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1. 发明授权

US08137809B2 Ultra high molecular weight polyethylene multifilament yarns, and process for producing thereof 有权
标题翻译：超高分子量聚乙烯复丝纱线及其制造方法
公开(公告)号：US08137809B2
公开(公告)日：2012-03-20
申请号：US12933772
申请日：2009-04-09
申请人： Roelof Marissen , Harm van der Werff , Joseph Arnold Paul Maria Simmelink , Evert Florentinus Florimondus De Danschutter
发明人： Roelof Marissen , Harm van der Werff , Joseph Arnold Paul Maria Simmelink , Evert Florentinus Florimondus De Danschutter
IPC分类号： D02G3/00
CPC分类号： D01F6/04 , Y10T428/2913 , Y10T428/2967
摘要： The invention relates to a gel spun, ultrahigh molecular weight polyethylene (UHMWPE) multifilament yarn characterized in that said yarn comprises individual monofilaments having a coefficient of variation of their linear density, hereafter CVintra, of less than 30%, wherein the CVintra of a monofilament was determined from linear density values corresponding to a number of 20 representative lengths randomly extracted by cutting from said monofilament and using Formula 1 wherein χi is the linear density of any one of the representative lengths extracted from the monofilament under investigation and Formula 1A is the averaged linear density over the n=20 measured linear densities of said n=20 representative lengths. The invention also relates to a gel spun UHMWPE multifilament yarn characterized in that the yarn has a coefficient of variation in linear density between the monofilaments comprising said yarn, hereafter CVinter, of less than 50%. The invention also relates to a gel spinning process of producing thereof characterized in that a chamber is present before the spinning plate such that no further partitioning of the UHMWPE solution takes place before said solution being finally partitioned into individual monofilaments by the spinning plate and in which chamber the solution has a residence time τ at a constant throughput of UHMWPE solution of at least 5 sec. The invention also relates to a rope, net, medical cable or a composite comprising the yarns of the invention.
摘要翻译：本发明涉及一种凝胶纺丝超高分子量聚乙烯（UHMWPE）复丝纱线，其特征在于所述纱线包括其线密度变异系数（以下简称CVintra）的单根单丝小于30％，其中单丝的CVintra 由对应于通过从所述单丝切割而随机提取的20个代表性长度的数目的线密度值确定，并且使用公式1，其中χi是从被研究的单丝中提取的任何代表性长度的线密度，而式1A是平均值所述n = 20个代表性长度的n = 20个线性密度的线密度。本发明还涉及一种凝胶纺丝UHMWPE复丝纱，其特征在于，所述纱线具有小于50％的包含所述纱线的单丝之间的线密度变化系数（以下称CVinter）。本发明还涉及其制造的凝胶纺丝方法，其特征在于在纺丝板之前存在室，使得在所述溶液最终通过纺丝板分成单个单丝之前不再进一步分配UHMWPE溶液，其中室中，溶液在UHMWPE溶液的恒定通量下具有至少5秒的停留时间τ。本发明还涉及一种绳，网，医用电缆或包含本发明纱线的复合材料。

2. 发明授权

US09687593B2 HPPE member and method of making a HPPE member 有权
公开(公告)号：US09687593B2
公开(公告)日：2017-06-27
申请号：US13992342
申请日：2011-12-12
申请人： Claudia Maria Vaz , Leonardus Gerardus Bernardus Bremer , Joseph Arnold Paul Maria Simmelink , Marko Dorschu , Jozef Maria Rudi Hendrik Goossens , Harm van der Werff
发明人： Claudia Maria Vaz , Leonardus Gerardus Bernardus Bremer , Joseph Arnold Paul Maria Simmelink , Marko Dorschu , Jozef Maria Rudi Hendrik Goossens , Harm van der Werff
IPC分类号： A61L31/04 , A61L27/16 , A61L29/04 , C08K3/08 , C08K3/22 , D06M11/47 , D01F11/12 , D06M11/83
CPC分类号： A61L31/048 , A61L27/16 , A61L29/041 , C08K3/08 , C08K3/22 , C08L23/06 , C08L2207/062 , D01F11/123 , D01F11/127 , D06M11/47 , D06M11/83 , Y10T428/2927
摘要： The invention concerns a high performance polyethylene (HPPE) member comprising at least 5 wt-% of a radiopaque component, the HPPE member is biocompatible and the radiopaque component is a particulate at least partially arranged inside a HPPE filament of the HPPE member. Furthermore, the radiopaque component has a particle size of at most 1 μm, preferably the radiopaque component has a particle size if at most 0.5 μm. The invention also concerns a method of making the HPPE member and various medical devices and repair products comprising the HPPE member.

