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1. 发明授权

US06821474B2 Method for preparing dielectric composite materials 失效
标题翻译：介电复合材料的制备方法
公开(公告)号：US06821474B2
公开(公告)日：2004-11-23
申请号：US10391366
申请日：2003-03-18
申请人： Robert J. Lauf , Kimberly K. Anderson , Frederick C. Montgomery , Jack L. Collins , John J. Felten
发明人： Robert J. Lauf , Kimberly K. Anderson , Frederick C. Montgomery , Jack L. Collins , John J. Felten
IPC分类号： H05B600
CPC分类号： C01G23/003 , C01G23/006 , C01G23/0536 , C01P2004/60 , C01P2004/61 , C04B35/462 , C04B35/468 , C04B35/472 , C04B35/6281 , C04B35/62886 , C04B2235/02 , C04B2235/3215 , C04B2235/3224 , C04B2235/3232 , C04B2235/3236 , C04B2235/3296 , C04B2235/44 , C04B2235/449 , C04B2235/528 , C04B2235/79 , C04B2235/94 , H01G4/206 , H05K1/162
摘要： The invention allows the fabrication of small, dense beads of dielectric materials with selected compositions, which are incorporated into a polymeric matrix for use in capacitors, filters, and the like. A porous, generally spherical bead of hydrous metal oxide containing titanium or zirconium is made by a sol-gel process to form a substantially rigid bead having a generally fine crystallite size and correspondingly finely distributed internal porosity. The resulting gel bead may be washed and hydrothermally reacted with a soluble alkaline earth salt (typically Ba or Sr) at elevated temperature and pressure to convert the bead into a mixed hydrous titanium- or zirconium-alkaline earth oxide while retaining the generally spherical shape. Alternatively, the gel bead may be made by coprecipitation. This mixed oxide bead is then washed, dried and calcined to produce the desired (BaTiO3, PbTiO3, SrZrO3) structure. The sintered beads are incorporated into a selected polymer matrix. The resulting dielectric composite material may be electrically “poled” if desired.
摘要翻译：本发明允许制造具有所选组合物的小而致密的电介质材料的珠粒，其被并入用于电容器，过滤器等中的聚合物基质中。通过溶胶 - 凝胶法制备含有钛或锆的含水金属氧化物的多孔，通常为球形的珠粒，以形成具有通常微细尺寸和相应地精细分布的内部孔隙率的基本刚性的珠粒。所得到的凝胶珠可以在升高的温度和压力下与可溶性碱土金属盐（通常为Ba或Sr）进行洗涤和水热反应，以将珠粒转化为混合的含水钛或锆 - 碱土金属氧化物，同时保持大致球形。或者，凝胶珠可以通过共沉淀制成。然后将该混合氧化物珠洗涤，干燥并煅烧以产生所需的（BaTiO 3，PbTiO 3，SrZrO 3）结构。将烧结的珠子并入选定的聚合物基质中。如果需要，所得到的电介质复合材料可以电“极化”。

