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1. 发明授权

US08674149B2 Oxidative mono-halogenation of methane 有权
标题翻译：甲烷的氧化单卤化
公开(公告)号：US08674149B2
公开(公告)日：2014-03-18
申请号：US13123908
申请日：2009-08-19
申请人： Robert G. Bowman , Eric E. Stangland , Mark E. Jones , Dean M. Millar , Simon G. Podkolzin , Brien A. Stears , Richard M. Wehmeyer
发明人： Robert G. Bowman , Eric E. Stangland , Mark E. Jones , Dean M. Millar , Simon G. Podkolzin , Brien A. Stears , Richard M. Wehmeyer
IPC分类号： C07C17/154 , C07C19/03
CPC分类号： C07C17/154 , C07C19/03
摘要： Oxidatively halogenate methane by placing a feedstream that comprises methane, a source of halogen, a source of oxygen and, optionally, a source of diluent gas in contact with a first catalyst (e.g. a solid super acid or a solid super base) that has greater selectivity to methyl halide and carbon monoxide than to methylene halide, trihalomethane or carbon tetrahalide. Improve overall selectivity to methyl halide by using a second catalyst that converts at least part of the feedstream to a mixture of methyl halide, methylene halide, trihalomethane, carbon tetrahalide and unreacted oxygen, and placing that mixture in contact with the first catalyst which converts at least a portion of the methylene halide, trihalomethane and carbon tetrahalide to carbon monoxide, hydrogen halide and water.
摘要翻译：通过放置包含甲烷，卤素源，氧源和任选的稀释气体源的进料流，将第一催化剂（例如固体超强酸或固体超级碱）接触，从而氧化卤化甲烷，所述第一催化剂对甲基卤和一氧化碳的选择性高于二氯甲烷，三卤甲烷或四卤化碳。通过使用将至少部分进料流转化为甲基卤化物，二卤甲烷，三卤代甲烷，四卤化碳和未反应的氧的混合物的第二催化剂来提高对甲基卤的总体选择性，并将该混合物与第一种催化剂接触，二卤甲烷，三卤代甲烷和四卤化碳中的至少一部分与一氧化碳，卤化氢和水反应。

2. 发明申请

US20110201841A1 OXIDATIVE MONO-HALOGENATION OF METHANE 有权
标题翻译：氧化甲烷的单氧化反应
公开(公告)号：US20110201841A1
公开(公告)日：2011-08-18
申请号：US13123908
申请日：2009-08-19
申请人： Robert G. Bowman , Eric E. Stangland , Mark E. Jones , Dean M. Millar , Simon G. Podkolzin , Brien A. Stears , Richard M. Wehmeyer
发明人： Robert G. Bowman , Eric E. Stangland , Mark E. Jones , Dean M. Millar , Simon G. Podkolzin , Brien A. Stears , Richard M. Wehmeyer
IPC分类号： C07C51/14 , C07C17/013
CPC分类号： C07C17/154 , C07C19/03
摘要： Oxidatively halogenate methane by placing a feedstream that comprises methane, a source of halogen, a source of oxygen and, optionally, a source of diluent gas in contact with a first catalyst (e.g. a solid super acid or a solid super base) that has greater selectivity to methyl halide and carbon monoxide than to methylene halide, trihalomethane or carbon tetrahalide. Improve overall selectivity to methyl halide by using a second catalyst that converts at least part of the feedstream to a mixture of methyl halide, methylene halide, trihalomethane, carbon tetrahalide and unreacted oxygen, and placing that mixture in contact with the first catalyst which converts at least a portion of the methylene halide, trihalomethane and carbon tetrahalide to carbon monoxide, hydrogen halide and water.
摘要翻译：通过放置包含甲烷，卤素源，氧源和任选的稀释气体源的进料流，将第一催化剂（例如固体超强酸或固体超级碱）接触，从而氧化卤化甲烷，所述第一催化剂对甲基卤和一氧化碳的选择性高于二氯甲烷，三卤甲烷或四卤化碳。通过使用将至少部分进料流转化为甲基卤化物，二卤甲烷，三卤代甲烷，四卤化碳和未反应的氧的混合物的第二催化剂来提高对甲基卤的总体选择性，并将该混合物与第一种催化剂接触，二卤甲烷，三卤代甲烷和四卤化碳中的至少一部分与一氧化碳，卤化氢和水反应。