3. 发明授权

US10315380B2 Process for the manufacture of a multilayer material sheet, multilayer material sheet and use hereof 有权
公开(公告)号：US10315380B2
公开(公告)日：2019-06-11
申请号：US13515936
申请日：2010-12-16
申请人： Koen van Putten , Johannes Maria Mathias Wilms , Ernst Jan van Klinken , Harm van der Werff , Leonard Josef Arnold Nielaba , Roelof Marissen
发明人： Koen van Putten , Johannes Maria Mathias Wilms , Ernst Jan van Klinken , Harm van der Werff , Leonard Josef Arnold Nielaba , Roelof Marissen
IPC分类号： B32B37/10 , B32B27/02 , B32B5/12 , B32B5/26 , B32B27/12 , B32B37/18 , F41H5/04
摘要： The invention relates to a process for the manufacture of a multilayer material sheet comprising unidirectional high performance fibers, the process comprising the steps of positioning the fibers in a parallel fashion, consolidation of the fibers to obtain a monolayer, stacking at least two monolayers such that the fiber direction in one monolayer is at an angle α to the direction of the fibers in an adjacent monolayer and fixation whereby the stack of at least two monolayers is subjected to a pressure and temperature treatment for a duration of a least 2 seconds, followed by cooling the stack under pressure to a temperature of 120° C. or lower. The invention furthermore relates to the multilayer material sheet obtainable with the process according to the invention. This multilayer material sheet has a reduced uptake of liquids.

4. 发明申请

US20130004704A1 PROCESS FOR THE MANUFACTURE OF A MULTILAYER MATERIAL SHEET, MULTILAYER MATERIAL SHEET AND USE HEREOF 审中-公开
标题翻译：制造多层材料表的方法，多层材料表及其用途
公开(公告)号：US20130004704A1
公开(公告)日：2013-01-03
申请号：US13515936
申请日：2010-12-16
申请人： Koen van Putten , Johannes Maria Mathias Wilms , Ernst Jan van Klinken , Harm van der Werff , Leonard Josef Arnold Nielaba , Roelof Marissen
发明人： Koen van Putten , Johannes Maria Mathias Wilms , Ernst Jan van Klinken , Harm van der Werff , Leonard Josef Arnold Nielaba , Roelof Marissen
IPC分类号： B32B37/10 , B32B27/02 , B32B5/12
CPC分类号： B32B5/12 , B32B5/26 , B32B27/12 , B32B37/1027 , B32B37/18 , B32B2250/20 , B32B2260/023 , B32B2260/046 , B32B2262/0253 , B32B2262/0269 , B32B2305/10 , B32B2307/54 , B32B2309/02 , B32B2309/12 , B32B2323/04 , B32B2355/00 , B32B2375/00 , B32B2377/00 , B32B2571/02 , F41H5/0485 , Y10T428/24124
摘要： The invention relates to a process for the manufacture of a multilayer material sheet comprising unidirectional high performance fibers, the process comprising the steps of positioning the fibers in a parallel fashion, consolidation of the fibers to obtain a monolayer, stacking at least two monolayers such that the fiber direction in one monolayer is at an angle a to the direction of the fibers in an adjacent monolayer and fixation whereby the stack of at least two monolayers is subjected to a pressure and temperature treatment for a duration of a least 2 seconds, followed by cooling the stack under pressure to a temperature of 120° C. or lower. The invention furthermore relates to the multilayer material sheet obtainable with the process according to the invention. This multilayer material sheet has a reduced uptake of liquids.
摘要翻译：本发明涉及一种制造包含单向高性能纤维的多层材料片的方法，该方法包括以平行方式定位纤维的步骤，使纤维固化以获得单层，堆叠至少两个单层，使得一个单层中的纤维方向与相邻单层中的纤维的方向成一定角度并固定，由此将至少两个单层的叠层经历至少2秒的持续时间的压力和温度处理，其次是将叠层在压力下冷却至120℃以下的温度。本发明还涉及可通过本发明的方法获得的多层材料片。该多层材料片材具有降低的液体吸收。

