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1. 发明授权

US06395848B1 Polymerization of fluoromonomers 有权
标题翻译：氟单体的聚合
公开(公告)号：US06395848B1
公开(公告)日：2002-05-28
申请号：US09704333
申请日：2000-11-02
申请人： Richard Alan Morgan , Clay Woodward Jones , Theodore Treat , Jeffrey A. Hrivnak
发明人： Richard Alan Morgan , Clay Woodward Jones , Theodore Treat , Jeffrey A. Hrivnak
IPC分类号： C08F1418
CPC分类号： C08F214/262 , C08F14/26 , Y10S526/91 , Y10S526/911 , C08F2/16
摘要： Aqueous dispersion polymerization of fluoromonomers is improved by using a combination of fluorosurfactants, one of which is a perfluoropolyether carboxylic acid or sulfonic acid or salt of either.
摘要翻译：通过使用含氟表面活性剂的组合来改善氟单体的水分散聚合，其中一种是全氟聚醚羧酸或其磺酸或其盐之一。

2. 发明授权

US06429258B1 Polymerization of fluoromonomers 有权
标题翻译：氟单体的聚合
公开(公告)号：US06429258B1
公开(公告)日：2002-08-06
申请号：US09570853
申请日：2000-05-12
申请人： Richard Alan Morgan , Clay Woodward Jones , Theodore Arthur Treat , Jeffrey A. Hrivnak
发明人： Richard Alan Morgan , Clay Woodward Jones , Theodore Arthur Treat , Jeffrey A. Hrivnak
IPC分类号： C08J216
CPC分类号： C08F214/262 , C08F14/26 , C08F2/16
摘要： Aqueous dispersion polymerization of fluoromonomers is improved by using a combination of fluorosurfactants, one of which is a perfluoropolyether carboxylic acid or salt.
摘要翻译：通过使用其中一种是全氟聚醚羧酸或盐的含氟表面活性剂的组合来改善氟单体的水分散聚合。

3. 发明授权

US07914853B2 Process for forming filled bearings from fluoropolymer dispersions stabilized with anionic polyelectrolyte dispering agents 有权
标题翻译：用阴离子聚电解质分散剂稳定的含氟聚合物分散体形成填充轴承的方法
公开(公告)号：US07914853B2
公开(公告)日：2011-03-29
申请号：US12791911
申请日：2010-06-02
申请人： Robert John Cavanaugh , Clay Woodward Jones
发明人： Robert John Cavanaugh , Clay Woodward Jones
IPC分类号： B05D3/02
CPC分类号： C08L27/18 , C08K3/24 , C08L1/08 , C08L33/02 , C08L33/14 , C08L79/08 , C09D127/18 , C08L2666/26 , C08L2666/04 , C08L2666/20
摘要： The present invention provides a process for making a filled fluoropolymer bearing comprising providing an aqueous fluoropolymer dispersion comprising fluoropolymer particles and anionic polyelectrolyte dispersing agent in an amount sufficient for stabilization. The dispersion contains less than about 300 ppm fluorosurfactant based on the weight of the dispersion. The dispersion is coagulated to make a mush and a bearing filler is added to the dispersion prior to or after making the mush. The mush containing bearing filler is applied onto a bearing substrate to produce a coated substrate which is sintered and formed into a bearing.
摘要翻译：本发明提供了一种制备填充的含氟聚合物轴承的方法，包括提供含氟聚合物颗粒和阴离子聚电解质分散剂的水性含氟聚合物分散体，其量足以使其稳定。基于分散体的重量，分散体含有少于约300ppm的含氟表面活性剂。分散体凝结成糊状物，并且在制备糊料之前或之后将分散体加入到分散体中。将含糊的含轴承填料施加到轴承基材上以制备被烧结并形成轴承的涂覆基材。

4. 发明授权

US07871673B2 Process for forming filled bearings from fluoropolymer dispersions stabilized with anionic polyelectrolyte dispersing agents 有权
公开(公告)号：US07871673B2
公开(公告)日：2011-01-18
申请号：US12791906
申请日：2010-06-02
申请人： Robert John Cavanaugh , Clay Woodward Jones
发明人： Robert John Cavanaugh , Clay Woodward Jones
IPC分类号： B05D3/02
CPC分类号： C08L27/18 , C08K3/24 , C08L1/08 , C08L33/02 , C08L33/14 , C08L79/08 , C09D127/18 , C08L2666/26 , C08L2666/04 , C08L2666/20
摘要： The present invention provides a process for making a filled fluoropolymer bearing comprising providing an aqueous fluoropolymer dispersion comprising fluoropolymer particles and anionic polyelectrolyte dispersing agent in an amount sufficient for stabilization. The dispersion contains less than about 300 ppm fluorosurfactant based on the weight of the dispersion. The dispersion is coagulated to make a mush and a bearing filler is added to the dispersion prior to or after making the mush. The mush containing bearing filler is applied onto a bearing substrate to produce a coated substrate which is sintered and formed into a bearing.

