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1. 发明授权

US5565553A Disazo dyes with a vinylsulfonyl type fiber-reactive radical substituted diazo component and a 2-sulfophenylene middle component carrying a fiber-reactive radical in the 5-position 失效
标题翻译：具有乙烯基磺酰基型纤维反应性自由基取代的重氮组分的双偶氮染料和在5位上携带纤维反应性基团的2-磺基亚苯基中间组分
公开(公告)号：US5565553A
公开(公告)日：1996-10-15
申请号：US584582
申请日：1996-01-11
申请人： Rolf Deitz , Paul Herzig , Athanassios Tzikas
发明人： Rolf Deitz , Paul Herzig , Athanassios Tzikas
IPC分类号： C09B62/513 , C09B62/44 , C09B62/447 , C09B62/665 , C09B62/67 , D06P3/66 , C09B62/09 , D06P1/38 , D06P3/58
CPC分类号： C09B62/4401 , C09B62/447
摘要： Reactive dyes of the formula ##STR1## where A, K and Z are each as defined in the claims, are especially useful for dyeing or printing cellulosic fiber materials, producing dyeings and prints having good fastness properties in a high yield.
摘要翻译：式（1）的活性染料其中A，K和Z各自如权利要求中所定义，特别可用于染色或印刷纤维素纤维材料，以高产率生产具有良好牢度性能的染色和印花。

2. 发明授权

US5817779A Azo reactive dyes, their preparation and use 失效
标题翻译：偶氮活性染料，其制备和用途
公开(公告)号：US5817779A
公开(公告)日：1998-10-06
申请号：US783183
申请日：1997-01-15
申请人： Rolf Deitz , Paul Herzig , Athanassios Tzikas
发明人： Rolf Deitz , Paul Herzig , Athanassios Tzikas
IPC分类号： C09B62/44 , C09B62/513 , C09B62/09 , D06P1/38 , D06P1/382 , D06P1/384
CPC分类号： C09B62/4415 , C09B62/513
摘要： Described are compounds of formula ##STR1## which are suitable as fibre-reactive dyes for dyeing and printing a very wide range of different fibre materials.
摘要翻译：描述了适用于染色和印刷非常宽范围的不同纤维材料的纤维活性染料的式（Ⅰ）化合物。

3. 发明授权

US5548071A Fiber-reactive triazine dyes with one AZO chromophore having a vinylsulfonyl type reactive radical and a second chromophore 失效
标题翻译：具有一个具有乙烯基磺酰基型反应性基团的AZO发色团的纤维反应性三嗪染料和第二种发色团
公开(公告)号：US5548071A
公开(公告)日：1996-08-20
申请号：US242562
申请日：1994-05-13
申请人： Rolf Deitz , Athanassios Tzikas , Paul Herzig
发明人： Rolf Deitz , Athanassios Tzikas , Paul Herzig
IPC分类号： C09B62/503 , C09B62/44 , D06P3/66 , C09B62/04 , D06P1/38
CPC分类号： C09B62/4403
摘要： The invention relates to compounds of the formula ##STR1## where the variables are each as defined in the claims. The compounds are suitable for use as dyes, in particular for dyeing and printing cellulose-containing fibre materials and produce dyeings and prints having good allround fastness properties.
摘要翻译：本发明涉及式（1）的化合物，其中变量各自如权利要求中所定义。该化合物适合用作染料，特别是用于染色和印刷含纤维素的纤维材料，并且生产具有良好全面牢固性能的染色和印花。

4. 发明授权

US5207801A Reactive dye mixtures, processes for their preparation and their use: reactive sulfonated tri-phenol-dioxazine dye mixture for cellulose fibers 失效
标题翻译：反应性染料混合物，其制备方法及其用途：用于纤维素纤维的反应性硫化三苯并二恶嗪染料混合物
公开(公告)号：US5207801A
公开(公告)日：1993-05-04
申请号：US787991
申请日：1991-11-05
申请人： Peter Aeschlimann , Paul Herzig , Athanassios Tzikas
发明人： Peter Aeschlimann , Paul Herzig , Athanassios Tzikas
IPC分类号： C09B62/02 , C09B62/44 , C09B62/503 , C09B67/22 , D06P1/382 , D06P3/66
CPC分类号： C09B67/004 , C09B62/021 , C09B62/4401 , C09B62/5033 , Y10S8/917 , Y10S8/918 , Y10S8/924 , Y10S8/926
摘要： The invention relates to reactive dye mixtures comprising the reactive dyes of the formulae ##STR1## in which X.sub.1, X.sub.2 and X.sub.3 are reactive radicals bonded via a diaminoalkylene bridge and the other substituents are as defined in claim 1.The reactive dye mixtures are suitable for dyeing and printing cellulosic fibre materials and give wet- and light-fast dyeings in luminous blue shades.
摘要翻译：本发明涉及包含式（1）和（IMAGE）（2）的反应性染料的活性染料混合物，其中X 1，X 2和X 3是通过二氨基亚烷基桥键连接的反应性基团，其它取代基如活性染料混合物适用于染色和印刷纤维素纤维材料，并以发光蓝色色调提供湿和轻快染色。