5. 发明授权

US5882791A Para-aromatic polyamide yarn having low filament linear density and a process for manufacturing same 失效
标题翻译：具有低丝线密度的对芳族聚酰胺纱线及其制造方法
公开(公告)号：US5882791A
公开(公告)日：1999-03-16
申请号：US910446
申请日：1997-08-05
申请人： Harm van der Werff , Jozef Johannes Maria Baltussen , Mattheus Harmannes Hofman
发明人： Harm van der Werff , Jozef Johannes Maria Baltussen , Mattheus Harmannes Hofman
IPC分类号： D01D5/06 , D01F6/60 , D02G3/02 , D02G3/44 , D02G3/00
CPC分类号： D01F6/605 , Y10T428/2913 , Y10T428/2969
摘要： A p-aramid microfilament yarn and a process for manufacturing the same. In the p-aramid yarn, which has a yarn linear density of at least 300 dtex, comprising a bundle of filaments with a linear density of less than 0.8 dtex, the g value is higher than 2.5 GPa, the elongation (EAB) is higher than 3.4%, and the L002 value is higher than 350 .ANG.. More particularly, the filament linear density is 0.3 to 0.8. The yarn according to the invention has surprisingly favorable properties, such as a high internal shear modulus. The invention also pertains to a process for manufacturing such a microfilament yarn in which p-aramid is subjected to an air gap-wet spinning process of the known type, in which the draw ratio in the air gap combined with the diameter of the capillaries through which the polymer is extruded ensures that microfilament yarn having the desired properties is obtained.
摘要翻译：对位芳族聚酰胺微丝纱及其制造方法。在具有至少300dtex的纱线线密度的对位芳族聚酰胺纱线中，包含线密度小于0.8dtex的长丝束，g值高于2.5GPa，伸长率（EAB）更高超过3.4％，L002值高于350安格姆。更具体地，丝线密度为0.3〜0.8。根据本发明的纱线具有惊人的有利的性能，例如高的内部剪切模量。本发明还涉及一种制造这种微丝纱的方法，其中对芳族聚酰胺经受已知类型的气隙 - 湿纺丝工艺，其中气隙中的拉伸比与毛细管的直径通过挤出聚合物确保获得具有所需性质的微丝纱线。

6. 发明申请

US20110238092A1 ULTRAHIGH MOLECULAR WEIGHT POLYETHYLENE YARN 审中-公开
标题翻译：超高分子量聚乙烯亚胺
公开(公告)号：US20110238092A1
公开(公告)日：2011-09-29
申请号：US13000131
申请日：2009-06-18
申请人： Claudia Maria Vaz , Erik Becker , Harm van der Werff
发明人： Claudia Maria Vaz , Erik Becker , Harm van der Werff
IPC分类号： D01F6/04 , D01F6/30 , D03D9/00 , A61B17/04 , A61B17/00 , D01D5/12
CPC分类号： D01F6/04 , A61B17/06166 , A61B2017/0619 , D01D5/08 , D01F6/30 , Y10T428/2978 , Y10T428/298 , Y10T442/10
摘要： The invention relates to an ultrahigh molecular weight polyethylene (UHMwPE) yarn and to a method for producing thereof. The invention also relates to a medical device comprising the yarn. A UHMwPE yarn is provided having a diameter of 30 μm or more and a residual spin solvent of less than 100 ppm, wherein the yarn is a gel-spun monofilament.
摘要翻译：本发明涉及一种超高分子量聚乙烯（UHMWPE）纱线及其制造方法。本发明还涉及包括纱线的医疗装置。提供直径为30μm以上的UHMwPE纱线和小于100ppm的残留旋转溶剂，其中纱线为凝胶纺丝单丝。

7. 发明授权

US07780888B2 Process for making a carbon nanotubes/ultra-high molar mass polyethylene composite fibre 有权
标题翻译：制造碳纳米管/超高摩尔质量聚乙烯复合纤维的方法
公开(公告)号：US07780888B2
公开(公告)日：2010-08-24
申请号：US11658155
申请日：2005-07-14
申请人： Harm van der Werff , Shilun Ruan , Tongxi Yu , Ping Gao , Roelef Marissen
发明人： Harm van der Werff , Shilun Ruan , Tongxi Yu , Ping Gao , Roelef Marissen
IPC分类号： D01F6/00 , C08K3/02
CPC分类号： B82Y30/00 , D01F1/10 , D01F6/04
摘要： The invention relates to a process for making a carbon nanotubes/ultra-high molar mass polyethylene (CNTs/UHPE) composite fiber comprising the steps of a) pre-treating CNTs with an acidic aqueous solution; b) making a composition containing pre-treated CNTs dispersed in a solution of UHPE in a spin solvent; and c) spinning the composition obtained into fibers; wherein step b) comprises making a dispersion of pre-treated CNTs in an alcohol, and mixing this dispersion with a mixture of UHPE and spin solvent. With this process CNTs/UHPE composite fibers showing improved tensile properties are obtained at relatively low CNTs content. A further advantage is that no or hardly any additional components, like dispersion aids, need to be added to make a stable dispersion of CNTs in the spin composition. The invention also relates to a CNTs/UHPE composite fiber obtainable by the process according to the invention, and to semi-finished or end-use articles containing said composite fiber.
摘要翻译：本发明涉及一种制备碳纳米管/超高摩尔质量聚乙烯（CNTs / UHPE）复合纤维的方法，包括以下步骤：a）用酸性水溶液预处理CNT; b）制备含有预处理的CNT分散在UHPE在旋转溶剂中的溶液中的组合物; 和c）将得到的组合物纺丝成纤维; 其中步骤b）包括将预处理的CNT分散在醇中，并将该分散体与UHPE和旋转溶剂的混合物混合。通过这种方法，CNTs / UHPE复合纤维在较低的CNTs含量下得到显示出改善的拉伸性能。另一个优点是不需要或几乎没有任何附加的组分，如分散助剂，以便使CNT在纺丝组合物中的稳定分散。本发明还涉及通过本发明的方法获得的CNTs / UHPE复合纤维，以及含有所述复合纤维的半成品或最终用途制品。

