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    • 5. 发明授权
    • Continuous process for the manufacture of cyanuric acid
    • 用于制造氰尿酸的连续工艺
    • US4294962A
    • 1981-10-13
    • US162718
    • 1980-06-25
    • Elizabeth A. BagnallBasil A. GuilianoHenry A. Pfeffer, III
    • Elizabeth A. BagnallBasil A. GuilianoHenry A. Pfeffer, III
    • C07D251/32
    • C07D251/32
    • A highly-pure cyanuric acid is manufactured in a continuous process whereby urea and/or biuret are dissolved in an inert solvent and circulated at a high velocity and a temperature in the range of about 180.degree. C. to about 250.degree. C. through a loop between a heat exchanger and a forced circulation evaporative crystallizer body. Cyanuric acid crystallizes from the reaction mixture as it circulates to form a slurry. Ammonia formed during the reaction is removed at reduced pressure as the reaction mixture enters the evaporative crystallizer body. A portion of the slurry of cyanuric acid is continuously removed as it circulates through the loop and may be filtered to recover the cyanuric acid. The filtrate is returned to a feed tank and additional solvent, urea or biuret added to meet the concentration desired in the reaction mixture. The solution from the feed tank is added to the reaction mixture circulating through the loop at a rate to replace the volume of cyanuric acid slurry that is removed.
    • 以连续的方法制造高纯度的三聚氰酸,由此将脲和/或缩二脲溶解在惰性溶剂中并通过高温和约180℃至约250℃的温度循环 在热交换器和强制循环蒸发结晶器主体之间循环。 当反应混合物循环形成淤浆时,氰尿酸结晶。 当反应混合物进入蒸发结晶器体时,反应期间形成的氨被减压除去。 氰尿酸浆料的一部分在循环通过环路时被连续地除去,并且可以过滤以回收氰尿酸。 将滤液返回到进料罐,并加入另外的溶剂,尿素或缩二脲以满足反应混合物中所需的浓度。 将来自进料罐的溶液加入到通过回路循环的反应混合物中,以取代被除去的氰尿酸浆料的体积。