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1. 发明授权

US5837763A Compositions and methods for manufacturing waxes filled with intercalates and exfoliates formed with oligomers and polymers 失效
标题翻译：用于制备填充有由低聚物和聚合物形成的插层和去角质的蜡的组合物和方法
公开(公告)号：US5837763A
公开(公告)日：1998-11-17
申请号：US582480
申请日：1996-01-03
申请人： Robert Matthew Ferraro , Charles Randolph Landis , Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Robert Matthew Ferraro , Charles Randolph Landis , Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： C01B33/44 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C11C5/00 , C08J5/10 , C08L29/00
CPC分类号： A61K8/26 , A61Q5/04 , B82Y30/00 , C01B33/44 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C11C5/002 , A61K2800/56 , C01P2002/74 , C01P2004/20 , C01P2004/54 , C01P2004/64
摘要： Compositions and methods that include a wax, in an amount of about 20% to about 99.95% by weight, containing an intercalate, or exfoliate thereof, in an amount of about 0.05% to about 80% by weight of the composition formed by contacting a layered phyllosilicate with an oligomer and/or polymer to sorb or intercalate the intercalant polymer or mixtures of intercalant polymers between adjacent phyllosilicate platelets. Sufficient intercalant polymer is sorbed between adjacent phyllosilicate platelets to expand the spacing between adjacent platelets (interlayer spacing) to a distance of at least about 5 .ANG., preferably to at least about 10 .ANG. (as measured after water removal) and more preferably in the range of about 30-45 .ANG., so that the intercalate easily can be exfoliated, sometimes naturally, without shearing being necessary.
摘要翻译：组合物和方法，其包含约20％至约99.95％重量的蜡，其含量为所述组合物的约0.05重量％至约80重量％，所述组合物或其剥离物通过使层状页硅酸盐与低聚物和/或聚合物吸附或插入相邻页硅酸盐片剂之间的插入聚合物或插入剂聚合物的混合物。在相邻的页硅酸盐片段之间吸附足够的嵌入聚合物以将相邻片晶之间的间隔（层间距）扩展至至少约5安培的距离，优选至少约10安培（在除水后测量），更优选在范围内约30-45安士，所以插入物很容易被剥离，有时自然而不需要剪切。

2. 发明授权

US5698624A Exfoliated layered materials and nanocomposites comprising matrix polymers and said exfoliated layered materials formed with water-insoluble oligomers and polymers 失效
标题翻译：剥离的层状材料和包含基质聚合物的纳米复合材料和由水不溶性低聚物和聚合物形成的所述剥离层状材料
公开(公告)号：US5698624A
公开(公告)日：1997-12-16
申请号：US488263
申请日：1995-06-07
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： C01B33/44 , C08K7/00 , C08K9/04 , C11C5/00 , C08K3/34 , C08K5/35 , C08K5/36
CPC分类号： B82Y30/00 , C01B33/44 , C08K7/00 , C08K9/04 , C11C5/002 , C01P2002/74 , C01P2004/20 , C01P2004/54 , C01P2004/64
摘要： Nanocomposites are manufactured by combining a matrix polymer and exfoliated intercalates formed by contacting a phyllosilicate with a water-insoluble polymer to adsorb or intercalate the polymer between adjacent phyllosilicate platelets. Sufficient water-insoluble polymer is adsorbed between adjacent phyllosilicate platelets to expand the adjacent platelets to a spacing of at least about 10 .ANG. (as measured after water removal), up to about 100 .ANG. and preferably in the range of about 30-40 .ANG., so that the intercalate easily can be exfoliated, e.g., when mixed with a polymer melt, to provide a matrix polymer/platelet composite (nanocomposite) material--the platelets being exfoliated from the intercalate.
摘要翻译：通过组合基质聚合物和通过使页硅酸盐与水不溶性聚合物接触而形成的剥离的嵌入物来制造纳米复合材料，以在相邻的页硅酸盐片剂之间吸附或嵌入聚合物。在相邻的页硅酸盐片之间吸附足够的水不溶性聚合物以使相邻的血小板膨胀至至少约10安培（除水后测量）的间隔，高达约100安培，优选在约30-40埃范围内，使得插入剂容易地被剥离，例如当与聚合物熔体混合时，提供基质聚合物/血小板复合材料（纳米复合材料） - 血小板从插层中剥离。