8. 发明授权

US6042941A Sulphurous p-aramid yarn 有权
标题翻译：硫磺对位芳族聚酰胺纱
公开(公告)号：US6042941A
公开(公告)日：2000-03-28
申请号：US171221
申请日：1998-11-17
申请人： Bastiaan Krins , Monique Helene Marielle Meeusen-Wierts , Harm van der Werff
发明人： Bastiaan Krins , Monique Helene Marielle Meeusen-Wierts , Harm van der Werff
IPC分类号： C08G69/32 , C08G69/48 , D01F6/60 , D02G3/00 , D02F6/00
CPC分类号： D01F6/605 , C08G69/32 , C08G69/48 , Y10T428/2913 , Y10T428/2969
摘要： A fiber of a para-aromatic polyamide polymer having a surprisingly higher modulus. This fiber has a quantity of sulphur bound to the aromatic nuclei of the polymer and wherein the quantity of nucleus-bound sulphur is 0.05-0.20% by weight. A process for the manufacture of para-aromatic polyamide fiber of increased modulus.
摘要翻译： PCT No.PCT / EP97 / 01102 Sec。 371日期：1998年11月17日 102（e）日期1998年11月17日PCT 1997年3月5日PCT公布。第WO97 / 39049号公报日期1997年10月23日具有令人惊讶的更高模量的对位芳族聚酰胺聚合物的纤维。该纤维具有与聚合物的芳族核结合的硫的量，其中核结合硫的量为0.05-0.20重量％。一种增加模量的对位芳族聚酰胺纤维的制造方法。

9. 发明授权

US5962627A Optically anisotropic spinning solution comprising a mixture of P-aramid and aliphatic polyamide, and fibers to be made therefrom 失效
标题翻译：包含对位芳族聚酰胺和脂肪族聚酰胺的混合物的光学各向异性纺丝溶液以及由其制成的纤维
公开(公告)号：US5962627A
公开(公告)日：1999-10-05
申请号：US844820
申请日：1997-04-22
申请人： Harm van der Werff , Johannes Marinus Surquin
发明人： Harm van der Werff , Johannes Marinus Surquin
IPC分类号： D01F6/90 , C08G69/32 , C08L77/10
CPC分类号： D01F6/905 , G02B6/02033 , Y10T428/2969 , Y10T428/2971 , Y10T428/31504 , Y10T428/31725
摘要： It has been found that fibers which incorporate very good mechanical properties as well as very good adhesive properties can be made from an optically anisotropic spinning solution containing a mixture of a paraphenylene groups-containing, wholly aromatic polyamide component and another polyamide component if for the para-aromatic polyamide component full or partial use is made of copolymer in which 2,6-naphthylene units are present in addition to the paraphenylene units and the other polyamide component is an aliphatic polyamide. Preferably, the weight ratio of the para-aromatic polyamide component to the aliphatic polyamide component is 95:5 to 85:15. The aromatic copolyamide containing paraphenylene and 2,6-naphthylene is preferably obtained by polymerising paraphenylene diamine (PPD) and a stoichiometric amount of a mixture composed of terephthalic acid dichloride (TDC) and 2,6-naphthylene carboxylic acid dichloride (NDC) in a molar ratio TDC:NDC of 99:1 to 80:20.
摘要翻译：已经发现，包含非常好的机械性能和非常好的粘合性能的纤维可以由包含对苯二甲酸基团的全芳族聚酰胺组分和另一种聚酰胺组分的混合物的光学各向异性纺丝溶液制成，如果对于芳族聚酰胺组分全部或部分使用由除了对亚苯基单元之外存在2,6-亚萘基单元并且其它聚酰胺组分为脂族聚酰胺的共聚物制成。对位芳族聚酰胺成分与脂肪族聚酰胺成分的重量比优选为95:5〜85:15。含有对苯二甲酸和2,6-亚萘基的芳香族共聚酰胺优选通过在对苯二甲酰胺（PPD）和化学计量量的由对苯二甲酸二氯化物（TDC）和2,6-亚萘基羧酸二氯化物（NDC）组成的混合物摩尔比TDC：NDC为99:1至80:20。

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