2. 发明授权

US06600645B1 Dielectric composite materials and method for preparing 失效
标题翻译：介电复合材料及其制备方法
公开(公告)号：US06600645B1
公开(公告)日：2003-07-29
申请号：US10256843
申请日：2002-09-27
申请人： Robert J. Lauf , Kimberly K. Anderson , Frederick C. Montgomery , Jack L. Collins , John J. Felten
发明人： Robert J. Lauf , Kimberly K. Anderson , Frederick C. Montgomery , Jack L. Collins , John J. Felten
IPC分类号： H01G406
CPC分类号： C01G23/003 , C01G23/006 , C01G23/0536 , C01P2004/60 , C01P2004/61 , C04B35/462 , C04B35/468 , C04B35/472 , C04B35/6281 , C04B35/62886 , C04B2235/02 , C04B2235/3215 , C04B2235/3224 , C04B2235/3232 , C04B2235/3236 , C04B2235/3296 , C04B2235/44 , C04B2235/449 , C04B2235/528 , C04B2235/79 , C04B2235/94 , H01G4/206 , H05K1/162
摘要： The invention allows the fabrication of small, dense beads of dielectric materials with selected compositions, which are incorporated into a polymeric matrix for use in capacitors, filters, and the like. A porous, generally spherical bead of hydrous metal oxide containing titanium or zirconium is made by a sol-gel process to form a substantially rigid bead having a generally fine crystallite size and correspondingly finely distributed internal porosity. The resulting gel bead may be washed and hydrothermally reacted with a soluble alkaline earth salt (typically Ba or Sr) at elevated temperature and pressure to convert the bead into a mixed hydrous titanium- or zirconium-alkaline earth oxide while retaining the generally spherical shape. Alternatively, the gel bead may be made by coprecipitation. This mixed oxide bead is then washed, dried and calcined to produce the desired (BaTiO3, PbTiO3, SrZrO3) structure. The sintered beads are incorporated into a selected polymer matrix. The resulting dielectric composite material may be electrically “poled” if desired.
摘要翻译：本发明允许制造具有所选组合物的小而致密的电介质材料的珠粒，其被并入用于电容器，过滤器等中的聚合物基质中。通过溶胶 - 凝胶法制备含有钛或锆的含水金属氧化物的多孔，通常为球形的珠粒，以形成具有通常微细尺寸和相应地精细分布的内部孔隙率的基本刚性的珠粒。所得到的凝胶珠可以在升高的温度和压力下与可溶性碱土金属盐（通常为Ba或Sr）进行洗涤和水热反应，以将珠粒转化成混合的含水钛或锆 - 碱土金属氧化物，同时保持大致球形。或者，凝胶珠可以通过共沉淀制成。然后将该混合氧化物珠洗涤，干燥并煅烧以产生所需的（BaTiO 3，PbTiO 3，SrZrO 3）结构。将烧结的珠子并入选定的聚合物基质中。如果需要，所得到的电介质复合材料可以电“极化”。

3. 发明授权

US06492016B1 Method for preparing spherical ferrite beads and use thereof 失效
标题翻译：制备球形铁氧体磁珠的方法及其用途
公开(公告)号：US06492016B1
公开(公告)日：2002-12-10
申请号：US09917356
申请日：2001-07-27
申请人： Robert J. Lauf , Kimberly K. Anderson , Frederick C. Montgomery , Jack L. Collins
发明人： Robert J. Lauf , Kimberly K. Anderson , Frederick C. Montgomery , Jack L. Collins
IPC分类号： C01G4906
CPC分类号： H01F1/11 , C01G49/0036 , C01P2002/76 , C01P2004/20 , C01P2004/61 , C01P2004/62 , Y10T428/256 , Y10T428/257 , Y10T428/258 , Y10T428/2982
摘要： The invention allows the fabrication of small, dense, highly polished spherical beads of hexagonal ferrites with selected compositions for use in nonreciprocal microwave and mm-wave devices as well as in microwave absorbent or reflective coatings, composites, and the like. A porous, generally spherical bead of hydrous iron oxide is made by a sol-gel process to form a substantially rigid bead having a generally fine crystallite size and correspondingly finely distributed internal porosity. The resulting gel bead is washed and hydrothermally reacted with a soluble alkaline earth salt (typically Ba or Sr) under conditions of elevated temperature and pressure to convert the bead into a mixed hydrous iron-alkaline earth oxide while retaining the generally spherical shape. This mixed oxide bead is then washed, dried, and calcined to produce the desired (BaFe12O19 or SrFe12O19) crystal structure. The calcined bead is then sintered to form a dense bead of the BaFe12O19 and SrFe12O19 phase suitable for polishing and incorporation into various microwave devices and components.
摘要翻译：本发明允许制造用于非互易微波和毫米波装置以及微波吸收或反射涂层，复合材料等的选定组合物的小而致密，高度抛光的六方晶系铁氧体球形珠。通过溶胶 - 凝胶法制备多孔的，通常为球形的含水氧化铁珠，以形成具有通常微细尺寸和相应地精细分布的内部孔隙率的基本刚性的珠粒。在升高的温度和压力的条件下，将所得凝胶珠洗涤并与可溶性碱土金属盐（通常为Ba或Sr）水热反应，以将珠粒转化为混合的含水铁 - 碱土金属氧化物，同时保持大致球形。然后将该混合氧化物珠粒洗涤，干燥并煅烧以产生所需的（BaFe12O19或SrFe12O19）晶体结构。然后将煅烧的珠粒烧结以形成适合抛光并掺入各种微波装置和组件的BaFe12O19和SrFe12O19相的致密珠粒。

