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1. 发明授权

US09334345B2 Polymerizable compositions containing (meth)acrylate monomers having sulfide linkages 有权
标题翻译：含有具有硫键的（甲基）丙烯酸酯单体的可聚合组合物
公开(公告)号：US09334345B2
公开(公告)日：2016-05-10
申请号：US13605100
申请日：2012-09-06
申请人： Robert D. Herold , Nina V. Bojkova , Marvin J. Graham , Charles R. Hickenboth , Gregory J. McCollum , William H. Retsch, Jr. , Hongying Zhou
发明人： Robert D. Herold , Nina V. Bojkova , Marvin J. Graham , Charles R. Hickenboth , Gregory J. McCollum , William H. Retsch, Jr. , Hongying Zhou
IPC分类号： C08F220/38 , C08F128/04 , C07C323/12 , C08F36/20 , C09K3/00 , C08F222/10 , G02B1/04
CPC分类号： C08F128/04 , C07C323/12 , C08F36/20 , C08F220/38 , C08F222/1006 , C08F2220/382 , C09K3/00 , G02B1/04 , C08L33/14
摘要： Provided is a polymerizable composition including (meth)acrylate monomers having at least two sulfide (—S—) linkages in the monomer. The polymerizable compositions include a first (meth)acrylate monomer represented by the following Formula (I), where L1 is selected from a multivalent optionally substituted hydrocarbyl group optionally interrupted with at least one of —C(O)—, —S—, —O— and combinations thereof, and a divalent linking group represented by the following Formula (A). In Formula (A), Y is O or S. Also in Formula (I), L2 is independently for each n a divalent optionally substituted hydrocarbyl group optionally interrupted with at least one of —O— and —S—, R1 is independently selected for each n from hydrogen and methyl, and n is from 2 to 6. The polymerizable compositions also may include a polymerization moderator. Also provided are polymerizates including photochromic articles and optical elements prepared from such polymerizable compositions.
摘要翻译：提供了包含在单体中具有至少两个硫（-S-）键的（甲基）丙烯酸酯单体的聚合性组合物。可聚合组合物包括由下式（I）表示的第一（甲基）丙烯酸酯单体，其中L 1选自任选被-C（O） - ， - S - ， - O-及其组合，以及由下式（A）表示的二价连接基团。在式（A）中，Y是O或S.另外在式（I）中，对于任选被-O-和-S-中的至少一个任意中断的每个任意二价的任选取代的烃基，L2独立地选自：每个n为氢和甲基，n为2-6。可聚合组合物还可包括聚合调节剂。还提供了包括光致变色制品和由这些可聚合组合物制备的光学元件的聚合物。

2. 发明申请

US20130082220A1 POLYMERIZABLE COMPOSITIONS CONTAINING (METH)ACRYLATE MONOMERS HAVING SULFIDE LINKAGES 有权
标题翻译：含有（甲基）丙烯酸酯单体的可聚合组合物具有硫酸盐链接
公开(公告)号：US20130082220A1
公开(公告)日：2013-04-04
申请号：US13605100
申请日：2012-09-06
申请人： Robert D. Herold , Nina V. Bojkova , Marvin J. Graham , Charles R. Hickenboth , Gregory J. McCollum , William H. Retsch, JR. , Hongying Zhou
发明人： Robert D. Herold , Nina V. Bojkova , Marvin J. Graham , Charles R. Hickenboth , Gregory J. McCollum , William H. Retsch, JR. , Hongying Zhou
IPC分类号： C08F36/20 , C07C323/12 , C09K3/00
CPC分类号： C08F128/04 , C07C323/12 , C08F36/20 , C08F220/38 , C08F222/1006 , C08F2220/382 , C09K3/00 , G02B1/04 , C08L33/14
摘要： Provided is a polymerizable composition including (meth)acrylate monomers having at least two sulfide (—S—) linkages in the monomer. The polymerizable compositions include a first (meth)acrylate monomer represented by the following Formula (I), where L1 is selected from a multivalent optionally substituted hydrocarbyl group optionally interrupted with at least one of —C(O)—, —S—, —O— and combinations thereof, and a divalent linking group represented by the following Formula (A). In Formula (A), Y is O or S. Also in Formula (I), L2 is independently for each n a divalent optionally substituted hydrocarbyl group optionally interrupted with at least one of —O— and —S—, R1 is independently selected for each n from hydrogen and methyl, and n is from 2 to 6. The polymerizable compositions also may include a polymerization moderator. Also provided are polymerizates including photochromic articles and optical elements prepared from such polymerizable compositions.
摘要翻译：提供了包含在单体中具有至少两个硫（-S-）键的（甲基）丙烯酸酯单体的聚合性组合物。可聚合组合物包括由下式（I）表示的第一（甲基）丙烯酸酯单体，其中L 1选自任选被-C（O） - ， - S - ， - O-及其组合，以及由下式（A）表示的二价连接基团。在式（A）中，Y是O或S.另外在式（I）中，对于任选被-O-和-S-中的至少一个任意中断的每个任意二价的任选取代的烃基，L2独立地选自：每个n为氢和甲基，n为2-6。可聚合组合物还可包括聚合调节剂。还提供了包括光致变色制品和由这些可聚合组合物制备的光学元件的聚合物。

