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1. 发明授权

US5470497A Refrigeration working fluid compositions containing trifluoroethane and neopentyl glycol or trimethylolpropane esters of C.sub.7 and C.sub.9 acids 失效
标题翻译：含有C 3和C 9酸的三氟乙烷和新戊二醇或三羟甲基丙烷酯的制冷工作流体组合物
公开(公告)号：US5470497A
公开(公告)日：1995-11-28
申请号：US365187
申请日：1994-12-28
申请人： Richard H. Schlosberg , Carolyn B. Duncan , Martin A. Krevalis, Jr.
发明人： Richard H. Schlosberg , Carolyn B. Duncan , Martin A. Krevalis, Jr.
IPC分类号： C09K5/04 , C10M105/38 , C10M171/00 , C10N20/00 , C10N30/00 , C10N40/30
CPC分类号： C09K5/045 , C10M105/38 , C10M171/008 , C09K2205/24 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2211/022 , C10M2211/06 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： There are disclosed refrigeration working fluid compositions comprising 1,1,1-trifluoroethane refrigerant and either a neopentylglycol ester of 3,5,5-trimethylhexanoic acid or a trimethylolpropane ester of a mixture of 65 wt. % 3,5,5-trimethylhexanoic acid, 22.2 wt. % n-heptanoic acid and 12.8 wt. % methylhexanoic acid. The esters exhibit suitable viscosity ranges and miscibility with the refrigerant over a broad compositional range.
摘要翻译：公开了包含1,1,1-三氟乙烷制冷剂和3,5,5-三甲基己酸的新戊二醇酯或65重量％混合物的混合物的三羟甲基丙烷酯的制冷工作流体组合物。％3,5,5-三甲基己酸，22.2重量％％正庚酸和12.8重量％％甲基己酸。该酯在宽的组成范围内表现出合适的粘度范围和与制冷剂的混溶性。

2. 发明授权

US5494597A Refrigeration working fluid compositions containing difluoroethane or pentafluoroethane and a polyolester lubricant 失效
标题翻译：含有二氟乙烷或五氟乙烷和多元醇酯润滑剂的制冷工作流体组合物
公开(公告)号：US5494597A
公开(公告)日：1996-02-27
申请号：US298515
申请日：1994-08-30
申请人： Martin A. Krevalis, Jr. , Richard H. Schlosberg , Carolyn B. Duncan
发明人： Martin A. Krevalis, Jr. , Richard H. Schlosberg , Carolyn B. Duncan
IPC分类号： C09K5/04 , C10M105/38 , C10M171/00 , C10N20/02 , C10N30/00 , C10N40/30 , C10M105/34
CPC分类号： C10M171/008 , C09K5/045 , C10M105/38 , C09K2205/22 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2211/022 , C10M2211/06 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： There are disclosed refrigeration working fluid compositions comprising R125 (pentafluoroethane) or R152a (1,1-difluoroethane) refrigerants and certain polyol esters of C.sub.7 to C.sub.10 branched alkanoic acids or mixtures of such branched acids with linear C.sub.7 to C.sub.10 monoalkanoic acids. The polyols are neopentylglycol, technical grade pentaerythritol and trimethylolpropane; the esters exhibit suitable viscosity ranges and miscibility with refrigerants over a broad compositional range. The acids have a defined average effective carbon chain length in order to be miscible with the refrigerants over the range of 5 to 55 wt. % ester lubricant.
摘要翻译：公开了包含R125（五氟乙烷）或R152a（1,1-二氟乙烷）制冷剂和C7至C10支链烷酸的某些多元醇酯或这些支链酸与线性C 7至C 10单链烷酸的混合物的制冷工作流体组合物。多元醇是新戊二醇，工业级季戊四醇和三羟甲基丙烷; 该酯在宽的组成范围内表现出合适的粘度范围和与制冷剂的混溶性。这些酸具有确定的平均有效碳链长度，以便与5至55重量％范围内的制冷剂混溶。％酯润滑剂。

3. 发明授权

US07456319B2 Para-alkylation of aromatic primary amines 失效
标题翻译：芳族伯胺的对烷基化
公开(公告)号：US07456319B2
公开(公告)日：2008-11-25
申请号：US11296997
申请日：2005-12-08
申请人： George A Knudsen , Richard H. Schlosberg
发明人： George A Knudsen , Richard H. Schlosberg
IPC分类号： C07C209/68
CPC分类号： C07C209/68 , C07C211/45
摘要： A method is provided for producing primarily para alkyl aromatic amines by alkylating a primary aromatic amine with an olefin in the presence of an acid activated clay.
摘要翻译：提供了一种通过在酸活化粘土存在下用烯烃烷基化伯芳族胺来主要制备对位烷基芳族胺的方法。