5. 发明授权

US5434252A Reactive dyes containing a 2,6-diaminopyridine coupling component 失效
标题翻译：含有2,6-二氨基吡啶偶联成分的活性染料
公开(公告)号：US5434252A
公开(公告)日：1995-07-18
申请号：US328599
申请日：1994-10-25
申请人： Paul Herzig , Athanassios Tzikas , Anton Andreoli , Claudia Carisch
发明人： Paul Herzig , Athanassios Tzikas , Anton Andreoli , Claudia Carisch
IPC分类号： C09B62/085 , C07D213/82 , C07D213/85 , C07D401/12 , C09B62/026 , C09B62/09 , C09B62/44 , C09B62/447 , C09B62/51 , C09B62/513 , C09B67/22 , C09B67/26 , D06P3/66 , D06P1/382
CPC分类号： C07D213/82 , C07D213/85 , C07D401/12 , C09B62/026 , C09B62/4401 , C09B62/447
摘要： Reactive dyes of the formula ##STR1## in which D, R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are as defined in claim 1, are particularly suitable for dyeing or printing cellulosic fiber materials or naturally occurring or synthetic polyamide fiber materials with a high tinctorial yield, and produce dyeings and prints having good fastness properties.
摘要翻译：其中D，R1，R2，R3和R4如权利要求1中所定义的式（1）的活性染料特别适用于染色或印刷纤维素纤维材料或具有高的纤维素纤维材料或天然存在或合成的聚酰胺纤维材料并且产生具有良好坚牢性的染色和印花。

6. 发明授权

US5128456A Reactive dyes 失效
标题翻译：反应性染料
公开(公告)号：US5128456A
公开(公告)日：1992-07-07
申请号：US604551
申请日：1990-10-26
申请人： Athanassios Tzikas , Paul Herzig
发明人： Athanassios Tzikas , Paul Herzig
IPC分类号： C09B62/085 , D06P3/66
CPC分类号： C09B62/085
摘要： Novel reactive dyes of the formula ##STR1## in which (R).sub.0-3 is 0-3 substituents R, independent of one another, from the group comprising halogen, nitro, cyano, trifluoromethyl, sulfamoyl, carbamoyl, C.sub.1-4 alkyl, C.sub.1-4 alkoxy, amino, acetylamino, ureido, hydroxyl, carboxyl, sulfomethyl and sulfo, R.sub.1 is hydrogen, C.sub.1-8 alky or C.sub.5-7 cycloalkyl and R.sub.2 is C.sub.1-8 alkyl or C.sub.5-7 cycloalkyl, it being possible for the alkyl and cycloalkyl radicals R.sub.1 and R.sub.2 to be substituted independently of one another by hydroxyl, C.sub.1-4 alkoxy, hydroxy-C.sub.1-4 alkoxy, HO--(CH.sub.2 CH.sub.2 --O).sub.2-4 --, sulfato-C.sub.1-4 alkoxy, C.sub.2-4 alkanoyl, C.sub.1-4 alkoxy-carbonyl, C.sub.2-4 alkanoyloxy, carboxyl, cyano, halogen, C.sub.1-4 alkylamino, or N,N-Di-C.sub.1-4 alkylamino, or sulfato, or in which R.sub.1 is C.sub.1-8 alkyl or C.sub.5-7 cycloalkyl, and the alkyl or cycloalkyl radical can be substituted as defined, and R.sub.2 is a C.sub.1-8 alkyl or C.sub.5-7 cycloalkyl radical which is substituted by sulfo, give deep yellow to orange dyeings and prints with good fastness properties on cellulose fibres.
摘要翻译：式（1）的新型活性染料其中（R）0-3为0-3取代基R彼此独立地为卤素，硝基，氰基，三氟甲基，氨磺酰基，氨基甲酰基，C 1-4烷基，C 1-4烷氧基，氨基，乙酰氨基，脲基，羟基，羧基，磺基甲基和磺基，R 1是氢，C 1-8烷基或C 5-7环烷基，R 2是C 1-8烷基或C 5-7环烷基，烷基和环烷基 R 1和R 2彼此独立地被羟基，C 1-4烷氧基，羟基-C 1-4烷氧基，HO-（CH 2 CH 2 -O）2-4 - ，硫酸基-C 1-4烷氧基，C 2-4烷酰基，C 1-4烷氧基羰基 C 2-4烷酰氧基，羧基，氰基，卤素，C 1-4烷基氨基或N，N-二-C 1-4烷基氨基或硫酸酯，或其中R 1为C 1-8烷基或C 5-7环烷基，并且烷基或环烷基可为被定义为取代基，R2是被磺基取代的C 1-8烷基或C 5-7环烷基，在纤维素纤维上产生深黄色至橙色染色和具有良好牢度性质的印花。

