neuman , Philip J. Lingle , Ronald E. Laird , Thomas A. Seder , Grzegorz Stachowiak
IPC分类号： C03C17/34 , C23C14/08 , C23C14/34
CPC分类号： C03C17/3618 , B32B17/10174 , C03C17/36 , C03C17/3626 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C2217/78 , C03C2218/154
摘要： A coated article is provided so as to have a fairly high visible transmission (TY or Tvis) to sheet resistance (Rs) ratio (i.e., a ratio Tvis/Rs). The higher this ratio, the better the coated article's combined functionality of providing for both good solar performance (e.g., ability to reflect and/or absorb IR radiation) and high visible transmission. In certain example embodiments, coated articles herein may be heat treatable. Coated articles herein may be used in the context of insulating glass (IG) window units, architectural or residential monolithic window units, vehicle window units, and/or the like.
摘要翻译：提供涂层制品以具有相当高的可见透射率（TY或Tvis）至薄层电阻（Rs）比（即比率Tvis / Rs）。该比例越高，涂层制品提供良好的太阳能性能（例如，反射和/或吸收IR辐射的能力）和高可见透射率的组合功能越好。在某些示例性实施方案中，本文的涂覆制品可以是可热处理的。本文中的涂层制品可用于中空玻璃（IG）窗单元，建筑或住宅单片窗单元，车窗单元等的上下文中。

7. 发明授权

US06623846B2 Low-emissivity glass coatings having a layer of nitrided nichrome and methods of making same 无效
标题翻译：具有一层氮化镍铬合金的低辐射玻璃涂层及其制造方法
公开(公告)号：US06623846B2
公开(公告)日：2003-09-23
申请号：US09797903
申请日：2001-03-05
申请人： Ronald E. Laird
发明人： Ronald E. Laird
IPC分类号： B32B1706
CPC分类号： C03C17/3618 , C03C17/36 , C03C17/3626 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3694 , C03C2217/78 , Y10T428/24975 , Y10T428/265
摘要： Low-E glass coated glass articles are comprised of a glass substrate and a multiple layer coating on a surface of the glass substrate. Relatively high light transmissivity of greater than about 72% and satisfactory color characteristics are achieved. The coating includes a layer of a transparent dielectric material adjacent the surface of the glass substrate, and respective layers of nitrided nichrome and silver each of which are formed by sputter-coating onto the glass substrate in a nitrogen-containing atmosphere. Most preferably, the coating also includes a layer of silicon oxynitride interposed between the layer of dielectric material and the layer of nitrided nichrome. The silicon oxynitride layer may include an oxygen gradient layer wherein the concentration of oxygen decreases from one location in the silicon oxynitride layer to another location at a different depth in that same layer. If present, the oxygen gradient is most preferably such that the greater amount of oxygen concentration is nearer the bottom of the layer (i.e., towards the glass substrate) with the lesser amount of oxygen concentration being nearer the top of the layer (i.e., away from the glass layer).
摘要翻译： Low-E玻璃涂层玻璃制品由玻璃基板和玻璃基板表面上的多层涂层构成。实现了大于约72％的高透光率和令人满意的颜色特性。该涂层包括邻近玻璃基板表面的透明电介质材料层，以及各自的氮化镍铬合金层和银层，其各自通过在含氮气氛中溅射涂覆在玻璃基板上形成。最优选地，涂层还包括置于介电材料层和氮化镍铬合金层之间的氮氧化硅层。氧氮化硅层可以包括氧气梯度层，其中氧浓度从氧氮化硅层中的一个位置降低到同一层中不同深度的另一个位置。如果存在氧气梯度，则最优选地，氧浓度越大，层的底部越接近玻璃基底（即朝向玻璃基底），氧浓度越接近层的顶部（即，离开从玻璃层）。