5. 发明申请

US20100113680A1 Aqueous Fluoropolymer Dispersion Stabilized with Amine Oxide Surfactant and Process for Making Coagulated Fluoropolymer Resin 失效
标题翻译：用氧化胺表面活性剂稳定的含氟聚合物分散体和制备凝结的含氟聚合物树脂的方法
公开(公告)号：US20100113680A1
公开(公告)日：2010-05-06
申请号：US12687905
申请日：2010-01-15
申请人： Clay Woodward Jones
发明人： Clay Woodward Jones
IPC分类号： C08F6/22 , C08L27/18
CPC分类号： C08K5/32 , C08L27/12
摘要： An aqueous fluoropolymer dispersion comprising an aqueous medium, fluoropolymer particles, and an amine oxide surfactant. Coagulated fluoropolymer resin is produced from the dispersion by adding an acidic reagent in sufficient amount to cause coagulation and separation of the coagulated fluoropolymer resin from the aqueous medium. Another particulate component such as particular polymer, filler, pigment, solid lubricant, etc., may be added to the dispersion and co-coagulated to form a mixture of coagulated fluoropolymer resin and particulate component.
摘要翻译：一种包含含水介质，含氟聚合物颗粒和氧化胺表面活性剂的含水氟聚合物分散体。通过加入足够量的酸性试剂使分散体从凝胶化的含氟聚合物树脂与水性介质凝结分离，由分散体生成凝聚的含氟聚合物树脂。可以将另外的颗粒组分如特定的聚合物，填料，颜料，固体润滑剂等添加到分散体中并共凝固形成凝固的含氟聚合物树脂和颗粒组分的混合物。

6. 发明授权

US5723556A Fluoromonomer/functionalized hydrocarbon monomer copolymerization process and copolymer product 失效
公开(公告)号：US5723556A
公开(公告)日：1998-03-03
申请号：US763425
申请日：1996-12-11
申请人： Clay Woodward Jones
发明人： Clay Woodward Jones
IPC分类号： C08F2/24 , C08F8/12 , C08F214/18 , C08F214/26 , C08F218/04 , C08F14/18
CPC分类号： C08F214/186 , C08F214/265 , C08F218/04 , C08F8/12 , C08J5/18 , C08F2800/20
摘要： Amorphous copolymer of fluoromonomer, such as tetrafluoroethylene, with vinyl ester, such as vinyl acetate, having a substantially uniform composition is made by aqueous dispersion polymerization by maintaining essentially constant the proportion of the fluoromonomer and vinyl ester copolymerizing with one another. In one embodiment, this proportion consistency is obtained by reducing the agitation rate of the aqueous polymerization medium during the copolymerization reaction at constant fluoromonomer feed pressure within the polymerization reactor.

7. 发明授权

US08097673B2 Aqueous fluoropolymer dispersion stabilized with amine oxide surfactant and process for making coagulated fluoropolymer resin 有权
标题翻译：用氧化胺表面活性剂稳定的含水氟聚合物分散体和制备凝固的含氟聚合物树脂的方法
公开(公告)号：US08097673B2
公开(公告)日：2012-01-17
申请号：US13097151
申请日：2011-04-29
申请人： Clay Woodward Jones
发明人： Clay Woodward Jones
IPC分类号： C08F6/22 , C08L27/18
CPC分类号： C08K5/32 , C08L27/12
摘要： An aqueous fluoropolymer dispersion comprising an aqueous medium, fluoropolymer particles, and an amine oxide surfactant. Coagulated fluoropolymer resin is produced from the dispersion by adding an acidic reagent in sufficient amount to cause coagulation and separation of the coagulated fluoropolymer resin from the aqueous medium. Another particulate component such as particular polymer, filler, pigment, solid lubricant, etc., may be added to the dispersion and co-coagulated to form a mixture of coagulated fluoropolymer resin and particulate component.
摘要翻译：一种包含含水介质，含氟聚合物颗粒和氧化胺表面活性剂的含氟聚合物水分散体。通过加入足够量的酸性试剂使分散体从凝胶化的含氟聚合物树脂与水性介质凝结分离，由分散体生成凝聚的含氟聚合物树脂。可以将另外的颗粒组分如特定的聚合物，填料，颜料，固体润滑剂等添加到分散体中并共凝固形成凝固的含氟聚合物树脂和颗粒组分的混合物。