3. 发明授权

US5877248A Intercalates and exfoliates formed with oligomers and polymers and composite materials containing same 失效
标题翻译：用低聚物和聚合物形成的插层物和去角质物以及含有它们的复合材料
公开(公告)号：US5877248A
公开(公告)日：1999-03-02
申请号：US968408
申请日：1997-11-12
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： C01B33/44 , C08K3/00 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C08L101/00 , C11C5/00 , C08J5/10 , C08L39/06
CPC分类号： B82Y30/00 , A61K8/26 , A61K8/27 , A61K8/8176 , A61Q5/04 , C01B33/44 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C11C5/002 , A61K2800/56 , C01P2002/74 , C01P2004/20 , C01P2004/54 , C01P2004/64
摘要： Nanocomposites are manufactured by combining a host material, such as an organic solvent or a matrix polymer and exfoliated intercalates formed by contacting a phyllosilicate with a polymer to adsorb or intercalate the polymer between adjacent phyllosilicate platelets. Sufficient polymer is adsorbed between adjacent phyllosilicate platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG., preferably at least about 10 .ANG. (as measured after water removal), up to about 100 .ANG. and preferably in the range of about 30-40 .ANG., so that the intercalate easily can be exfoliated, e.g., when mixed with an organic solvent or a polymer melt, to provide a carrier material for drugs and the like, or to provide a matrix polymer/platelet composite (nanocomposite) material--the platelets being exfoliated from the intercalate.
摘要翻译：纳米复合材料通过将主体材料如有机溶剂或基质聚合物和通过使页硅酸盐与聚合物接触形成的剥离的嵌入物组合而制造，以在相邻的页硅酸盐片剂之间吸附或嵌入聚合物。在相邻的页硅酸盐片晶之间吸附足够的聚合物以将相邻的血小板膨胀至至少约5安培的间隔，优选至少约10安培（在除水后测量），高达约100安培，优选在约30约 -40 ANGSTROM，使得嵌入物容易被剥离，例如当与有机溶剂或聚合物熔体混合时，提供用于药物等的载体材料，或提供基质聚合物/血小板复合材料（纳米复合材料） - 血小板从插层中剥离。

4. 发明授权

US06461423B1 Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith 有权
标题翻译：插层和去角质形成羟基官能团; 多羟基官能团和芳香族化合物; 含有其的复合材料以及用其改性流变性的方法
公开(公告)号：US06461423B1
公开(公告)日：2002-10-08
申请号：US09578129
申请日：2000-05-24
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： B05D700
CPC分类号： C01B33/44 , C08K9/04 , F16C2240/64
摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer having a hydroxyl and/or an aromatic ring functionality to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 Å (as measured after water removal to a maximum of 5% by weight water), up to about 100 Å and preferably in the range of about 10-45 Å, so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to or after combination with the organic liquid or the matrix polymer.
摘要翻译：通过使分层材料例如页硅酸盐与具有羟基和/或芳环官能团的嵌入剂单体接触形成的嵌入体，以在分层材料的相邻片晶之间吸附或插入插入剂单体。在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5埃的水平（在除水后测量为最多5重量％的水），至多约100埃，优选在约10-45埃，使得插入物容易被剥离成单独的血小板。插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。或者，插入的复合物可以在与有机液体或基质聚合物组合之前或之后剥离。

5. 发明授权

US5760121A Intercalates and exfoliates formed with oligomers and polymers and composite materials containing same 失效
公开(公告)号：US5760121A
公开(公告)日：1998-06-02
申请号：US637092
申请日：1996-05-02
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： C01B33/44 , C08K3/00 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C08L101/00 , C11C5/00 , C08J5/10 , C08L77/00
CPC分类号： B82Y30/00 , A61K8/26 , A61K8/27 , A61K8/8176 , A61Q5/04 , C01B33/44 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C11C5/002 , A61K2800/56 , C01P2002/74 , C01P2004/20 , C01P2004/54 , C01P2004/64
摘要： Nanocomposites are manufactured by combining a host material, such as an organic solvent or a matrix polymer and exfoliated intercalates formed by contacting a phyllosilicate with a polymer to adsorb or intercalate the polymer between adjacent phyllosilicate platelets. Sufficient polymer is adsorbed between adjacent phyllosilicate platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG., preferably at least about 10 .ANG. (as measured after water removal), up to about 100 .ANG. and preferably in the range of about 30-40 .ANG., so that the intercalate easily can be exfoliated, e.g., when mixed with an organic solvent or a polymer melt, to provide a carrier material for drugs and the like, or to provide a matrix polymer/platelet composite (nanocomposite) material--the platelets being exfoliated from the intercalate.