8. 发明授权

US5563734A Durable low-emissivity solar control thin film coating 失效
标题翻译：耐用的低辐射太阳能控制薄膜涂层
公开(公告)号：US5563734A
公开(公告)日：1996-10-08
申请号：US337686
申请日：1994-11-10
申请人： Jesse D. Wolfe , Abraham I. Belkind , Ronald E. Laird
发明人： Jesse D. Wolfe , Abraham I. Belkind , Ronald E. Laird
IPC分类号： G02B1/10 , C03C17/36 , G02B5/28 , F21V9/04
CPC分类号： C03C17/3618 , C03C17/36 , C03C17/3626 , C03C17/3644 , C03C17/366 , C03C17/3681 , G02B5/282 , C03C2217/24 , C03C2217/242 , C03C2217/78
摘要： An infrared reflecting interference filter capable of transmitting a desired proportion of visible radiation while reflecting a large portion of incident solar radiation is provided. The filter comprises a transparent substrate onto which is deposited a dielectric layer, followed by metal and dielectric layers. In between each of the dielectric and metal layers is deposited a precoat layer that promotes adhesion between the dielectric and the metal. One aspect of the invention is the use of a film comprising nickel and chromium nitride for each of the metal precoat layers. These precoat layers are thin so that there is less absorption of visible light but yet maintains good adhesive properties. Another aspect of the invention is the use of silver as the metal layer. Specifically, silver is sputtered in an atmosphere containing a mixture of nitrogen and argon or other inert gas. It was found that the presence of nitrogen produces a silver layer that is more durable than silver films sputtered in an atmosphere containing essentially pure inert gas. In one embodiment, the interference filter comprises a glass substrate onto which is deposited a thin-film design consisting of five layers, namely: titanium dioxide, nickel-chromium nitride, silver, nickel-chromium nitride, and silicon nitride.
摘要翻译：提供能够在反射大部分入射的太阳辐射的同时传输期望比例的可见光的红外反射干涉滤光器。滤光器包括透明基板，在其上沉积介电层，其次是金属和电介质层。在每个介电层和金属层之间沉积预涂层，其促进电介质和金属之间的粘附。本发明的一个方面是使用包含镍和氮化铬的膜用于每个金属预涂层。这些预涂层是薄的，因此对可见光的吸收较少但仍具有良好的粘合性能。本发明的另一方面是使用银作为金属层。具体地说，将银溅射在含有氮气和氩气或其它惰性气体的混合物的气氛中。发现氮的存在产生比在基本上纯的惰性气体的气氛中溅射的银膜更耐用的银层。在一个实施例中，干涉滤光器包括玻璃基板，在其上沉积由五层组成的薄膜设计，即：二氧化钛，镍 - 氮化铬，银，镍 - 氮化铬和氮化硅。

9. 发明授权

US5377045A Durable low-emissivity solar control thin film coating 失效
标题翻译：耐用的低辐射太阳能控制薄膜涂层
公开(公告)号：US5377045A
公开(公告)日：1994-12-27
申请号：US126724
申请日：1993-09-24
申请人： Jesse D. Wolfe , Abraham I. Belkind , Ronald E. Laird
发明人： Jesse D. Wolfe , Abraham I. Belkind , Ronald E. Laird
IPC分类号： C03C17/36 , G02B5/28 , G02B1/10
CPC分类号： C03C17/3618 , C03C17/36 , C03C17/3626 , C03C17/3642 , C03C17/3652 , C03C17/366 , G02B5/282 , C03C2217/40 , C03C2217/78
摘要： An infrared reflecting interference filter capable of transmitting a desired proportion of visible radiation while reflecting a large portion of incident solar radiation is provided. The filter consists of a transparent substrate coated first with a dielectric layer, next a partially metal reflectance layer, and finally an outer protective dielectric layer. In addition, between each metal-dielectric interface is deposited a nucleation or glue layer that facilitates adhesions and improves chemical and mechanical resistance. The interference filters are durable and can be modified to provide a full range of optical and electrical characteristics. The dielectric layer can comprise of composite films consisting of silicon nitride in combination with zirconium nitride, titanium nitride, and/or hafnium nitride.
摘要翻译：提供能够在反射大部分入射的太阳辐射的同时传输期望比例的可见光的红外反射干涉滤光器。滤光器由首先涂覆有介电层，接下来是部分金属反射层，最后涂覆外部保护介电层的透明基板组成。此外，在每个金属 - 电介质界面之间沉积有助于粘连并提高化学和机械阻力的成核或胶层。干涉滤光片是耐用的，可以进行修改，以提供全方位的光学和电气特性。介电层可以包括由氮化硅与氮化锆，氮化钛和/或氮化铪组合的复合膜。

10. 发明授权

US07226528B2 Methods of making coated articles by sputtering silver in oxygen inclusive atmosphere 有权
标题翻译：通过在包含氧气的气氛中溅射银制造涂层制品的方法
公开(公告)号：US07226528B2
公开(公告)日：2007-06-05
申请号：US10802918
申请日：2004-03-18
申请人： Ronald E. Laird , George Neuman , Philip J. Lingle , Jean-Marc Lemmer , Keith H. Schillinger
发明人： Ronald E. Laird , George Neuman , Philip J. Lingle , Jean-Marc Lemmer , Keith H. Schillinger
IPC分类号： C23C14/34
CPC分类号： C03C17/3423 , B32B17/10036 , B32B17/10174 , B32B17/10761 , B32B27/34 , C03C17/36 , C03C17/3618 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C2217/78 , C23C14/0063 , C23C14/0084 , C23C14/08 , C23C14/185
摘要： A sputter coated article is provided with improved mechanical durability (e.g., pre-HT scratch resistance) and/or thermal stability by sputtering at least one Ag inclusive layer in an atmosphere including at least O2 gas. For instance, in certain example embodiments an Ag inclusive target may be sputtered in an atmosphere including a combination of Ar and O2 gas. In certain embodiments, this enables the resulting AgOx infrared (IR) reflecting layer to better adhere to adjacent contact layer(s).
摘要翻译：通过在包括至少O 2 2气体的气氛中溅射至少一种Ag包覆层，提供具有改善的机械耐久性（例如，预HT耐刮擦性）和/或热稳定性的溅射涂层制品。例如，在某些示例性实施方案中，包含Ag的靶可以在包括Ar和O 2 2气体的组合的气氛中溅射。在某些实施例中，这使得所得到的AgO x红外（IR）反射层更好地粘附到相邻的接触层。

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