3. 发明申请

US20130225777A1 POLYMERIZABLE COMPOSITIONS CONTAINING ETHYLENICALLY UNSATURATED MONOMERS HAVING EPISULFIDE FUNCTIONAL GROUPS AND RELATED METHODS 有权
标题翻译：含有乙酰辅酶官能团的乙烯单元的聚合物组合物及相关方法
公开(公告)号：US20130225777A1
公开(公告)日：2013-08-29
申请号：US13864785
申请日：2013-04-17
申请人： Charles R. Hickenboth , Federico Menta , Nina V. Bojkova
发明人： Charles R. Hickenboth , Federico Menta , Nina V. Bojkova
IPC分类号： C08G75/00
CPC分类号： C08G75/00 , C08F220/38 , C08F222/1006 , G02B1/04 , C08L33/14 , C08L81/02
摘要： Provided is a polymerizable composition of (a) a monomer composition including ethylenically unsaturated monomer having a β-epithiopropyl functional group; (b) optionally, a compound having two or more β-epithiopropyl functional groups but no polymerizable ethylenically unsaturated groups; (c) an isourea functional polymerization initiator; and (d) a catalyst for reaction between the β-epithiopropyl functional groups. Also provided is a method of reducing the yellowness index of a sulfur-containing polymerizate prepared by addition polymerization, the method including reacting in the presence of an isourea functional polymerization initiator and a catalyst for reaction between β-epithiopropyl functional groups, a polymerizable composition of: (a) a monomer composition including ethylenically unsaturated monomer having a β-epithiopropyl functional group; and, optionally, (b) a compound having two or more β-epithiopropyl functional groups but no polymerizable ethylenically unsaturated groups.
摘要翻译：提供（a）包含具有β-环硫丙基官能团的烯属不饱和单体的单体组合物的可聚合组合物; （b）任选的具有两个或更多个β-环硫丙基官能团但不具有可聚合的烯属不饱和基团的化合物; （c）异脲官能聚合引发剂; 和（d）β-环硫丙基官能团之间的反应催化剂。还提供了降低通过加成聚合制备的含硫聚合物的黄度指数的方法，该方法包括在异脲官能聚合引发剂和用于β-环硫丙基官能团之间反应的催化剂存在下反应的方法，：（a）包含具有β-环硫丙基官能团的烯属不饱和单体的单体组合物; 和（b）具有两个或多个β-环硫丙基官能团但不具有可聚合烯属不饱和基团的化合物。

4. 发明授权

US09133362B2 Coating composition having mechanochromic crystals 有权
标题翻译：涂层组合物具有机械色素晶体
公开(公告)号：US09133362B2
公开(公告)日：2015-09-15
申请号：US13549818
申请日：2012-07-16
申请人： Charles R. Hickenboth , Gregory J. McCollum , Elizabeth Furar
发明人： Charles R. Hickenboth , Gregory J. McCollum , Elizabeth Furar
IPC分类号： G01L1/24 , C09D175/04 , B82Y30/00
CPC分类号： C09D175/04 , B82Y30/00 , G01L1/24
摘要： A mechanochromic coating composition is disclosed comprising a binder composition and a crystalline mechanophore. The mechanophore changes color upon application of a mechanical load to the coating composition.
摘要翻译：公开了包含粘合剂组合物和结晶机械载体的机械着色涂料组合物。机械载体在施加机械载荷至涂料组合物时改变颜色。