4. 发明授权

US06899827B2 Inorganic optical taggant and method of making 失效
标题翻译：无机光学标签和制作方法
公开(公告)号：US06899827B2
公开(公告)日：2005-05-31
申请号：US10439608
申请日：2003-05-16
申请人： Robert J. Lauf , Kimberly K. Anderson , Frederick C. Montgomery
发明人： Robert J. Lauf , Kimberly K. Anderson , Frederick C. Montgomery
IPC分类号： C09K11/00 , C09K11/77 , H01M4/00 , H01M6/10
CPC分类号： C09K11/7729 , C01B25/372 , C01G23/04 , C01G25/02 , C01P2002/54 , C01P2004/61 , C01P2006/60 , C04B35/44 , C04B35/486 , C04B35/624 , C04B2235/3224 , C04B2235/3229 , C04B2235/764 , C04B2235/94 , C04B2235/9653 , Y10S149/123 , Y10S252/965
摘要： Sintered, translucent ceramic microbeads, preferably alumina, titania, zirconia, yttria, zirconium phosphate, or yttrium aluminum garnet (YAG) are doped with one or more optically active species. The beads may be added to substances such as explosives in order to create a distinctive optical signature that identifies a manufacturer, lot number, etc. in the event of the need for forensic analysis. Because the beads have a generally spherical surface, the radius of curvature provides an additional distinguishing characteristic by which a particular sample may be identified. The beads could also be formulated into paints if needed to create distinctive optical signatures for camouflage, decoys, or other countermeasures and could also be applied as a dust to track the movement of personnel, vehicles, etc.
摘要翻译：烧结的，半透明的陶瓷微珠，优选氧化铝，二氧化钛，氧化锆，氧化钇，磷酸锆或钇铝石榴石（YAG）掺杂有一种或多种光学活性物质。珠子可以添加到诸如爆炸物的物质中，以便在需要法医分析的情况下创建识别制造商，批号等的特征性光学特征。由于珠具有通常为球形的表面，所以曲率半径提供了可以识别特定样品的另外的区别特征。如果需要，珠子也可以配制成油漆，以产生伪装，诱饵或其他对策的独特的光学特征，也可以作为灰尘来应用以跟踪人员，车辆等的运动。

