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1. 发明授权

US07368072B2 Photochromic contact lenses and methods of manufacturing 有权
标题翻译：光致变色隐形眼镜及制造方法
公开(公告)号：US07368072B2
公开(公告)日：2008-05-06
申请号：US10315656
申请日：2002-12-10
申请人： Barry Van Gemert , Anil Kumar , Frank P. Mallak , Robert W. Walters
发明人： Barry Van Gemert , Anil Kumar , Frank P. Mallak , Robert W. Walters
IPC分类号： B29D11/00 , G02B3/00 , G02B1/00
CPC分类号： B29D11/00048 , B29D11/00317 , B29D11/00653
摘要： Described are contact lenses having photochromic materials within the central or pupillary area of the lens and methods for manufacturing such lenses. In one method, a photochromic amount of at least one photochromic material is added to the pupillary region of a casting mold containing a polymerizable monomer that can be at least partially cured before and/or after the addition. Another method involves providing an amount of polymerizable photochromic monomer for the pupillary region and an amount of polymerizable non-photochromic monomer for the remainder of the contact lens in a casting mold. The photochromic and non-photochromic monomers can differ by their degree of polymerization, viscosity and/or density.
摘要翻译：描述了在透镜的中心或瞳孔区域内具有光致变色材料的隐形眼镜及其制造方法。在一种方法中，将光致变色量的至少一种光致变色材料添加到含有可聚合单体的铸模的瞳孔区域中，该可聚合单体可以在添加之前和/或之后至少部分固化。另一种方法包括提供一定量的用于瞳孔区域的可聚合光致变色单体和一定量的用于在模具中的隐形眼镜的其余部分的可聚合的非光致变色单体。光致变色和非光致变色单体可以通过其聚合度，粘度和/或密度而不同。

2. 发明申请

US20120145973A1 Photochromic Materials That Include Indeno-Fused Naphthopyrans 有权
标题翻译：包含茚诺芬萘醌的光致变色材料
公开(公告)号：US20120145973A1
公开(公告)日：2012-06-14
申请号：US13314297
申请日：2011-12-08
申请人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
发明人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
IPC分类号： G02B5/23 , C07D413/10 , C07D405/10 , C07D311/78
CPC分类号： C07D405/04 , C07D311/78 , C07D311/94 , C07D405/10 , C07D407/12 , C07D409/04 , C07D493/04 , C07D495/04 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1022 , C09K2211/1033 , C09K2211/1059 , C09K2211/1088 , G02B5/23 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： The present invention relates to photochromic materials that include one or more indeno-fused naphthopyrans that have particular groups at the 7, 11, and 13 positions thereof, and at the position alpha to the oxygen of the pyran ring thereof. With some embodiments, hydrogen or an alkoxy group is bonded to the 7 position, an optionally substituted phenyl is bonded to the 11 position, two alkyl groups are bonded to the 13 position, and two optionally substituted phenyl groups are bonded to the position alpha to the oxygen of the pyran ring of the indeno-fused naphthopyran compound. The 13 position of the indeno-fused naphthopyrans is free of ether groups in which an ether oxygen is bonded to the 13 position, and hydroxyl. The present invention also relates to photochromic articles and compositions that include such indeno-fused naphthopyrans.
摘要翻译：本发明涉及光致变色材料，其包括一种或多种茚并稠合的萘并吡喃，其在其7,11和13位具有特定基团，并且在其吡喃环的氧的位置。在一些实施方案中，氢或烷氧基键合至7位，任选取代的苯基键合至11位，两个烷基键合至13位，并且两个任选取代的苯基键合至位置α 茚并稠合萘并吡喃化合物的吡喃环的氧。茚并稠合萘并吡喃的13位没有醚基，其中醚氧与13位结合，羟基。本发明还涉及包含这种茚并稠合萘并吡喃的光致变色制品和组合物。