3. 发明授权

US09233367B2 Process for synthesis of molybdenum sulfide-based catalysts 有权
标题翻译：硫化钼基催化剂的合成工艺
公开(公告)号：US09233367B2
公开(公告)日：2016-01-12
申请号：US14008774
申请日：2011-04-01
申请人： Robert J. Gulotty, Jr. , Dean M. Millar , Albert E. Schweizer, Jr. , Raymond M. Collins
发明人： Robert J. Gulotty, Jr. , Dean M. Millar , Albert E. Schweizer, Jr. , Raymond M. Collins
IPC分类号： B01J37/20 , B01J23/88 , B01J23/882 , B01J27/051 , B01J35/02 , B01J37/00 , B01J37/02 , B01J37/03 , B01J37/08 , B01J37/16 , C01G51/00
CPC分类号： B01J37/20 , B01J23/88 , B01J23/882 , B01J27/051 , B01J27/0515 , B01J35/023 , B01J37/0045 , B01J37/0236 , B01J37/033 , B01J37/08 , B01J37/16 , C01G51/30
摘要： A process for preparing a molybdenum sulfide-based catalyst comprises drying a precipitated molybdenum sulfide-based catalyst precursor, for example, a wet filter cake, such that a particulate catalyst precursor, containing from 12 to 15 percent by weight water, is formed. The particulate catalyst precursor is desirably in the form of free-flowing particles. The particulate catalyst precursor is then auto-reduced. A rotary furnace that subjects the catalyst precursor to at least two zones having distinct temperatures may be conveniently used for drying, auto-reduction, or both. The staged drying and auto-reduction steps reduce the tendency of the precursor to self-heat, which is undesirable because it reduces both the activity and selectivity of the final catalyst.
摘要翻译：制备硫化钼基催化剂的方法包括干燥沉淀的硫化钼基催化剂前体，例如湿滤饼，使得形成含有12至15重量％水的颗粒状催化剂前体。颗粒状催化剂前体理想地是自由流动的颗粒的形式。然后将颗粒状催化剂前体自动还原。使催化剂前体经受至少两个具有不同温度的区域的旋转炉可以方便地用于干燥，自动还原或两者。分阶段的干燥和自动还原步骤降低了前体自热的倾向，这是不希望的，因为它降低了最终催化剂的活性和选择性。

4. 发明申请

US20120208695A1 SUPPORTED RHODIUM SYNTHESIS GAS CONVERSION CATALYST COMPOSITIONS 审中-公开
标题翻译：支持铑合成气转化催化剂组合物
公开(公告)号：US20120208695A1
公开(公告)日：2012-08-16
申请号：US13501108
申请日：2010-11-02
申请人： Billy B. Bardin , David G. Barton , Adam Chojecki , Howard W. Clark , Daniela Ferrari , Robert J. Gulotty, JR. , Yu Liu , Mark H. McAdon , Dean M. Millar , Neelesh Rane , Hendrik E. Tuinstra
发明人： Billy B. Bardin , David G. Barton , Adam Chojecki , Howard W. Clark , Daniela Ferrari , Robert J. Gulotty, JR. , Yu Liu , Mark H. McAdon , Dean M. Millar , Neelesh Rane , Hendrik E. Tuinstra
IPC分类号： B01J21/08 , B01J21/06 , B01J21/04 , B01J21/10
CPC分类号： B01J23/6527 , B01J21/04 , B01J21/10 , B01J23/6482 , B01J23/6525 , B01J23/6562 , B01J23/6567 , B01J37/0203 , B01J37/0205 , B01J37/0207
摘要： A supported catalyst composition suitable for use in converting synthesis gas to alcohols comprises a catalytic metal, a catalyst promoter and a catalyst support.
摘要翻译：适用于将合成气转化为醇的负载催化剂组合物包括催化金属，催化剂促进剂和催化剂载体。