5. 发明授权

US06599493B2 Method for preparing hydrous iron oxide gels and spherules 失效
标题翻译：水合氧化铁凝胶和球晶的制备方法
公开(公告)号：US06599493B2
公开(公告)日：2003-07-29
申请号：US09917117
申请日：2001-07-27
申请人： Jack L. Collins , Robert J. Lauf , Kimberly K. Anderson
发明人： Jack L. Collins , Robert J. Lauf , Kimberly K. Anderson
IPC分类号： C01G4900
CPC分类号： C01G49/02 , C01G49/0036 , C01P2004/32 , C01P2004/62
摘要： The present invention is directed to methods for preparing hydrous iron oxide spherules, hydrous iron oxide gels such as gel slabs, films, capillary and electrophoresis gels, iron monohydrogen phosphate spherules, hydrous iron oxide spherules having suspendable particles homogeneously embedded within to form composite sorbents and catalysts, iron monohydrogen phosphate spherules having suspendable particles of at least one different sorbent homogeneously embedded within to form a composite sorbent, iron oxide spherules having suspendable particles homogeneously embedded within to form a composite of hydrous iron oxide fiber materials, iron oxide fiber materials, hydrous iron oxide fiber materials having suspendable particles homogeneously embedded within to form a composite, iron oxide fiber materials having suspendable particles homogeneously embedded within to form a composite, dielectric spherules of barium, strontium, and lead ferrites and mixtures thereof, and composite catalytic spherules of barium or strontium ferrite embedded with oxides of Mg, Zn, Pb, Ce and mixtures thereof. These variations of hydrous iron oxide spherules and gel forms prepared by the gel-sphere, internal gelation process offer more useful forms of inorganic ion exchangers, catalysts, getters, dielectrics, and ceramics.
摘要翻译：本发明涉及制备含水氧化铁球，含水氧化铁凝胶如凝胶板，薄膜，毛细管和电泳凝胶，单磷酸铁球，含有均匀嵌入其中的悬浮颗粒的含水氧化铁球，形成复合吸附剂的方法，催化剂，具有均匀嵌入以形成复合吸附剂的至少一种不同吸附剂的悬浮颗粒的磷酸一氢化铁小球，具有均匀嵌入其中的可悬浮颗粒的氧化铁球，形成水合氧化铁纤维材料，氧化铁纤维材料，含水具有均匀地嵌入其中以形成复合材料的悬浮颗粒的氧化铁纤维材料，具有均匀地嵌入其中的可悬浮颗粒的氧化铁纤维材料，以形成钡，锶和铅铁氧体的介电球，及其混合物，以及复合催化剂包含Mg，Zn，Pb，Ce的氧化物的钡或锶铁氧体的球体及其混合物。通过凝胶球，内部凝胶化方法制备的含水氧化铁球和凝胶形式的这些变化提供了更有用的无机离子交换剂，催化剂，吸气剂，电介质和陶瓷的形式。

6. 发明授权

US06248286B1 Method of making a functionally graded material 失效
标题翻译：制作功能分级材料的方法
公开(公告)号：US06248286B1
公开(公告)日：2001-06-19
申请号：US09453774
申请日：1999-12-03
申请人： Robert J. Lauf , Paul A. Menchhofer , Claudia A. Walls
发明人： Robert J. Lauf , Paul A. Menchhofer , Claudia A. Walls
IPC分类号： B28B114
CPC分类号： B28B1/008 , B22F7/06 , B22F2999/00 , B28B1/00 , C04B35/117 , B22F2207/01 , B22F3/22
摘要： A gelcasting method of making an internally graded article includes the steps of: preparing at least two slurries, each of the slurries including a different gelcastable powder suspended in a gelcasting solution, the slurries characterized by having comparable shrinkage upon drying and sintering thereof; casting the slurries into a mold having a selected shape, wherein relative proportions of the slurries is varied in at least one direction within the selected shape; gelling the slurries to form a solid gel while preserving the variation in relative proportions of the slurries; drying the gel to form a dried green body; and sintering the dry green body to form a solid object, at least one property thereof varying because of the variation in relative proportions of the starting slurries. A gelcasting method of making an internally graded article alternatively includes the steps of: preparing a slurry including a least two different phases suspended in a gelcasting solution, the phases characterized by having different settling characteristics; casting the slurry into a mold having a selected shape; allowing the slurry to stand for a sufficient period of time to permit desired gravitational fractionation in order to achieve a vertical compositional gradient in the molded slurry; gelling the slurry to form a solid gel while preserving the vertical compositional gradient in the molded slurry; drying the gel to form a dried green body; and sintering the dry green body to form a solid object, at least one property thereof varying along the vertical direction because of the compositional gradient in the molded slurry.
摘要翻译：制备内部分级制品的凝胶浇铸方法包括以下步骤：制备至少两种浆料，每种浆料包括悬浮在凝胶浇注溶液中的不同的可凝胶涂覆粉末，其特征在于其干燥和烧结时具有相当的收缩率; 将浆料浇铸到具有选定形状的模具中，其中浆料的相对比例在所选形状内的至少一个方向上变化; 胶凝形成固体凝胶，同时保持浆料相对比例的变化; 干燥凝胶以形成干燥的生坯; 并且将干燥的生坯烧结以形成固体物体，由于起始浆料的相对比例的变化，其至少一种性质变化。制备内部分级制品的凝胶浇铸方法交替包括以下步骤：制备包含悬浮在凝胶浇注溶液中的至少两个不同相的浆料，其特征在于具有不同的沉降特性; 将浆料浇注到具有选定形状的模具中; 允许浆料静置足够的时间以允许所需的重力分馏，以便在模制浆料中达到垂直组分梯度; 将浆料胶凝以形成固体凝胶，同时保持模制浆料中的垂直组分梯度; 干燥凝胶以形成干燥的生坯; 并且将干燥的生坯烧结以形成固体物体，由于模制浆料中的组成梯度，其至少一种特性沿垂直方向变化。