3. 发明授权

US07560056B2 Photochromic contact lenses and methods of manufacturing 有权
标题翻译：光致变色隐形眼镜及制造方法
公开(公告)号：US07560056B2
公开(公告)日：2009-07-14
申请号：US12027522
申请日：2008-02-07
申请人： Barry Van Gemert , Anil Kumar , Frank P. Mallak , Robert W. Walters
发明人： Barry Van Gemert , Anil Kumar , Frank P. Mallak , Robert W. Walters
IPC分类号： G02C7/10 , B29D11/00
CPC分类号： B29D11/00048 , B29D11/00317 , B29D11/00653
摘要： Described are contact lenses having photochromic materials within the central or pupillary area of the lens and methods for manufacturing such lenses. In one method, a photochromic amount of at least one photochromic material is added to the pupillary region of a casting mold containing a polymerizable monomer that can be at least partially cured before and/or after the addition. Another method involves providing an amount of polymerizable photochromic monomer for the pupillary region and an amount of polymerizable non-photochromic monomer for the remainder of the contact lens in a casting mold. The photochromic and non-photochromic monomers can differ by their degree of polymerization, viscosity and/or density.
摘要翻译：描述了在透镜的中心或瞳孔区域内具有光致变色材料的隐形眼镜及其制造方法。在一种方法中，将光致变色量的至少一种光致变色材料添加到含有可聚合单体的铸模的瞳孔区域中，该可聚合单体可以在添加之前和/或之后至少部分固化。另一种方法包括提供一定量的用于瞳孔区域的可聚合光致变色单体和一定量的用于在模具中的隐形眼镜的其余部分的可聚合的非光致变色单体。光致变色和非光致变色单体可以通过其聚合度，粘度和/或密度而不同。

4. 发明申请

US20080125512A1 PHOTOCHROMIC CONTACT LENSES AND METHODS OF MANUFACTURING 有权
标题翻译：光敏接触镜片及其制造方法
公开(公告)号：US20080125512A1
公开(公告)日：2008-05-29
申请号：US12027522
申请日：2008-02-07
申请人： Barry Van Gemert , Anil Kumar , Frank P. Mallak , Robert W. Walters
发明人： Barry Van Gemert , Anil Kumar , Frank P. Mallak , Robert W. Walters
IPC分类号： G02C7/04 , B29D11/02
CPC分类号： B29D11/00048 , B29D11/00317 , B29D11/00653
摘要： Described are contact lenses having photochromic materials within the central or pupillary area of the lens and methods for manufacturing such lenses. In one method, a photochromic amount of at least one photochromic material is added to the pupillary region of a casting mold containing a polymerizable monomer that can be at least partially cured before and/or after the addition. Another method involves providing an amount of polymerizable photochromic monomer for the pupillary region and an amount of polymerizable non-photochromic monomer for the remainder of the contact lens in a casting mold. The photochromic and non-photochromic monomers can differ by their degree of polymerization, viscosity and/or density.
摘要翻译：描述了在透镜的中心或瞳孔区域内具有光致变色材料的隐形眼镜及其制造方法。在一种方法中，将光致变色量的至少一种光致变色材料添加到含有可聚合单体的铸模的瞳孔区域中，该可聚合单体可以在添加之前和/或之后至少部分固化。另一种方法包括提供一定量的用于瞳孔区域的可聚合光致变色单体和一定量的用于在模具中的隐形眼镜的其余部分的可聚合的非光致变色单体。光致变色和非光致变色单体可以通过其聚合度，粘度和/或密度而不同。

