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1. 发明授权

US5688626A Gamut toner aggregation processes 失效
标题翻译：色域调色剂聚集过程
公开(公告)号：US5688626A
公开(公告)日：1997-11-18
申请号：US628062
申请日：1996-04-08
申请人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Richard P. N. Veregin , Maria N. V. McDougall
发明人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Richard P. N. Veregin , Maria N. V. McDougall
IPC分类号： G03G9/08 , G03G9/097 , G03G9/09
CPC分类号： G03G9/09733 , G03G9/0804 , G03G9/0815
摘要： A process for the preparation of a combination of color toners comprised of a cyan toner, a magenta toner, a yellow toner, and a black toner, each of said toners being comprised of resin and pigment, and wherein the pigment is cyan, magenta, yellow and black, each of the said pigments are dispersed in a nonionic, or neutral charge surfactant, and wherein each toner in the combination is prepared by (i) preparing a pigment dispersion, which dispersion is comprised of a pigment and nonionic water soluble surfactant; (ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant; (iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates; and (iv) heating said bound toner size aggregates above about the Tg of the resin.
摘要翻译：一种用于制备由青色调色剂，品红色调色剂，黄色调色剂和黑色调色剂组成的彩色调色剂的组合的方法，每种所述调色剂由树脂和颜料组成，并且其中所述颜料是青色，品红色，黄色和黑色，每种所述颜料分散在非离子或中性电荷表面活性剂中，并且其中组合中的每种调色剂通过以下制备：（i）制备颜料分散体，该分散体由颜料和非离子水溶性表面活性剂 ; （ii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂的胶乳或乳液共混物剪切所述颜料分散体; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg）以形成静电结合的调色剂尺寸聚集体; 和（iv）将所述结合的调色剂尺寸聚集体加热到高于树脂的Tg的高度。

2. 发明授权

US5650256A Toner processes 失效
标题翻译：墨粉处理
公开(公告)号：US5650256A
公开(公告)日：1997-07-22
申请号：US720646
申请日：1996-10-02
申请人： Richard P. N. Veregin , Maria N. V. McDougall , Francisco E. Torres , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , T. Hwee Ng , Arthur Helbrecht
发明人： Richard P. N. Veregin , Maria N. V. McDougall , Francisco E. Torres , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , T. Hwee Ng , Arthur Helbrecht
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/0815
摘要： A process for the preparation of toner comprising:(i) preparing a pigment dispersion, which dispersion is comprised of a pigment, and an ionic surfactant;(ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant, and wherein said resin contains an acid functionality;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates;(iv) adding anionic surfactant to stabilize the aggregates obtained in (iii);(v) coalescing said aggregates by heating said bound aggregates above about the Tg of the resin;(vi) reacting said resin of (v) with acid functionality with a base to form an acrylic acid salt, and which salt is ion exchanged in water with a base or a salt, optionally in the presence of metal oxide particles, to control the toner triboelectrical charge, which toner is comprised of resin and pigment; and(vii) optionally drying the toner obtained.
摘要翻译：一种制备调色剂的方法，包括：（i）制备颜料分散体，该分散体由颜料和离子表面活性剂组成; （ii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂组成的胶乳或乳液共混物剪切所述颜料分散体，并且其中所述树脂含有酸官能团; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg）以形成静电结合的调色剂尺寸聚集体; （iv）加入阴离子表面活性剂以稳定（iii）中获得的聚集体; （v）通过将所述结合的聚集体加热到约树脂的Tg附近来聚结所述聚集体; （vi）将所述（ⅴ）的酸性官能团的树脂与碱反应形成丙烯酸盐，并且任选地在金属氧化物颗粒存在下，盐与碱或盐在水中进行离子交换，以控制调色剂摩擦电荷，调色剂由树脂和颜料组成; 和（vii）任选地干燥获得的调色剂。