7. 发明授权

US5742211A Radio-frequency and microwave load comprising a carbon-bonded carbon fiber composite 失效
标题翻译：包含碳键碳纤维复合材料的射频和微波载荷
公开(公告)号：US5742211A
公开(公告)日：1998-04-21
申请号：US620616
申请日：1996-03-22
申请人： Robert J. Lauf , April D. McMillan , Arvid C. Johnson , Carl A. Everleigh , Arthur J. Moorhead
发明人： Robert J. Lauf , April D. McMillan , Arvid C. Johnson , Carl A. Everleigh , Arthur J. Moorhead
IPC分类号： H01P1/22 , H01P1/26
CPC分类号： H01P1/22 , H01P1/26
摘要： A billet of low-density carbon-bonded carbon fiber (CBCF) composite is machined into a desired attenuator or load element shape (usually tapering). The CBCF composite is used as a free-standing load element or, preferably, brazed to the copper, brass or aluminum components of coaxial transmission lines or microwave waveguides. A novel braze method was developed for the brazing step. The resulting attenuator and/or load devices are robust, relatively inexpensive, more easily fabricated, and have improved performance over conventional graded-coating loads.
摘要翻译：将低密度碳键合碳纤维（CBCF）复合材料的坯料加工成所需的衰减器或负载元件形状（通常是锥形的）。 CBCF复合材料用作独立的负载元件，或者优选地钎焊到同轴传输线或微波波导的铜，黄铜或铝组件。开发了用于钎焊步骤的新型钎焊方法。所得到的衰减器和/或负载装置是鲁棒的，相对便宜的，更容易制造的，并且具有比常规分级涂层负载更好的性能。

8. 发明授权

US5648180A Method for joining carbon-carbon composites to metals 失效
标题翻译：将碳 - 碳复合材料与金属接合的方法
公开(公告)号：US5648180A
公开(公告)日：1997-07-15
申请号：US620509
申请日：1996-03-22
申请人： Robert J. Lauf , April D. McMillan , Arthur J. Moorhead
发明人： Robert J. Lauf , April D. McMillan , Arthur J. Moorhead
IPC分类号： B23K35/00 , B23K35/32 , C04B37/02 , B32B5/14 , B23K35/22 , B32B15/04
CPC分类号： B23K35/007 , C04B35/63496 , C04B35/83 , C04B37/026 , C04B37/028 , B23K35/325 , C04B2235/6567 , C04B2235/775 , C04B2237/086 , C04B2237/122 , C04B2237/124 , C04B2237/126 , C04B2237/32 , C04B2237/385 , C04B2237/406 , C04B2237/407 , C04B2237/52 , C04B2237/72 , Y10T428/12625
摘要： A method for joining carbon-carbon composites to metals by brazing. Conventional brazing of recently developed carbon-bonded carbon fiber (CBCF) material to a metal substrate is limited by the tendency of the braze alloy to "wick" into the CBCF composite rather than to form a strong bond. The surface of the CBCF composite that is to be bonded is first sealed with a fairly dense carbonaceous layer achieved by any of several methods. The sealed surface is then brazed to the metal substrate by vacuum brazing with a Ti-Cu-Be alloy.
摘要翻译：通过钎焊将碳 - 碳复合材料与金属接合的方法。最近开发的碳键合碳纤维（CBCF）材料对金属基底的常规钎焊受到钎焊合金“吸”到CBCF复合材料而不是形成强键的倾向的限制。首先将要结合的CBCF复合材料的表面用几种方法中的任一种实现的相当致密的碳质层密封。然后通过与Ti-Cu-Be合金的真空钎焊将密封的表面钎焊到金属基底上。