4. 发明授权

US07005537B2 Production of esters 有权
标题翻译：生产酯
公开(公告)号：US07005537B2
公开(公告)日：2006-02-28
申请号：US09750567
申请日：2000-12-26
申请人： Edmund J. Mozeleski , Carl R. Beck , Kirk C. Nadler , Richard H. Schlosberg
发明人： Edmund J. Mozeleski , Carl R. Beck , Kirk C. Nadler , Richard H. Schlosberg
IPC分类号： C07C67/36 , C07C67/38 , C07C67/24
CPC分类号： C07C67/38 , C07C67/37 , C07C69/24
摘要： Disclosed is a process for the production of esters. In particular, the process includes contacting an olefin or an ether with carbon monoxide and an acid composition comprising BF3.2CH3OH to from a product composition, adding an alcohol to the product composition, and separating the BF3.2CH3OH from the ester. The separated BF3.2CH3OH may then be recycled to the reaction unit.
摘要翻译：公开了一种生产酯的方法。特别地，该方法包括使烯烃或醚与一氧化碳和包含BF 3/2CH 3 OH的酸组合物从产物组合物接触，向醇中加入醇产物组合物，并从该酯中分离出BF 3/3CH 3 OH。然后将分离的BF 3/2CH 3 OH再循环到反应单元中。

5. 发明授权

US06994799B2 Ester-containing fluid compositions 失效
公开(公告)号：US06994799B2
公开(公告)日：2006-02-07
申请号：US09747146
申请日：2000-12-22
申请人： Eddy Van Driessche , Georges Mathys , Richard H. Schlosberg , Christian Francois , Chris De Roover
发明人： Eddy Van Driessche , Georges Mathys , Richard H. Schlosberg , Christian Francois , Chris De Roover
IPC分类号： C09K5/00
CPC分类号： C09D11/033 , C07C69/24 , C09D7/20 , C10M105/34 , C10M2207/2815 , C10N2270/00
摘要： Disclosed are ester-containing fluid compositions, methods of making such compositions, and methods of using such compositions. The fluid compositions comprise a mix of branched and linear ester compounds, and the fluid compositions are characterized by certain performance limitations. The preferred method of making the fluid compositions enables the ester mix to be made in a one step process with little finishing required to obtain desirable performance characteristics.

7. 发明授权

US5453561A Reactive separation process 失效
标题翻译：反应分离过程
公开(公告)号：US5453561A
公开(公告)日：1995-09-26
申请号：US187673
申请日：1994-01-27
申请人： Ramzi Y. Saleh , Michael Siskin , Glen B. Brons , Stephen N. Vaughn , Richard H. Schlosberg
发明人： Ramzi Y. Saleh , Michael Siskin , Glen B. Brons , Stephen N. Vaughn , Richard H. Schlosberg
IPC分类号： B01D17/025 , C07C7/148 , C07C11/02 , C07C29/10 , C10G50/00 , C07C7/00
CPC分类号： C07C29/10 , C07C7/148
摘要： The invention concerns a method for reactive separation of mixtures containing hydrocarbons and oxygenated hydrocarbons, by contacting a mixture of hydrocarbons such as C.sub.2 to C.sub.26 hydrocarbons and mixtures thereof and oxygenated hydrocarbons, such as C.sub.2 to C.sub.40 oxygenated hydrocarbons and mixtures thereof to form a mixture of hydrocarbons and lower molecular weight oxygenated hydrocarbons and heating the mixture in water at temperature typically from about and pressure sufficient to cleave the oxygenated hydrocarbons to lower molecular weight products to form a liquid layer containing water soluble reaction products and an organic layer containing primarily hydrocarbons.
摘要翻译：本发明涉及通过使烃类混合物例如C 2至C 26烃及其混合物和含氧烃如C2至C40含氧烃及其混合物的混合物与烃和氧化烃的混合物进行反应分离的方法，以形成混合物碳氢化合物和较低分子量的氧化烃，并将混合物在水中加热，其温度通常为足以将氧化烃切割成较低分子量产物的温度，形成含有水溶性反应产物和主要含有烃的有机层的液体层。