5. 发明申请

US20130047843A1 Metal Organic Framework Filled Polymer Based Membranes 审中-公开
标题翻译：金属有机骨架填充聚合物膜
公开(公告)号：US20130047843A1
公开(公告)日：2013-02-28
申请号：US13577577
申请日：2011-02-11
申请人： Scott T. Matteucci , Leonardo C. Lopez , Shawn D. Feist , Peter N. Nickias , Dean M. Millar , Michael P. Tate
发明人： Scott T. Matteucci , Leonardo C. Lopez , Shawn D. Feist , Peter N. Nickias , Dean M. Millar , Michael P. Tate
IPC分类号： C08L77/12 , B01D53/22 , C08L75/06
CPC分类号： B01D67/0079 , B01D53/228 , B01D69/148 , B01D71/028 , B01D71/56 , B01D71/80
摘要： A membrane for separation of gases, the membrane including a metal-organic phase and a polymeric phase, the metal-organic phase having porous crystalline metal compounds and ligands, the polymeric phase having a molecularly self assembling polymer.
摘要翻译：用于分离气体的膜，所述膜包括金属 - 有机相和聚合物相，所述金属 - 有机相具有多孔结晶金属化合物和配体，所述聚合物相具有分子自组装聚合物。

6. 发明申请

US20130029841A1 CATALYST COMPOSITIONS FOR PRODUCING MIXED ALCOHOLS 有权
标题翻译：用于生产混合的醇的催化剂组合物
公开(公告)号：US20130029841A1
公开(公告)日：2013-01-31
申请号：US13639105
申请日：2011-03-30
申请人： Daniela Ferrari , Neelesh J. Rane , Adam Chojecki , Gerolamo Budroni , David G. Barton , Mark H. McAdon , Robert J. Gulotty, JR. , Dean M. Millar , Palanichamy Manikandan
发明人： Daniela Ferrari , Neelesh J. Rane , Adam Chojecki , Gerolamo Budroni , David G. Barton , Mark H. McAdon , Robert J. Gulotty, JR. , Dean M. Millar , Palanichamy Manikandan
IPC分类号： B01J23/652 , B01J23/656
CPC分类号： B01J23/6482 , B01J21/04 , B01J23/002 , B01J23/6525 , B01J23/6562 , B01J23/6567 , B01J37/0205 , B01J2523/00 , B01J2523/13 , B01J2523/55 , B01J2523/68 , B01J2523/74 , B01J2523/827 , B01J2523/48 , B01J2523/824
摘要： Catalyst compositions for producing mixed alcohols from a synthesis gas feed. The catalyst composition comprises a catalytic metal combination on a catalyst support, a first optional promoter and a second optional promoter, where the catalytic metal combination consists essentially of iridium, vanadium, and molybdenum.
摘要翻译：用于从合成气进料生产混合醇的催化剂组合物。催化剂组合物包括在催化剂载体上的催化金属组合，第一任选的促进剂和第二任选的促进剂，其中催化金属组合基本上由铱，钒和钼组成。

7. 发明授权

US5397560A Microporous crystalline aluminosilicate designated DCM-2 失效
标题翻译：称为DCM-2的微孔结晶硅铝酸盐
公开(公告)号：US5397560A
公开(公告)日：1995-03-14
申请号：US137652
申请日：1993-10-15
申请人： Dean M. Millar , Gregg E. Lewis , Juan M. Garces
发明人： Dean M. Millar , Gregg E. Lewis , Juan M. Garces
IPC分类号： B01J29/06 , B01J29/70 , C01B39/46 , C07C1/20 , C07C1/26 , C01B33/34
CPC分类号： C01B39/46 , B01J29/06 , B01J29/70 , C07C1/20 , C07C1/26 , C07C2529/70 , Y02P30/42
摘要： A novel microporous crystalline aluminosilicate designated DCM-2 is disclosed. The composition, as synthesized, contains lithium cations and is represented by the oxide composition: Li.sub.2 O.multidot.Al.sub.2 O.sub.3 .multidot.10SiO.sub.2. The lithium cations may be exchanged with hydrogen ions, and in the acid form the composition is useful as an adsorbent and as a catalyst for converting alkyl halides and alkanols to light hydrocarbons.
摘要翻译：公开了一种称为DCM-2的新型微孔结晶硅铝酸盐。合成的组合物含有锂阳离子，并由氧化物组成：Li2OxAl2O3×10SiO2表示。锂阳离子可以与氢离子交换，并且在酸形式中，组合物可用作吸附剂和用作将烷基卤化物和链烷醇转化成轻质烃的催化剂。