5. 发明授权

US08148490B2 Method of making a cyclic guanidine from a guanidinium salt and a weak acid and coating compositions containing the same 有权
标题翻译：从胍盐和弱酸制备环状胍的方法以及含有它们的涂料组合物
公开(公告)号：US08148490B2
公开(公告)日：2012-04-03
申请号：US12720996
申请日：2010-03-10
申请人： Gregory J. McCollum , Charles R. Hickenboth , Richard F. Karabin , Thomas C. Moriarity , Steven R. Zawacky
发明人： Gregory J. McCollum , Charles R. Hickenboth , Richard F. Karabin , Thomas C. Moriarity , Steven R. Zawacky
IPC分类号： C08G59/00 , C07D471/00 , C07D293/00
CPC分类号： C08G59/4021 , C07D487/04 , C08G59/686 , C09D163/00
摘要： The present invention is directed to a method for preparing a cyclic guanidine comprising reacting (i) a guanidinium, (ii) a polyamine, and (iii) a weak acid. The present invention is also directed to a coating composition comprising the cyclic guanidine.
摘要翻译：本发明涉及一种制备环状胍的方法，其包括使（ⅰ）胍，（ⅱ）多胺和（ⅲ）弱酸反应。本发明还涉及包含环状胍的涂料组合物。

6. 发明申请

US20110224403A1 METHOD OF MAKING A CYCLIC GUANIDINE FROM DICYANDIAMIDE AND COATING COMPOSITIONS CONTAINING SAME 有权
标题翻译：制备来自二酰亚胺的环状官能团和含有它的涂料组合物的方法
公开(公告)号：US20110224403A1
公开(公告)日：2011-09-15
申请号：US12720971
申请日：2010-03-10
申请人： Steven R. Zawacky , Charles R. Hickenboth , Richard F. Karabin , Gregory J. McCollum , Thomas C. Moriarity
发明人： Steven R. Zawacky , Charles R. Hickenboth , Richard F. Karabin , Gregory J. McCollum , Thomas C. Moriarity
IPC分类号： C08G59/00 , C07D471/04
CPC分类号： C07D471/04 , C07D487/04 , C08G59/4021 , C08G59/50 , C09D5/4461 , C09D5/4488
摘要： The present invention is directed to a method for preparing a cyclic guanidine comprising reacting (i) a cyanamide, (ii) a polyamine, and (iii) a weak acid. The present invention is also directed to a coating composition comprising the cyclic guanidine.
摘要翻译：本发明涉及一种制备环状胍的方法，包括使（ⅰ）氰胺，（ⅱ）多胺和（ⅲ）弱酸反应。本发明还涉及包含环状胍的涂料组合物。

7. 发明授权

US08334380B2 Method for producing bicyclic guanidines by use of a cyclic urea and a dehydrating agent 失效
标题翻译：通过使用环状脲和脱水剂生产双环胍的方法
公开(公告)号：US08334380B2
公开(公告)日：2012-12-18
申请号：US12195751
申请日：2008-08-21
申请人： Donald W. Boyd , Venkatachalam Eswarakrishnan , Charles R. Hickenboth , Richard F. Karabin , Gregory J. McCollum , Britt A. Minch , Thomas C. Moriarity , Steven R. Zawacky
发明人： Donald W. Boyd , Venkatachalam Eswarakrishnan , Charles R. Hickenboth , Richard F. Karabin , Gregory J. McCollum , Britt A. Minch , Thomas C. Moriarity , Steven R. Zawacky
IPC分类号： C07D471/04
CPC分类号： C07D487/04
摘要： The present invention is directed to a method for producing bicyclic guanidines comprising heating a reaction mixture comprising cyclic urea and a dehydrating agent to a temperature ≧90° C.
摘要翻译：本发明涉及一种制备双环胍的方法，包括将包含环脲和脱水剂的反应混合物加热至温度≥90℃。