5. 发明授权

US06555028B2 Polymeric matrix compatibilized naphthopyrans 有权
标题翻译：聚合物基体相容萘并吡喃
公开(公告)号：US06555028B2
公开(公告)日：2003-04-29
申请号：US09828260
申请日：2001-04-06
申请人： Robert W. Walters , Barry Van Gemert
发明人： Robert W. Walters , Barry Van Gemert
IPC分类号： G02B523
CPC分类号： C07D407/12 , C07D311/92 , C07D311/94 , C07D311/96 , C08G65/3315 , C08G65/3318 , C08G65/3346 , C08K5/1545 , C09B57/00 , C09B57/02 , C09B69/109 , C09K9/02 , G02B1/041 , G02B1/043 , G02B5/23
摘要： Described are polymeric matrix compatibilized naphthopyran compounds, examples of which are certain 2H-naphtho[1,2-b]pyrans, 3H-naphtho[2,1-b]pyrans and indeno[2,1-f]naphtho[1,2-b]pyrans each having at least one substituent containing terminal and/or pendant groups selected from hydroxyl, carboxyl, sulfo, sulfono, (meth)acryloxy, 2-(methacryloxy)ethylcarbamyl, epoxy or a mixture thereof. Specific substituents are also present on the naphtho, indeno and/or pyrano portions of the compounds. These compounds may be represented by the following graphic formulae: Also described are various substrates that contain or that are coated with such compounds. Optically clear articles such as contact lenses or other plastic transparencies that incorporate the novel naphthopyran compounds or combinations thereof with complementary photochromic compounds, are also described.
摘要翻译：描述的是聚合物基质相容的萘并吡喃化合物，其实例是一定的2H-萘并[1,2-b]吡喃，3H-萘并[2,1-b]吡喃和茚并[2,1-f]萘并[1,2 （甲基丙烯酰氧基）乙基氨基甲酰基，环氧基或它们的混合物中的至少一个含有末端和/或侧基的取代基的-b]吡喃各自具有选自羟基，羧基，磺基，磺基，（甲基）丙烯酰氧基，具体的取代基也存在于化合物的萘酚，茚并和/或吡喃葡萄糖部分上。这些化合物可以由以下图形表示：还描述了含有这些化合物或者被这些化合物包被的各种底物。还描述了光学清洁的物品，例如隐形眼镜或其它掺入新型萘并吡喃化合物或其组合与互补光致变色化合物的塑料透明胶片。

6. 发明授权

US09028728B2 Photochromic materials that include indeno-fused naphthopyrans 有权
标题翻译：包括茚并稠合萘并吡喃的光致变色材料
公开(公告)号：US09028728B2
公开(公告)日：2015-05-12
申请号：US13314297
申请日：2011-12-08
申请人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
发明人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
IPC分类号： G02B5/23 , C07D405/04 , C07D405/10 , C07D407/12 , C07D409/04 , C07D493/04 , C07D495/04 , C09K9/02 , G03C1/73 , C07D311/78 , C07D311/94 , G03C1/00 , G03C1/685
CPC分类号： C07D405/04 , C07D311/78 , C07D311/94 , C07D405/10 , C07D407/12 , C07D409/04 , C07D493/04 , C07D495/04 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1022 , C09K2211/1033 , C09K2211/1059 , C09K2211/1088 , G02B5/23 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： The present invention relates to photochromic materials that include one or more indeno-fused naphthopyrans that have particular groups at the 7, 11, and 13 positions thereof, and at the position alpha to the oxygen of the pyran ring thereof. With some embodiments, hydrogen or an alkoxy group is bonded to the 7 position, an optionally substituted phenyl is bonded to the 11 position, two alkyl groups are bonded to the 13 position, and two optionally substituted phenyl groups are bonded to the position alpha to the oxygen of the pyran ring of the indeno-fused naphthopyran compound. The 13 position of the indeno-fused naphthopyrans is free of ether groups in which an ether oxygen is bonded to the 13 position, and hydroxyl. The present invention also relates to photochromic articles and compositions that include such indeno-fused naphthopyrans.
摘要翻译：本发明涉及光致变色材料，其包括一种或多种茚并稠合的萘并吡喃，其在其7,11和13位具有特定基团，并且在其吡喃环的氧的位置。在一些实施方案中，氢或烷氧基键合至7位，任选取代的苯基键合至11位，两个烷基键合至13位，并且两个任选取代的苯基键合至位置α 茚并稠合萘并吡喃化合物的吡喃环的氧。茚并稠合萘并吡喃的13位没有醚基，其中醚氧与13位结合，羟基。本发明还涉及包含这种茚并稠合萘并吡喃的光致变色制品和组合物。