8. 发明授权

US08598239B2 Anderson-type heteropoly compound-based catalyst compositions and their use conversion of synthesis gas to oxygenates 有权
标题翻译：安德森型杂多化合物基催化剂组合物及其将合成气转化为含氧化合物
公开(公告)号：US08598239B2
公开(公告)日：2013-12-03
申请号：US13825607
申请日：2011-09-26
申请人： Palanichamy Manikandan , David G. Barton , Dean M. Millar
发明人： Palanichamy Manikandan , David G. Barton , Dean M. Millar
IPC分类号： C07C27/00
CPC分类号： B01J27/24 , B01J23/28 , B01J23/6525 , B01J23/6527 , B01J23/882 , B01J23/8993 , B01J35/0006 , B01J37/0009 , B01J37/031 , C07C29/157 , C07C29/158 , C07C29/16 , C07C45/50 , C07C31/10 , C07C31/08
摘要： Use a transition metal-containing, Anderson-type heteropoly compound catalyst to convert synthesis gas to an oxygenate, especially an alcohol that contains from one carbon atom to six carbon atoms.
摘要翻译：使用含过渡金属的Anderson型杂多化合物催化剂将合成气转化为含氧化合物，特别是含有一个碳原子至六个碳原子的醇。

9. 发明申请

US20130190411A1 ANDERSON-TYPE HETEROPOLY COMPOUND-BASED CATALYST COMPOSITIONS AND THEIR USE CONVERSION OF SYNTHESIS GAS TO OXYGENATES 有权
标题翻译：安德森型异构体化合物催化剂组合物及其合成气对氧化剂的使用转化
公开(公告)号：US20130190411A1
公开(公告)日：2013-07-25
申请号：US13825607
申请日：2011-09-26
申请人： Palanichamy Manikandan , David G. Barton , Dean M. Millar
发明人： Palanichamy Manikandan , David G. Barton , Dean M. Millar
IPC分类号： B01J27/24 , C07C29/158 , C07C45/50 , C07C29/157
CPC分类号： B01J27/24 , B01J23/28 , B01J23/6525 , B01J23/6527 , B01J23/882 , B01J23/8993 , B01J35/0006 , B01J37/0009 , B01J37/031 , C07C29/157 , C07C29/158 , C07C29/16 , C07C45/50 , C07C31/10 , C07C31/08
摘要： Use a transition metal-containing, Anderson-type heteropoly compound catalyst to convert synthesis gas to an oxygenate, especially an alcohol that contains from one carbon atom to six carbon atoms.
摘要翻译：使用含过渡金属的Anderson型杂多化合物催化剂将合成气转化为含氧化合物，特别是含有一个碳原子至六个碳原子的醇。

10. 发明授权

US5589153A Synthesis of crystalline porous solids in ammonia 失效
标题翻译：在氨中合成结晶多孔固体
公开(公告)号：US5589153A
公开(公告)日：1996-12-31
申请号：US460166
申请日：1995-06-02
申请人： Juan M. Garces , Dean M. Millar , Kevin E. Howard
发明人： Juan M. Garces , Dean M. Millar , Kevin E. Howard
IPC分类号： C01B33/38 , C01B37/02 , C01B39/02 , C01B39/48
CPC分类号： C01B39/48 , C01B37/02 , Y10S423/27
摘要： A process of preparing a crystalline porous solid selected from silicas and metallosilicates, such as, aluminosilicate zeolites or clathrasils. The process involves preparing a reaction mixture containing ammonia; water in a controlled concentration; a (hydrocarbyl)ammonium polysilicate hydrate salt; a mineralizer, such as ammonium fluoride; optionally, a source of a metal oxide, such as aluminum nitride; and optionally, a source of a charge-balancing cation or a structure directing agent; and maintaining the mixture at a temperature and for a time so as to produce the crystalline porous solid. A novel silica which is isostructural with zeolite P1 is prepared. Also prepared are a novel silica which is isostructural with zeolite beta and a novel TMA sodalite having a silica/alumina molar ratio between 12 and about 20.
摘要翻译：制备选自二氧化硅和金属硅酸盐如硅铝酸盐沸石或盐酸盐的结晶多孔固体的方法。该方法包括制备含有氨的反应混合物; 受控浓度的水; （烃基）聚硅酸铵水合物盐; 矿化剂，如氟化铵; 可选地，金属氧化物源如氮化铝; 和任选的电荷平衡阳离子源或结构导向剂; 并将混合物保持在一段温度和一段时间以产生结晶多孔固体。制备与沸石P1同构的新型二氧化硅。还制备了与沸石β同构结构的新型二氧化硅和具有12至约20的二氧化硅/氧化铝摩尔比的新型TMA方钠石。

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