9. 发明授权

US5503898A Method for producing textured substrates for thin-film photovoltaic cells 失效
标题翻译：用于生产用于薄膜光伏电池的织构化衬底的方法
公开(公告)号：US5503898A
公开(公告)日：1996-04-02
申请号：US229944
申请日：1994-04-19
申请人： Robert J. Lauf
发明人： Robert J. Lauf
IPC分类号： H01L31/0236 , H01L31/0392 , H01L31/18 , H01L31/04
CPC分类号： H01L31/0236 , H01L31/0392 , H01L31/18 , Y02E10/50 , Y10S438/967 , Y10T428/24421
摘要： The invention pertains to the production of ceramic substrates used in the manufacture of thin-film photovoltaic cells used for directly converting solar energy to electrical energy. Elongated ribbon-like sheets of substrate precursor containing a mixture of ceramic particulates, a binder, and a plasticizer are formed and then while green provided with a mechanically textured surface region used for supporting the thin film semiconductor of the photovoltaic cell when the sheets of the substrate precursor are subsequently cut into substrate-sized shapes and then sintered. The textured surface pattern on the substrate provides enhanced light trapping and collection for substantially increasing the, solar energy conversion efficiency of thin-film photovoltaic cells.
摘要翻译：本发明涉及用于制造用于将太阳能直接转换为电能的薄膜光伏电池的陶瓷基板的制造。形成包含陶瓷颗粒，粘合剂和增塑剂的混合物的细长带状的基材前体片，然后当绿色设置有用于支撑光伏电池的薄膜半导体的机械纹理表面区域时然后将衬底前体切割成基底尺寸的形状，然后烧结。衬底上纹理化的表面图案提供了增强的光捕获和收集，以显着增加薄膜光伏电池的太阳能转换效率。

10. 发明授权

US5306646A Method for producing textured substrates for thin-film photovoltaic cells 失效
标题翻译：用于生产用于薄膜光伏电池的织构化衬底的方法
公开(公告)号：US5306646A
公开(公告)日：1994-04-26
申请号：US996328
申请日：1992-12-23
申请人： Robert J. Lauf
发明人： Robert J. Lauf
IPC分类号： H01L31/0236 , H01L31/0392 , H01L31/18
CPC分类号： H01L31/0236 , H01L31/0392 , H01L31/18 , Y02E10/50 , Y10S438/967 , Y10T428/24421
摘要： The invention pertains to the production of ceramic substrates used in the manufacture of thin-film photovoltaic cells used for directly converting solar energy to electrical energy. Elongated ribbon-like sheets of substrate precursor containing a mixture of ceramic particulates, a binder, and a plasticizer are formed and then while green provided with a mechanically textured surface region used for supporting the thin film semiconductor of the photovoltaic cell when the sheets of the substrate precursor are subsequently cut into substrate-sized shapes and then sintered. The textured surface pattern on the substrate provides enhanced light trapping and collection for substantially increasing the solar energy conversion efficiency of thin-film photovoltaic cells.
摘要翻译：本发明涉及用于制造用于将太阳能直接转换为电能的薄膜光伏电池的陶瓷基板的制造。形成包含陶瓷颗粒，粘合剂和增塑剂的混合物的细长带状的基材前体片，然后当绿色设置有用于支撑光伏电池的薄膜半导体的机械纹理表面区域时然后将衬底前体切割成基底尺寸的形状，然后烧结。衬底上的纹理表面图案提供了增强的光捕获和收集，以显着提高薄膜光伏电池的太阳能转换效率。

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