8. 发明授权

US07872073B2 Dispersion spinning core-shell fluoropolymers 有权
标题翻译：分散纺丝芯 - 壳含氟聚合物
公开(公告)号：US07872073B2
公开(公告)日：2011-01-18
申请号：US12019804
申请日：2008-01-25
申请人： Clay Woodward Jones
发明人： Clay Woodward Jones
IPC分类号： C08L6/12
CPC分类号： D01D5/06 , C08L1/26 , C08L27/18 , D01D1/02 , D01F1/02 , D01F6/12 , D01F6/48 , Y10T428/3154 , C08L2666/26
摘要： A process is disclosed for dispersion spinning non-melt-processible fluoropolymer fiber in which a mixture of an aqueous dispersion of non-melt-processible fluoropolymer particles and an aqueous solution of a matrix polymer is formed. The non-melt-processible fluoropolymer particles have an SSG of less than about 2.40 and comprise a core of high molecular weight polytetrafluoroethylene and a shell of lower molecular weight polytetrafluoroethylene or modified polytetrafluoroethylene. The mixture is extruded into a coagulation bath containing a concentration of ions which coagulate the matrix polymer to form an intermediate fiber structure. The intermediate fiber structure is sintered to decompose the matrix polymer and coalesce the non-melt-processible fluoropolymer particles to form the fiber. The present invention also provides a spinning composition useful for the dispersion spinning of non-melt-processible fluoropolymer fiber.
摘要翻译：公开了用于分散纺丝不可熔融加工的含氟聚合物纤维的方法，其中形成了不可熔融加工的含氟聚合物颗粒的水性分散体和基质聚合物的水溶液的混合物。不可熔融加工的含氟聚合物颗粒具有小于约2.40的SSG，并且包含高分子量聚四氟乙烯核和低分子量聚四氟乙烯或改性聚四氟乙烯的壳。将混合物挤压成含有浓缩离子的凝固浴，其凝结基质聚合物以形成中间纤维结构。中间纤维结构被烧结以分解基质聚合物并聚结不可熔融加工的含氟聚合物颗粒以形成纤维。本发明还提供了一种可用于不可熔融加工的含氟聚合物纤维的分散纺丝的纺丝组合物。

9. 发明授权

US07754287B2 Process for forming filled bearings from fluoropolymer dispersions stabilized with anionic polyelectrolyte dispersing agents 失效
标题翻译：用阴离子聚电解质分散剂稳定的氟聚合物分散体形成填充轴承的方法
公开(公告)号：US07754287B2
公开(公告)日：2010-07-13
申请号：US11804547
申请日：2007-05-18
申请人： Robert John Cavanaugh , Clay Woodward Jones
发明人： Robert John Cavanaugh , Clay Woodward Jones
IPC分类号： B05D3/02
CPC分类号： C08L27/18 , C08K3/24 , C08L1/08 , C08L33/02 , C08L33/14 , C08L79/08 , C09D127/18 , C08L2666/26 , C08L2666/04 , C08L2666/20
摘要： The present invention provides a process for making a filled fluoropolymer bearing comprising providing an aqueous fluoropolymer dispersion comprising fluoropolymer particles and anionic polyelectrolyte dispersing agent in an amount sufficient for stabilization. The dispersion contains less than about 300 ppm fluorosurfactant based on the weight of the dispersion. The dispersion is coagulated to make a mush and a bearing filler is added to the dispersion prior to or after making the mush. The mush containing bearing filler is applied onto a bearing substrate to produce a coated substrate which is sintered and formed into a bearing.
摘要翻译：本发明提供了一种制备填充的含氟聚合物轴承的方法，包括提供含氟聚合物颗粒和阴离子聚电解质分散剂的水性含氟聚合物分散体，其量足以使其稳定。基于分散体的重量，分散体含有少于约300ppm的含氟表面活性剂。分散体凝结成糊状物，并且在制备糊料之前或之后将分散体加入到分散体中。将含糊的含轴承填料施加到轴承基材上以制备被烧结并形成轴承的涂覆基材。

10. 发明授权

US5760151A Tetrafluoroethylene copolymer 失效
公开(公告)号：US5760151A
公开(公告)日：1998-06-02
申请号：US691773
申请日：1996-01-02
申请人： Ralph Munson Aten , Clay Woodward Jones , Allan Harold Olson
发明人： Ralph Munson Aten , Clay Woodward Jones , Allan Harold Olson
IPC分类号： C08F214/26 , C08F16/24
CPC分类号： C08F214/262
摘要： Copolymers of tetrafluoroethylene and perfluoro(ethyl vinyl ether) having perfluoro(ethyl vinyl ether) content of at least 3 wt % exhibit excellent toughness even at melt viscosities of no greater than 25.times.10.sup.3 Pa.s. The copolymers can advantageously be made by aqueous dispersion copolymerization of the monomers in the absence of alkaline buffer and preferably in the absence of organic solvent.

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