3. 发明授权

US06780559B2 Toner processes 失效
公开(公告)号：US06780559B2
公开(公告)日：2004-08-24
申请号：US10215148
申请日：2002-08-07
申请人： Richard P. N. Veregin , Raj D. Patel , Maria N. V. McDougall
发明人： Richard P. N. Veregin , Raj D. Patel , Maria N. V. McDougall
IPC分类号： G03G908
CPC分类号： G03G9/0804 , C08J3/215 , G03G9/09
摘要： A toner process involving mixing a colorant dispersion and a metal oxide with a latex emulsion comprised of polymer, water, and an anionic surfactant, adding a cationic coagulant followed by heating the mixture to a temperature below about the glass transition temperature (Tg) of the latex polymer particles to provide toner size aggregates comprised of polymer pigment and dye, heating above about the Tg of the polymer and isolating the resulting product.

4. 发明授权

US07645552B2 Toner compositions 有权
标题翻译：调色剂组合物
公开(公告)号：US07645552B2
公开(公告)日：2010-01-12
申请号：US11003581
申请日：2004-12-03
申请人： Raj D. Patel , Daryl Vanbesien , Enno E. Agur , Edward G. Zwartz , Maria N. V. McDougall , Emily L. Moore , Patricia A. Burns , Kimberly D. Nosella , Ke Zhou , Vladislav Skorokhod , Wafa F. Bashir , Shigang (Steven) Qiu
发明人： Raj D. Patel , Daryl Vanbesien , Enno E. Agur , Edward G. Zwartz , Maria N. V. McDougall , Emily L. Moore , Patricia A. Burns , Kimberly D. Nosella , Ke Zhou , Vladislav Skorokhod , Wafa F. Bashir , Shigang (Steven) Qiu
IPC分类号： G03G9/087
CPC分类号： G03G9/08797 , G03G9/0804 , G03G9/08711 , G03G9/08791 , G03G9/08793 , G03G9/08795
摘要： Toner compositions include a non cross linked resin; a cross linked resin or gel; a wax; and a colorant. Processes for preparing a toner include mixing a non-cross linked resin and a cross-linked resin or gel in the presence of a wax, a colorant, and a coagulant to provide toner size aggregates; adding additional non-cross linked latex to the formed aggregates thereby providing a shell over the formed aggregates; heating the shell covered aggregates to form toner; and, optionally, isolating the toner.
摘要翻译：调色剂组合物包括非交联树脂; 交联树脂或凝胶; 蜡和着色剂。制备调色剂的方法包括在蜡，着色剂和凝结剂的存在下混合非交联树脂和交联树脂或凝胶以提供调色剂尺寸聚集体; 向所形成的聚集体中加入另外的非交联胶乳，从而在所形成的聚集体上提供壳; 加热外壳覆盖的聚集体以形成调色剂; 和可选地分离调色剂。

5. 发明授权

US06808851B2 Emulsion aggregation toner containing a mixture of waxes incorporating an improved process to prevent wax protrusions and coarse particles 有权
标题翻译：含有蜡的混合物的乳液聚集调色剂包括改进的方法以防止蜡突起和粗颗粒
公开(公告)号：US06808851B2
公开(公告)日：2004-10-26
申请号：US10248393
申请日：2003-01-15
申请人： Joseph A. Bartel , Patricia A. Burns , Raj D. Patel , Enno E. Agur , Danielle C. Boils , Edward G. Zwartz , Paul J. Gerroir , Maria N. V. McDougall
发明人： Joseph A. Bartel , Patricia A. Burns , Raj D. Patel , Enno E. Agur , Danielle C. Boils , Edward G. Zwartz , Paul J. Gerroir , Maria N. V. McDougall
IPC分类号： G03G9083
CPC分类号： G03G9/0804 , C08J3/215 , G03G9/0815
摘要： A process for the preparation of emulsion aggregation toner particles with high pigment loading having a reduced number of wax protrusions on the surface of the toner particles and fewer coarse toner particles. The process includes the introduction of a wax having a molecular weight between about 500 and 2,500, or a blend of waxes having different a molecular weight between 500 and 2,500.
摘要翻译：一种制备具有高颜料负载的乳液聚集调色剂颗粒的方法，其中调色剂颗粒表面上的蜡突起数量减少，较少的粗调色剂颗粒。该方法包括引入分子量为约500-2,500的蜡，或分子量不同于500至2500之间的蜡的共混物。