7. 发明授权

US5081296A Bis(.beta.-hydroxyethylthio)-C.sub.1 -C.sub.4 -alkylamines 失效
标题翻译： BIS（（BETA）-HYOXOXYETHYLTHIO）-C1-C4-烷基胺
公开(公告)号：US5081296A
公开(公告)日：1992-01-14
申请号：US510384
申请日：1990-04-17
申请人： Athanassios Tzikas , Paul Herzig
发明人： Athanassios Tzikas , Paul Herzig
IPC分类号： C07C323/25 , C07C67/00 , C07C313/00 , C07C317/28 , C07C323/42 , C07D213/69 , C07D231/22 , C07D251/50 , C07D251/52 , C07D498/04 , C09B62/44 , C09B62/503
CPC分类号： C09B62/4401 , C09B62/503
摘要： This application relates to intermediates useful for the preparation of fiber-reactive dyes, said intermediates having the formulae ##STR1## in which B is a --(CH.sub.2).sub.n -- or --O--(CH.sub.2).sub.n -- radical, where n is 1 to 6; Q is selected from the group consisting of hydrogen, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, halogen, carboxyl and sulfo; and A is an amino substituent of the formula ##STR2## and Z and Z', independently of one another, are .beta.-sulfatoethyl, .beta.-thiosulfatoethyl, .beta.-phosphatoethyl, .beta.-acyloxyethyl, .beta.-haloethyl or vinyl.
摘要翻译：本申请涉及可用于制备纤维活性染料的中间体，所述中间体具有式（IMAGE）＆lt; IMAGE＆gt;和＆lt; IMAGE＆gt;（31）或其中B是 - （CH 2）n - 或-O-（CH 2）n - 基，其中n为1至6; Q选自氢，C 1 -C 4烷基，C 1 -C 4烷氧基，卤素，羧基和磺基; 并且A是式（1a）的氨基取代基，Z和Z'彼此独立地是β-磺基乙基，β-硫代硫代乙基，β-磷酸乙基，β-酰氧基乙基，β-卤代乙基或乙烯基。

8. 发明授权

US5041539A Preparation of aqueous concentrates of yellow azo and azoxystilbene dyes utilizing alkanolamine salts 失效
标题翻译：使用链烷醇胺盐制备黄色偶氮和二烷染料的浓缩水
公开(公告)号：US5041539A
公开(公告)日：1991-08-20
申请号：US370089
申请日：1989-06-19
申请人： Athanassios Tzikas , Paul Herzig , Jurgen Markert
发明人： Athanassios Tzikas , Paul Herzig , Jurgen Markert
IPC分类号： C09B56/04 , C09B67/26 , C09B69/04
CPC分类号： C09B69/04 , C09B67/0073
摘要： The invention relates to a process for the preparation of concentrated storage-stable aqueous solutions of yellow azo- and azoxystilbene dyes which are obtained by self-condensation of 4-nitrotoluene-2-sulfonic acid in the presence of an alkali metal hydroxide, by converting the sparingly soluble alkali metal salt of the dye into a water-soluble ammonium salt by double cation exchange via a lipophilic ammonium salt, which process comprises carrying out the double ion exchange in a two-phase system of nitrobenzene/water and using, for the first ion exchange a di- or trialkylamine containing a total of 12 to 40 carbon atoms and, for the second ion exchange, a mono-, di- or trialkanolamine containing 2 to 4 carbon atoms in each alkyl moiety.The concentrated storage-stable dye solutions so obtained are particularly suitable for dyeing paper.
摘要翻译：本发明涉及一种通过在碱金属氢氧化物的存在下通过4-硝基甲苯-2-磺酸的自缩合而得到的黄色偶氮 - 和二喔啉染料的浓缩储存稳定水溶液的方法，通过亲脂性铵盐通过双阳离子交换将染料的微溶性碱金属盐转化为水溶性铵盐，该方法包括在硝基苯/水的两相体系中进行双离子交换，并使用首先离子交换含有总共12至40个碳原子的二 - 或三烷基胺，并且对于第二离子交换，每个烷基部分含有2至4个碳原子的单 - ，二 - 或三烷醇胺。如此得到的浓缩储存稳定的染料溶液特别适用于染色纸。