7. 发明授权

US07166357B2 Photochromic articles that activate behind ultraviolet radiation blocking transparencies and methods for preparation 有权
标题翻译：激活后紫外线阻挡透明胶片的光致变色制品及其制备方法
公开(公告)号：US07166357B2
公开(公告)日：2007-01-23
申请号：US10393179
申请日：2003-03-20
申请人： Anil Kumar , Michael S. Misura , Robert W. Walters , Barry Van Gemert , Anu Chopra , Clara E. Nelson
发明人： Anil Kumar , Michael S. Misura , Robert W. Walters , Barry Van Gemert , Anu Chopra , Clara E. Nelson
IPC分类号： B32B27/20 , B32B27/30 , B32B27/36 , B32B27/38 , B32B33/00
CPC分类号： C07D498/10 , C09K9/02 , C09K2211/1011 , C09K2211/1033 , C09K2211/1088 , Y10T428/31504 , Y10T428/31507 , Y10T428/31511 , Y10T428/31551 , Y10T428/31678 , Y10T428/31786 , Y10T428/31855 , Y10T428/31935 , Y10T428/31975 , Y10T428/31989 , Y10T428/31993
摘要： Described are photochromic articles that include a substrate and a photochromic amount of at least one organic photochromic material (b) represented by graphic formula XIII adapted to change from an unactivated state to an activated state by exposure to radiation substantially in a wavelength range from 380 to 410 nanometers (nm) when measured over a wavelength range of from 380 to 700 nm. The photochromic articles demonstrate a photochromic response when activated behind an ultraviolet blocking transparency such as an automotive windshield. For example, the photochromic articles retain at least 12 percent of the activation measured as change in optical density or delta OD under outdoor simulating conditions in the Outdoor Test when tested under conditions simulating an eyeglass wearer behind an automotive windshield in the Behind the Windshield Test. Methods for producing the aforedescribed photochromic articles are also described.
摘要翻译：描述的是光致变色制品，其包括基底和光致变色量的由图形式XIII表示的至少一种有机光致变色材料（b），其适于通过暴露于基本上在380至 - 的波长范围内的辐射而从未激活状态改变为活化状态在380至700nm的波长范围内测量时为410纳米（nm）。当紫外线阻挡透明体（例如汽车挡风玻璃）被激活时，光致变色制品表现出光致变色响应。例如，当在模拟在挡风玻璃测试后面的汽车挡风玻璃后面的眼镜佩戴者的条件下进行测试时，光致变色制品保持至少12％的活化作为室外模拟条件下的光密度或ΔOD的变化测量。还描述了制备上述光致变色制品的方法。

8. 发明授权

US09051344B2 Stability OLED materials and devices 有权
标题翻译：稳定性OLED材料和器件
公开(公告)号：US09051344B2
公开(公告)日：2015-06-09
申请号：US11241981
申请日：2005-10-04
申请人： Chun Lin , Peter B. Mackenzie , Robert W. Walters , Jui-Yi Tsai , Cory S. Brown , Jun Deng
发明人： Chun Lin , Peter B. Mackenzie , Robert W. Walters , Jui-Yi Tsai , Cory S. Brown , Jun Deng
IPC分类号： H01L51/54 , C09K11/06 , C07F15/00 , H01L51/00 , H01L51/50
CPC分类号： H01L51/0085 , C07F15/0033 , C07F15/0046 , C09K11/06 , C09K2211/1044 , C09K2211/185 , H01L51/009 , H01L51/5016 , H01L51/5206 , H01L51/5221 , H01L51/5231 , H01L2251/301 , H01L2251/308
摘要： Organic light emitting materials and devices comprising phosphorescent metal complexes comprising ligands comprising aryl or heteroaryl groups substituted at both ortho positions are described. An organic light emitting device, comprising: an anode; a hole transport layer; an organic emissive layer comprising an emissive layer host and an emissive dopant; an electron impeding layer; an electron transport layer; and a cathode disposed, in that order, over a substrate.
摘要翻译：描述了包含磷光金属络合物的有机发光材料和器件，其包含在两个邻位取代的包含芳基或杂芳基的配体。一种有机发光器件，包括：阳极; 空穴传输层; 包括发射层主体和发射掺杂剂的有机发射层; 电子阻挡层; 电子传输层; 以及依次设置在衬底上的阴极。