6. 发明授权

US5650252A Toner grafting processes 失效
标题翻译：调色剂接枝工艺
公开(公告)号：US5650252A
公开(公告)日：1997-07-22
申请号：US669118
申请日：1996-06-24
申请人： T. Hwee Ng , Arthur Helbrecht , Raj D. Patel , Michael A. Hopper , Richard P. N. Veregin
发明人： T. Hwee Ng , Arthur Helbrecht , Raj D. Patel , Michael A. Hopper , Richard P. N. Veregin
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/0806 , G03G9/0815
摘要： A process for the preparation of toner comprising:(i) preparing a pigment dispersion, which dispersion is comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(iv) heating said bound aggregates above about the Tg of the resin; and(v) thereafter washing the toner obtained, adding initiator, adding monomer, polymerizing by heating, and thereafter cooling, followed by an optional second washing.
摘要翻译：一种制备调色剂的方法，包括：（i）制备颜料分散体，该分散体由颜料，离子表面活性剂和任选的电荷控制剂组成; （ii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂的胶乳或乳液共混物剪切所述颜料分散体; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （iv）将所述结合的聚集体加热到树脂的Tg附近; 和（v）然后洗涤所获得的调色剂，加入引发剂，加入单体，通过加热进行聚合，然后冷却，然后进行任选的第二次洗涤。

7. 发明授权

US5744520A Aggregation processes 失效
标题翻译：汇总流程
公开(公告)号：US5744520A
公开(公告)日：1998-04-28
申请号：US684955
申请日：1996-07-19
申请人： Grazyna E. Kmiecik-Lawrynowicz , Richard P. N. Veregin , Raj D. Patel , Michael A. Hopper , Maria V. McDougall
发明人： Grazyna E. Kmiecik-Lawrynowicz , Richard P. N. Veregin , Raj D. Patel , Michael A. Hopper , Maria V. McDougall
IPC分类号： C08J3/215 , G03G9/113 , C08K9/08 , C08K3/22 , C08K5/41 , C08L1/26
CPC分类号： C08J3/215 , G03G9/1131 , G03G9/1133 , G03G9/1138 , G03G9/1139
摘要： A process for the preparation of polymer compositions which comprises mixing a conductive component with an anionic polymeric latex containing a polymer; adding a cationic surfactant, or flocculant whereby the aggregation of the latex particles and the conductive component particles results; subsequently adding colloidal stabilizer, followed by the addition of a base to obtain a pH of from about 7 to about 12; heating above about the polymer glass transition temperature thereby enabling the severage, or breakage of the formed aggregated particles; further heating above about the polymer glass transition temperature enabling the coalescence of the polymer and conductive component particles; and optionally washing and drying the resulting coalesced product.
摘要翻译：一种制备聚合物组合物的方法，其包括将导电组分与含有聚合物的阴离子聚合物胶乳混合; 加入阳离子表面活性剂或絮凝剂，由此导致胶乳颗粒和导电组分颗粒的聚集; 随后加入胶体稳定剂，然后加入碱以获得约7至约12的pH; 加热高于聚合物玻璃化转变温度，从而能够形成聚集的颗粒的覆盖或破裂; 进一步加热高于聚合物玻璃化转变温度，使聚合物和导电组分颗粒聚结; 并任选地洗涤和干燥所得的聚结产物。