9. 发明授权

US4876334A Triazinyl reactive dyes in which the triazinyl is furter substituted with a reactive radical 失效
公开(公告)号：US4876334A
公开(公告)日：1989-10-24
申请号：US150695
申请日：1988-02-01
申请人： Athanassios Tzikas , Paul Herzig
发明人： Athanassios Tzikas , Paul Herzig
IPC分类号： C09B62/44 , C09B62/503 , C09B62/64
CPC分类号： C09B62/503 , C09B62/4403
摘要： Reactive dyes of the formula ##STR1## in which D is the radical of a monoazo, polyazo, metal complex azo, anthraquinone, phthalocyanine, formazan, azomethine, dioxazine, phenazine, stilbene, triphenylmethane, xanthene, thioxanthone, nitroaryl, naphthoquinone, pyrenequinone or perylenetetracarbimide dye, B.sub.1 and B.sub.2 are independently of each other hydrogen or alkyl which has 1 to 4 carbon atoms and which can be substituted by halogen, hydroxyl, cyano, C.sub.1-4 alkoxy, C.sub.1-4 alkoxycarbonyl, carboxyl, sulfamoyl, sulfo or sulfato, X is fluorine, chlorine, bromine, sulfo, alkylsulfonyl having 1 to 4 C atoms or phenylsulfonyl, B is a --CH.sub.2 --.sub.n or --O--CH.sub.2 --.sub.n radical, n is 1 to 6, R is a radical of the formula ##STR2## Z is .beta.-sulfatoethyl, .beta.-thiosulfatoethyl, .beta.-phosphatoethyl, .beta.-acyloxyethyl, .beta.-haloethyl or vinyl, alk is an alkylene radical having 1 to 6 C atoms or a branched isomer thereof, Y is hydrogen, chlorine, bromine, fluorine, hydroxyl, sulfato, acyloxy having 1 to 4 C atoms, cyano, carboxyl, alkoxycarbonyl having 1 to 5 C atoms, carbamoyl or a --SO.sub.2 --Z radical, in which Z is as defined above, V is hydrogen or an alkyl radical having 1 to 4 C atoms and which can be substituted by carboxyl or sulfo groups or by derivatives thereof, or by alkoxy groups having 1 to 2 C atoms, halogen or hydroxyl, or a ##STR3## radical in which Z, alk and Y are as defined above, R.sub.1 is hydrogen or C.sub.1-6 alkyl, the alk's are independently of each other polymethylene radicals having 2 to 6 C atoms or branched isomers thereof, m is 1 to 6, p is 1 to 6 and q is 1 to 6, and the benzene or naphthalene radical A can contain further substituentsare suitable in particular for dyeing or printing cellulose-containing fibre materials by the cold pad-batch method and, while giving a high dyeing yield, produce dyeings and prints having good fastness properties.

10. 发明授权

US4786721A Fiber-reactive dyes containing a vinylsulfonylalkylamino- or sulfonyl-arylaminotriazine moiety 失效
标题翻译：含有乙烯基磺酰基烷基氨基 - 或磺酰基 - 芳基氨基三嗪部分的纤维反应性染料
公开(公告)号：US4786721A
公开(公告)日：1988-11-22
申请号：US896290
申请日：1986-08-13
申请人： Athanassios Tzikas , Peter Aeschlimann , Paul Herzig
发明人： Athanassios Tzikas , Peter Aeschlimann , Paul Herzig
IPC分类号： D06P1/38 , C09B62/04 , C09B62/44 , C09B62/503 , C09B62/51 , C09B62/513 , C09B62/515 , C09B62/06 , C09B62/08 , C09B62/085 , C09B62/09 , C09B62/095 , C09B62/10 , C09B62/523
CPC分类号： C09B62/4403
摘要： The reactive dyes are useful, in particular, for dyeing or printing cellulose-containing fiber materials by the cold pad-batch method and produce, with a high dyeing yield, dyeings and prints having good fastness properties.
摘要翻译：活性染料尤其可用于通过冷垫分批法染色或印刷含纤维素纤维材料，并以高染色产率生产具有良好牢度性质的染色和印花。

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