9. 发明申请

US20130215489A1 OPTICAL ELEMENT HAVING AN ELECTROCHROMIC APODIZED APERTURE AND AN APERTURE BODY FORMING AN ELECTROCHROMIC APODIZED APERTURE 审中-公开
标题翻译：具有电致变色光孔的光学元件和形成电致变色光孔的光孔体
公开(公告)号：US20130215489A1
公开(公告)日：2013-08-22
申请号：US13587218
申请日：2012-08-16
申请人： Forrest R. Blackburn , Jonathan Bork , John A. Charny , Stefan C. Dehaseth , Peter C. Foller , Andrew J. Lamb , Kevin W. Seybert , Michael A. Steimle , Robert H. Tang , Robert W. Walters
发明人： Forrest R. Blackburn , Jonathan Bork , John A. Charny , Stefan C. Dehaseth , Peter C. Foller , Andrew J. Lamb , Kevin W. Seybert , Michael A. Steimle , Robert H. Tang , Robert W. Walters
IPC分类号： G02F1/153
CPC分类号： G02F1/153 , B29D11/0074 , G02B5/005 , G02B27/58 , G03B9/02
摘要： An optical element includes an electrochromic apodized aperture having variable light transmittance through a clear aperture area in response to an applied electrical current. The apodized aperture includes an aperture body including an area defining the clear aperture area, the body having a fluid containment area substantially overlapping the clear aperture area, and includes at least one fill passage extending from the fluid containment area to at least one fill port outside of the clear aperture area; an electrochromic fluid within the fluid containment area substantially overlapping the clear aperture area and having variable light transmittance in response to an applied electrical current; a cover attached with the electrochromic fluid between the cover and body; electrical contacts electrically coupled to the electrochromic fluid for supplying electrical current thereto; and at least one passage seal in each said fill passage positioned outside of the clear aperture area.
摘要翻译：光学元件包括电致变色孔径，其响应于施加的电流通过透明孔径区域具有可变的透光率。变迹孔包括孔体，该孔体包括限定清洁孔径区域的区域，该主体具有基本上与透明孔径区域重叠的流体容纳区域，并且包括从流体容纳区域延伸至至少一个填充口外部的至少一个填充通道的清晰开口面积; 所述液体容纳区域内的电致变色液体基本上与所述透明孔径区域重叠并且响应于施加的电流具有可变的透光率; 盖子和主体之间附着有电致变色流体的盖子; 电接触电耦合到电致变色流体以供应电流的电接触; 并且每个所述填充通道中的至少一个通道密封件位于透光孔区域的外部。

10. 发明授权

US6025026A Process for producing an adherent polymeric layer on polymeric substrates and articles produced thereby 失效
标题翻译：用于在聚合物基材上生产粘附聚合物层的方法和由此制备的制品
公开(公告)号：US6025026A
公开(公告)日：2000-02-15
申请号：US092086
申请日：1998-06-05
申请人： Robert A. Smith , Robert W. Walters , Kevin J. Stewart , Michael S. Misura
发明人： Robert A. Smith , Robert W. Walters , Kevin J. Stewart , Michael S. Misura
IPC分类号： C08J7/12 , C08J7/14 , G02B5/23 , B05D3/02 , B05D1/38 , B05D3/06
CPC分类号： C08J7/14 , C08J7/12 , G02B5/23
摘要： Described is a process for producing adherent layer(s) on organic polymeric substrates following the steps of (a) treating the surface of the polymeric substrate to provide reactive groups; (b) applying to the surface a polymerizable composition of organic anhydrides, isocyanates and/or a mixture thereof that is substantially free of organosiloxanes; and (c) curing the polymerizable coating. Further steps include applying an additional layer which is substantially free of organosiloxanes and that may or may not contain the polymerizable composition of the present invention. Also described are products produced by the process that may be transparent, tinted, tinted and polarized or photochromic.
摘要翻译：描述了在（a）处理聚合物基材的表面以提供反应性基团的步骤之后，在有机聚合物基材上制备粘附层的方法; （b）向表面施加基本上不含有机硅氧烷的有机酸酐，异氰酸酯和/或其混合物的可聚合组合物; 和（c）固化可聚合涂层。进一步的步骤包括施加基本上不含有机硅氧烷的附加层，并且可以包含或可以不含有本发明的可聚合组合物。还描述了通过该方法生产的可以是透明的，有色的，着色的和极化的或光致变色的产品。

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