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1. 发明授权

US5264534A Oriented semicrystalline polymer films 失效
标题翻译：取向的半结晶聚合物膜
公开(公告)号：US5264534A
公开(公告)日：1993-11-23
申请号：US786126
申请日：1991-10-31
申请人： Robert F. Kovar , Richard W. Lusignea , R. Ross Haghighat
发明人： Robert F. Kovar , Richard W. Lusignea , R. Ross Haghighat
IPC分类号： C08G73/10 , C08J5/18 , C08G8/02 , B29C71/00
CPC分类号： C08J5/18 , C08G73/1007 , C08J2379/08 , Y10T428/31721
摘要： Processes for producing oriented films of semicrystalline thermoplastic polymers, such as polyimides, and films produced thereby are disclosed. One process includes partial crystallization or imidization, orientation and further crystallization or imidization. Another process includes rendering a film of semicrystalline thermoplastic polymer amorphous, orienting the film and introducing crystallinity.
摘要翻译：公开了用于制造半结晶热塑性聚合物的取向膜的方法，例如聚酰亚胺，以及由此制备的膜。一种方法包括部分结晶或酰亚胺化，取向和进一步结晶或酰亚胺化。另一种方法包括使半结晶热塑性聚合物薄膜无定形，取向薄膜并引入结晶度。

2. 发明授权

US5344703A Ordered polymer/sol-gel microcomposite laminates with peek resin adhesive 失效
标题翻译：有序聚合物/溶胶 - 凝胶微复合层压板与窥视树脂粘合剂
公开(公告)号：US5344703A
公开(公告)日：1994-09-06
申请号：US137897
申请日：1993-10-13
申请人： Robert F. Kovar , R. Ross Haghighat , Richard W. Lusignea
发明人： Robert F. Kovar , R. Ross Haghighat , Richard W. Lusignea
IPC分类号： B32B7/12 , B32B17/10 , B32B3/26 , B32B27/00
CPC分类号： B32B17/10009 , B32B17/1055 , B32B17/10981 , B32B7/12 , Y10T428/249953 , Y10T428/249967 , Y10T428/249969 , Y10T428/249978 , Y10T428/24998 , Y10T428/249985 , Y10T428/249987 , Y10T428/249993 , Y10T428/31504 , Y10T428/31627
摘要： Provided are methods for laminating ordered polymers such as PBZT/sol-gel glass microcomposite film layers by first roughing the bonding surfaces of such film layers and then inserting therebetween a PEEK resin adhesive layer and compressing the film and adhesive layers together at sufficient temperature and pressure to laminate such layers. In one embodiment the ordered polymer layers are hot-pressed before surface roughing, stacking and laminating of film and adhesive layers. The invention also includes the novel laminates prepared thereby which exhibit high tensile strength, high compressive strength and good interlaminar strength, suitable for high-performance structures in e.g. aircraft, spacecraft or other structures or vehicles.
摘要翻译：提供了通过首先将这些膜层的接合表面粗化并然后将PEEK树脂粘合剂层插入其中并在足够的温度和压力下将膜和粘合剂层压在一起的方法来层压有序聚合物如PBZT /溶胶 - 凝胶玻璃微复合膜层的方法以层压这些层。在一个实施方案中，有序聚合物层在表面粗糙化，层压和层压薄膜和粘合剂层之前被热压。本发明还包括由此制备的新型层压制品，其具有高拉伸强度，高抗压强度和良好的层间强度，适用于例如高性能结构。飞机，航天器或其他结构或车辆。