8. 发明申请

US20110224328A1 METHOD OF MAKING A CYCLIC GUANIDINE FROM A GUANIDINIUM SALT AND A WEAK ACID AND COATING COMPOSITIONS CONTAINING THE SAME 有权
标题翻译：从盐酸盐制备环状官能团的方法和含有它的弱酸和涂料组合物
公开(公告)号：US20110224328A1
公开(公告)日：2011-09-15
申请号：US12720996
申请日：2010-03-10
申请人： Gregory J. McCollum , Charles R. Hickenboth , Richard F. Karabin , Thomas C. Moriarity , Steven R. Zawacky
发明人： Gregory J. McCollum , Charles R. Hickenboth , Richard F. Karabin , Thomas C. Moriarity , Steven R. Zawacky
IPC分类号： C09D163/00 , C07D487/04 , C08G59/00
CPC分类号： C08G59/4021 , C07D487/04 , C08G59/686 , C09D163/00
摘要： The present invention is directed to a method for preparing a cyclic guanidine comprising reacting (i) a guanidinium, (ii) a polyamine, and (iii) a weak acid. The present invention is also directed to a coating composition comprising the cyclic guanidine.
摘要翻译：本发明涉及一种制备环状胍的方法，其包括使（ⅰ）胍，（ⅱ）多胺和（ⅲ）弱酸反应。本发明还涉及包含环状胍的涂料组合物。

9. 发明申请

US20090286978A1 METHOD FOR PRODUCING BICYCLIC GUANIDINES BY USE OF A CYCLIC THIOUREA 有权
标题翻译：通过使用循环硫酸生产双相性胍类的方法
公开(公告)号：US20090286978A1
公开(公告)日：2009-11-19
申请号：US12120725
申请日：2008-05-15
申请人： Britt A. Minch , Charles R. Hickenboth , Richard F. Karabin , Steven R. Zawacky , Thomas R. Hockswender , Gregory J. McCollum
发明人： Britt A. Minch , Charles R. Hickenboth , Richard F. Karabin , Steven R. Zawacky , Thomas R. Hockswender , Gregory J. McCollum
IPC分类号： C07D253/08
CPC分类号： C07D487/04
摘要： The present invention is directed to a method producing bicyclic guanidine comprising heating a cyclic thiourea to a temperature ranging from ≧140° C. in a substantially non-hydrocarbon solvent to form the bicyclic guanidine.
摘要翻译：本发明涉及一种产生双环胍的方法，其包括在基本上非烃溶剂中加热环状硫脲至> 140℃的温度以形成双环胍。

10. 发明授权

US08563560B2 Preparation of bicyclic guanidine salts in an aqueous media 有权
标题翻译：在水性介质中制备双环胍盐
公开(公告)号：US08563560B2
公开(公告)日：2013-10-22
申请号：US13035048
申请日：2011-02-25
申请人： Charles R. Hickenboth , Christopher A. Dacko , Steven R. Zawacky , Gregory J. McCollum
发明人： Charles R. Hickenboth , Christopher A. Dacko , Steven R. Zawacky , Gregory J. McCollum
IPC分类号： A01N43/90 , A61K31/519 , C07D487/00
CPC分类号： C07D487/04
摘要： Disclosed herein are bicyclic guanidine salts, useful as cure catalysts for electrodeposited coatings. The bicyclic guanidine salts are formed as the reaction product of reactants comprising (a) a compound having the general formula CXn, wherein X is N, O, or S and wherein n is 2 to 4; (b) an acid; (c) dipropylene triamine; and (d) water, and an associated method for forming a bicyclic guanidine salt from the same reaction ingredients.
摘要翻译：本文公开了双环胍盐，其可用作电沉积涂层的固化催化剂。双环胍盐形成为反应物的反应产物，其包含（a）具有通式CXn的化合物，其中X为N，O或S，且其中n为2至4; （b）酸; （c）二丙烯三胺; 和（d）水，以及由相同的反应成分形成双环胍盐的相关方法。

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