6. 发明授权

US5578672A Intercalates; exfoliates; process for manufacturing intercalates and exfoliates and composite materials containing same 失效
标题翻译：插层; 去角质用于制造插层和去角质的方法以及含有它们的复合材料
公开(公告)号：US5578672A
公开(公告)日：1996-11-26
申请号：US480080
申请日：1995-06-07
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： B29C47/00 , C01B33/44 , C08K3/34 , C08K9/04 , C08L101/00 , C11C5/00 , C08K9/06
CPC分类号： C11C5/002 , C01B33/44 , C08K9/04 , Y10T428/259
摘要： Intercalates formed by mixing the phyllosilicate with a polymer and a liquid carrier, and extruding the mixture through a die-opening to adsorb or intercalate the polymer between adjacent phyllosilicate platelets. Sufficient polymer is adsorbed between adjacent phyllosilicate platelets to expand the adjacent platelets to a spacing of at least about 10 .ANG. (as measured after water removal), up to about 55 .ANG. and preferably in the range of about 30-40 .ANG., so that the intercalate easily can be exfoliated into individual platelets by heating the polymer to its melting point, to provide a matrix polymer/platelet composite material.
摘要翻译：通过将页硅酸盐与聚合物和液体载体混合而形成的嵌入物，并且通过模具开口挤出混合物以在相邻的页硅酸盐片剂之间吸附或嵌入聚合物。在相邻的页硅酸盐片之间吸附足够的聚合物以使相邻的血小板膨胀至至少约10安培（除水后测量）的间隔，最高约为55安培，优选在约30-40安培范围内，通过将聚合物加热至其熔点，易于插入到各个血小板中，以提供基质聚合物/血小板复合材料。

7. 发明授权

US6126734A Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith 有权
标题翻译：插层和去角质形成羟基官能团; 多羟基官能团和芳香族化合物; 含有其的复合材料以及用其改性流变性的方法
公开(公告)号：US6126734A
公开(公告)日：2000-10-03
申请号：US158490
申请日：1998-09-22
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： C01B33/44 , C08K9/04 , B05D7/00
CPC分类号： C01B33/44 , C08K9/04
摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer having a hydroxyl and/or an aromatic ring functionality to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to or after combination with the organic liquid or the matrix polymer.
摘要翻译：通过使分层材料例如页硅酸盐与具有羟基和/或芳环官能团的嵌入剂单体接触形成的嵌入体，以在分层材料的相邻片晶之间吸附或插入插入剂单体。在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在约10-45安士，使得插入物容易被剥离成单独的血小板。插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。或者，插入的复合物可以在与有机液体或基质聚合物组合之前或之后剥离。

8. 发明授权

US6083559A Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith 有权
公开(公告)号：US6083559A
公开(公告)日：2000-07-04
申请号：US158491
申请日：1998-09-22
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： C01B33/44 , C08K9/04 , C08K3/34
CPC分类号： C01B33/44 , C08K9/04
摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer having a hydroxyl and/or an aromatic ring functionality to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to or after combination with the organic liquid or the matrix polymer.

9. 发明授权

US5880197A Intercalates and exfoliates formed with monomeric amines and amides: composite materials containing same and methods of modifying rheology therewith 失效
标题翻译：由单体胺和酰胺形成的嵌入物和去角质：含有其的复合材料和用其改性流变性的方法
公开(公告)号：US5880197A
公开(公告)日：1999-03-09
申请号：US577558
申请日：1995-12-22
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： C01B33/44 , C08K9/04 , C08K9/06
CPC分类号： C01B33/44 , C08K9/04 , Y10T428/259 , Y10T428/31725
摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer amine and/or amide to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to combination with the organic liquid or the matrix polymer.
摘要翻译：通过使分层材料例如页硅酸盐与嵌入单体胺和/或酰胺接触而形成的嵌入体，以在层状材料的相邻片晶之间吸附或插入插入剂单体。在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在约10-45安士，使得插入物容易被剥离成单独的血小板。插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。或者，插入的复合物可以在与有机液体或基质聚合物组合之前被剥离。

10. 发明授权

US06287634B1 Intercalates and exfoliates formed with monomeric ethers and esters; composite materials containing same methods of modifying rheology therewith 失效
标题翻译：用单体醚和酯形成的插层和去角质; 含有与其一起改性流变性的相同方法的复合材料
公开(公告)号：US06287634B1
公开(公告)日：2001-09-11
申请号：US08577700
申请日：1995-12-22
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： B05D700
CPC分类号： C08K9/04 , C01B33/44
摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer ether and/or ester to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 Å (as measured after water removal to a maximum of 5% by weight water), up to about 100 Å and preferably in the range of about 10-45 Å, so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to combination with the organic liquid or the matrix polymer.
摘要翻译：通过使层状材料（例如页硅酸盐）与嵌入单体醚和/或酯接触而形成的嵌入体，以在层状材料的相邻片晶之间吸附或插入插入剂单体。在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5埃的水平（在除水后测量为最多5重量％的水），至多约100埃，优选在约10-45埃，使得插入物容易被剥离成单独的血小板。插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。或者，插入的复合物可以在与有机液体或基质聚合物组合之前被剥离。

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