3. 发明授权

US06852250B2 Compositions produced by solvent exchange methods and articles of manufacture comprising same 失效
标题翻译：通过溶剂交换方法和包含其的制品制备的组合物
公开(公告)号：US06852250B2
公开(公告)日：2005-02-08
申请号：US10211424
申请日：2002-08-01
申请人： R. Ross Haghighat , Jae Ryu , Hamid R. Mojazza , Michael A. Vinciguerra , Peter Schuler
发明人： R. Ross Haghighat , Jae Ryu , Hamid R. Mojazza , Michael A. Vinciguerra , Peter Schuler
IPC分类号： C08J3/09 , C08G61/12 , C08G73/10 , C09D5/24 , C09D165/00 , H01B1/12 , H01B13/00 , H01L51/30 , H01L51/50 , H01B1/20
CPC分类号： H01L51/5088 , C08G61/126 , C08G73/1039 , C08G73/1057 , C09D165/00 , H01G9/028 , H01G11/48 , H01G11/56 , H01L51/0037 , Y02E10/549 , Y02E60/13 , Y02P70/521
摘要： Disclosed are coatings, films, and articles of manufacture comprising or derived from compositions that are produced by a method for exchanging solvent in a mixture that includes water and an optionally substituted thiophene. Also disclosed are methods for making and using said coatings, films, and articles of manufacture, including electro-optical implementations.
摘要翻译：公开了包括或衍生自通过包含水和任选取代的噻吩的混合物中的溶剂交换的方法产生的组合物的涂料，膜和制品。还公开了制造和使用包括电光实现的所述涂层，膜和制品的方法。

4. 发明授权

US06692662B2 Compositions produced by solvent exchange methods and uses thereof 失效
公开(公告)号：US06692662B2
公开(公告)日：2004-02-17
申请号：US09999171
申请日：2001-11-30
申请人： R. Ross Haghighat , Jae Ryu , Hamid R. Mojazza , Michael A. Vinciguerra , Peter Schuler
发明人： R. Ross Haghighat , Jae Ryu , Hamid R. Mojazza , Michael A. Vinciguerra , Peter Schuler
IPC分类号： H01B112
CPC分类号： H01L51/5088 , C08G61/126 , C08G73/1039 , C08G73/1057 , C09D165/00 , H01G9/028 , H01G11/48 , H01G11/56 , H01L51/0037 , Y02E10/549 , Y02E60/13 , Y02P70/521
摘要： Disclosed are compositions formed by a method for exchanging solvent in a mixture that includes water and an optionally substituted thiophene. Also disclosed are methods for making and using such compositions.

5. 发明授权

US5296296A Ordered polymer/sol-gel microcomposite laminates with glass adhesive 失效
标题翻译：带有玻璃粘合剂的有序聚合物/溶胶 - 凝胶微复合层压板
公开(公告)号：US5296296A
公开(公告)日：1994-03-22
申请号：US722583
申请日：1991-06-25
申请人： R. Ross Haghighat , Robert F. Koyar
发明人： R. Ross Haghighat , Robert F. Koyar
IPC分类号： B32B17/06
CPC分类号： B32B17/06 , Y10T428/31616 , Y10T428/31623 , Y10T428/31627 , Y10T428/3163
摘要： Provided is a method for laminating PBZT/fusible sol-gel glass microcomposite film layers by applying an adhesive of fusible sol-gel glass to the bonding surfaces of such films and compressing the film layers and the so-formed adhesive layer therebetween, at sufficient temperature and pressure to laminate the film and adhesive layers together. The sol-gel glass infiltrant and adhesive may be of the same or different materials. Desirably, the bonding surfaces of such films are roughened before application of the adhesive layer therebetween. The invention also includes the laminates prepared by the above method which laminates exhibit good coherent bonding between layers, high tensile strength and good interlaminar strength between layers for fabrication into durable high-strength space-age structures.
摘要翻译：提供了一种通过将可熔溶胶 - 凝胶玻璃的粘合剂施加到这样的膜的粘合表面上来压制PBZT /可熔溶胶 - 凝胶玻璃微复合膜层的方法，并以足够的温度压缩膜层和如此形成的粘合剂层以及将膜和粘合剂层层压在一起的压力。溶胶 - 凝胶玻璃渗透剂和粘合剂可以是相同或不同的材料。理想地，这些膜的粘合表面在其之间施加粘合剂层之前被粗糙化。本发明还包括通过上述方法制备的层压板，层压板在层之间表现出良好的相干粘合，高拉伸强度和层之间的良好的层间强度，以制造成耐用的高强度空间时代结构。

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