8. 发明授权

US4385981A Liquefaction of carbonous materials with vapor phase hydrogen donor solvents 失效
标题翻译：碳质材料与气相氢供体溶剂的液化
公开(公告)号：US4385981A
公开(公告)日：1983-05-31
申请号：US255569
申请日：1981-04-20
申请人： Daniel R. Neskora , Richard H. Schlosberg
发明人： Daniel R. Neskora , Richard H. Schlosberg
IPC分类号： C10G1/04 , C10G1/00
CPC分类号： C10G1/042
摘要： Disclosed is a method for enhancing the conversion of carbonous materials, such as coal and oil shale. The method comprises converting the carbonous material in the presence of a vapor phase hydrogen donor material containing 1 or more hydrogen donor solvents wherein each donor material is characterized by: (a) a heterocyclic ring in which the heteroatom is nitrogen, (b) having at least one donatable hydrogen located on the heterocyclic ring, and (c) becoming more unsaturated and/or aromatic upon the loss of the donatable hydrogen(s). The conversion is performed at substantially atmospheric pressure, at an effective vapor residence time and at a temperature from about the boiling point of the hydrogen donor material to about 550.degree. C.
摘要翻译：公开了一种提高碳质材料如煤和油页岩的转化率的方法。该方法包括在含有1个或更多个氢供体溶剂的气相氢供体材料的存在下转化碳质材料，其中每个供体材料的特征在于：（a）其中杂原子是氮的杂环，（b）具有位于杂环上的至少一个可供氢的氢，和（c）在可用氢的丧失时变得更不饱和和/或芳族。转化在基本上大气压下，在有效的蒸气停留时间和约从氢供体材料的沸点至约550℃的温度下进行。

9. 发明授权

US07504527B2 Low corrosive integrated process for preparing dialkyl carbonates 失效
标题翻译：用于制备碳酸二烷基酯的低腐蚀性综合工艺
公开(公告)号：US07504527B2
公开(公告)日：2009-03-17
申请号：US10641596
申请日：2003-08-15
申请人： Richard H. Schlosberg , J. Scott Buchanan , Jose Guadalupe Santiesteban , Zhaozhong Jiang , William A. Weber
发明人： Richard H. Schlosberg , J. Scott Buchanan , Jose Guadalupe Santiesteban , Zhaozhong Jiang , William A. Weber
IPC分类号： C07C69/96
CPC分类号： C07D317/38 , B01J2219/00006 , C07C29/128 , C07C29/1285 , C07C68/065 , C07D317/36 , C08G64/307 , C08G64/34 , Y02P20/125 , Y02P20/127 , Y02P20/584 , C07C69/96 , C07C31/202
摘要： An integrated process for the production of a dialkyl carbonate and a diol from an alkylene oxide, carbon dioxide and an aliphatic monohydric alcohol is described in which an alkylene oxide is first reacted with carbon dioxide in the presence of a halogen-free carbonation catalyst to provide a corresponding cyclic carbonate and the cyclic carbonate is then reacted with an aliphatic monohydric alcohol in the presence of the carbonation catalyst and/or a transesterification catalyst and recycling the carbonation catalyst to provide a corresponding dialkyl carbonate and diol, wherein the dialkyl carbonate product exhibits a halogen concentration of about 5 ppm or less.
摘要翻译：描述了一种用于从烯化氧，二氧化碳和脂族一元醇生产碳酸二烷基酯和二醇的综合方法，其中在无卤素碳酸化催化剂存在下，首先使环氧烷与二氧化碳反应，以提供然后在碳酸化催化剂和/或酯交换催化剂的存在下使相应的环状碳酸酯和环状碳酸酯与脂族一元醇反应，并循环碳酸化催化剂以提供相应的碳酸二烷基酯和二醇，其中碳酸二烷基酯产物显示出卤素浓度为约5ppm以下。

10. 发明授权

US07145029B2 Low corrosive integrated process for preparing dialkyl carbonates 失效
公开(公告)号：US07145029B2
公开(公告)日：2006-12-05
申请号：US10879792
申请日：2004-06-29
申请人： Richard H. Schlosberg , J. Scott Buchanan , Jose Guadalupe Santiesteban , Zhaozhong Jiang , William A. Weber
发明人： Richard H. Schlosberg , J. Scott Buchanan , Jose Guadalupe Santiesteban , Zhaozhong Jiang , William A. Weber
IPC分类号： C07C69/96
CPC分类号： C07D317/38 , B01J2219/00006 , C07C29/128 , C07C29/1285 , C07C68/065 , C07D317/36 , C08G64/307 , C08G64/34 , Y02P20/125 , Y02P20/127 , Y02P20/584 , C07C69/96 , C07C31/202
摘要： An integrated process for the production of a dialkyl carbonate and a diol from an alkylene oxide, carbon dioxide and an aliphatic monohydric alcohol is described in which an alkylene oxide is first reacted with carbon dioxide in the presence of a halogen-free carbonation catalyst to provide a corresponding cyclic carbonate and the cyclic carbonate is then reacted with an aliphatic monohydric alcohol in the presence of the carbonation catalyst and/or a transesterification catalyst and recycling the carbonation catalyst to provide a corresponding dialkyl carbonate and diol, wherein the dialkyl carbonate product exhibits a halogen concentration of about 5 ppm or less.

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