8. 发明授权

US5869216A Toner processes 失效
标题翻译：墨粉处理
公开(公告)号：US5869216A
公开(公告)日：1999-02-09
申请号：US6742
申请日：1998-01-13
申请人： Beng S. Ong , Walter Mychajlowskij , Raj D. Patel , Patricia A. Burns , Richard P. N. Veregin
发明人： Beng S. Ong , Walter Mychajlowskij , Raj D. Patel , Patricia A. Burns , Richard P. N. Veregin
IPC分类号： G03G9/087 , G03G9/08 , G03G9/097
CPC分类号： G03G9/0804 , G03G9/09733 , Y10S977/89
摘要： A process for the preparation of toner comprising blending an aqueous colorant dispersion and a latex emulsion containing resin; heating the resulting mixture at a temperature below about the glass transition temperature (Tg) of the latex resin to form toner sized aggregates; heating said resulting aggregates at a temperature above about the Tg of the latex resin to effect fusion or coalescence of the aggregates; redispersing said toner in water at a pH of above about 7; contacting the resulting mixture with a metal halide or salt, and then with a mixture of an alkaline base and a salicylic acid, a catechol, or mixtures thereof at a temperature of from about 25.degree. C. to about 80.degree. C.; and optionally isolating the toner product, washing, and drying.
摘要翻译：一种制备调色剂的方法，包括混合含水着色剂分散体和含树脂的胶乳乳液; 在低于胶乳树脂的玻璃化转变温度（Tg）的温度下加热所得混合物以形成调色剂尺寸的聚集体; 在高于约胶乳树脂的Tg的温度下加热所述聚集体，以实现聚集体的熔融或聚结; 将所述调色剂在pH高于约7的水中再分散; 在约25℃至约80℃的温度下将所得混合物与金属卤化物或盐接触，然后与碱性碱和水杨酸，儿茶酚或其混合物的混合物接触。并任选地分离调色剂产物，洗涤和干燥。

9. 发明授权

US06132924A Toner coagulant processes 有权
标题翻译：调色剂凝结剂工艺
公开(公告)号：US06132924A
公开(公告)日：2000-10-17
申请号：US173405
申请日：1998-10-15
申请人： Raj D. Patel , Michael A. Hopper , Richard P. N. Veregin
发明人： Raj D. Patel , Michael A. Hopper , Richard P. N. Veregin
IPC分类号： G03G9/087 , B82B1/00 , G03G9/08 , G03G9/09 , G03G9/097 , G03Q9/08
CPC分类号： G03G9/09708 , G03G9/0804
摘要： A process for the preparation of toner comprising mixing a colorant, a latex, and two coagulants, followed by aggregation and coalescence.
摘要翻译：调色剂的制备方法，包括混合着色剂，胶乳和两种凝结剂，然后聚集和聚结。

10. 发明授权

US5565296A Coated carriers by aggregation processes 失效
标题翻译：通过聚合过程的涂层载体
公开(公告)号：US5565296A
公开(公告)日：1996-10-15
申请号：US497737
申请日：1995-07-03
申请人： Grazyna E. Kmiecik-Lawrynowicz , Richard P. N. Veregin , Raj D. Patel , Michael A. Hopper , Maria V. McDougall
发明人： Grazyna E. Kmiecik-Lawrynowicz , Richard P. N. Veregin , Raj D. Patel , Michael A. Hopper , Maria V. McDougall
IPC分类号： C08J3/215 , G03G9/113
CPC分类号： C08J3/215 , G03G9/1131 , G03G9/1133 , G03G9/1138 , G03G9/1139
摘要： A process for the preparation of polymer compositions which comprises mixing a conductive component with an anionic polymeric latex containing a polymer; adding a cationic surfactant, or flocculant whereby the aggregation of the latex particles and the conductive component particles results; subsequently adding colloidal stabilizer, followed by the addition of a base to obtain a pH of from about 7 to about 12; heating above about the polymer glass transition temperature thereby enabling the severage, or breakage of the formed aggregated particles; further heating above about the polymer glass transition temperature enabling the coalescence of the polymer and conductive component particles; and optionally washing and drying the resulting coalesced product.
摘要翻译：一种制备聚合物组合物的方法，其包括将导电组分与含有聚合物的阴离子聚合物胶乳混合; 加入阳离子表面活性剂或絮凝剂，由此导致胶乳颗粒和导电组分颗粒的聚集; 随后加入胶体稳定剂，然后加入碱以获得约7至约12的pH; 加热高于聚合物玻璃化转变温度，从而能够形成聚集的颗粒的覆盖或破裂; 进一步加热高于聚合物玻璃化转变温度，使聚合物和导电组分颗粒聚结; 并任选地洗涤和干燥所得的聚结产物。

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