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1. 发明授权

US5053560A Method for the continuous production of potassium tert-butoxide 失效
标题翻译：连续生产叔丁醇钾的方法
公开(公告)号：US5053560A
公开(公告)日：1991-10-01
申请号：US363292
申请日：1989-06-07
申请人： Rheinhard Matthes , Hartwig Rauleder , Hans-Joachim Vahlensieck
发明人： Rheinhard Matthes , Hartwig Rauleder , Hans-Joachim Vahlensieck
IPC分类号： C07C27/00 , C07C29/70 , C07C31/30 , C07C67/00
CPC分类号： C07C29/70
摘要： A method for the continuous production of anhydrous potassium tert-butoxide in a packed distillation column, wherein aqueous potash lye is fed with excess tert-butyl alcohol to the top of the column. Water formed in the reaction as well as water brought in with the reactants is distilled out at the top using methylcyclohexane or n-heptane as withdrawing agent. The amount of the withdrawing agent and of the tert-butanol must be selected such that above the column boiler a content between 0.2 and 2 wt.-% of the withdrawing agent is present in the gas mixture, while the gas mixture in the middle of the column has either between 32 and 34 wt.-% of methylcyclohexane or 36 to 38 wt.-% of n-heptane. The water together with the withdrawing agent and tert-butanol is withdrawn from the top of the column and then condensed. The organic phase of the condensate is fed back to the column.
摘要翻译：在填充蒸馏塔中连续生产无水叔丁醇钾的方法，其中将钾盐水溶液加入到塔顶部的过量叔丁醇。在反应中形成的水以及与反应物一起引入的水在顶部使用甲基环己烷或正庚烷作为萃取剂被蒸馏出来。取出剂和叔丁醇的量必须选择为使得在塔式锅炉以上，在气体混合物中存在取出剂的0.2至2重量％的含量，而在中间的气体混合物该柱具有32至34重量％的甲基环己烷或36至38重量％的正庚烷。将水与萃取剂和叔丁醇一起从塔顶排出，然后冷凝。将冷凝物的有机相反馈回塔中。

2. 发明授权

US4876337A Method and apparatus for the preparation of cyanoalkyl-alkoxysilanes 失效
标题翻译：用于制备氰基烷基 - 烷氧基硅烷的方法和设备
公开(公告)号：US4876337A
公开(公告)日：1989-10-24
申请号：US278736
申请日：1988-12-02
申请人： Hartwig Rauleder , Claus-Dietrich Seiler , Hans-Joachim Vahlensieck
发明人： Hartwig Rauleder , Claus-Dietrich Seiler , Hans-Joachim Vahlensieck
IPC分类号： C07F7/18
CPC分类号： C07F7/1892
摘要： In a method of preparing cyanoalkyl-akoxysilanes, which is suitable for the production of these silanes on a large technical scale, the reaction of a chloroalkyl-alkoxysilane with an alkali metal cyanide in the presence of a solvent takes place in a stirring reactor which is provided with means for loading these starting materials and with an outlet opening for the alkali metal chloride by-product, and which is connected through a bypass valve to a column with a superimposed condenser. After the reaction in the reactor has ended, first the solvent is distilled out through the column and then the main part of the cyanosilane, and then the rest of the cyanosilane is distilled out while bypassing the column. The alkali metal chloride is then removed from the reactor through a lock.
摘要翻译：在适用于大规模生产这些硅烷的氰基烷基 - 烷氧基硅烷的制备方法中，在溶剂存在下氯烷基烷氧基硅烷与碱金属氰化物的反应在搅拌反应器中进行，提供了用于装载这些原料的装置和用于碱金属氯化物副产物的出口，并且通过旁通阀连接到具有叠加的冷凝器的塔。在反应器中的反应结束后，首先通过柱蒸馏除去溶剂，然后将氰基硅烷的主要部分蒸馏掉，然后在绕过柱子的同时蒸馏掉其余的氰基硅烷。然后通过锁从反应器中除去碱金属氯化物。

3. 发明授权

US4987268A Process for the preparation of asymmetric terminally mono-unsaturated glycol ethers 失效
标题翻译：制备不对称末端单不饱和二醇醚的方法
公开(公告)号：US4987268A
公开(公告)日：1991-01-22
申请号：US491774
申请日：1990-03-12
申请人： Hartwig Rauleder , Hans-Joachim Kotzsch , Hans-Joachim Vahlensieck
发明人： Hartwig Rauleder , Hans-Joachim Kotzsch , Hans-Joachim Vahlensieck
IPC分类号： C07C41/16 , C07C43/15
CPC分类号： C07C41/16 , C07C41/38
摘要： Monoalkylethers of alkyleneglycols and oligoalkyleneglycols are reacted completely with terminally unsaturated alkenyl halides to form terminally mono unsaturated glycolethers as product, wherein initially a complete reaction to the corresponding alcoholate takes place with only one equivalent of alcoholate former, such as alkali metal alcoholate or hydroxide, and two equivalents of glycolmonoether, then the alcoholate is reacted with one equivalent of alkenyl halide, whereupon a mixture of the desired product and the glycolmonoether of the alkali metal halide is filtered or distilled off, then this mixture is reacted with the second equivalent of the alcoholate former, whereupon the recovery of the product takes place by distillation from the reaction mixture and then, after addition of a further equivalent of glycolmonoether to the residue from the product recovery, the reaction of the first and the subsequent steps is repeated.
摘要翻译：亚烷基二醇和低聚亚烷基二醇的单烷基醚与末端不饱和烯烃卤化物完全反应，形成作为产物的末端单不饱和糖单体，其中最初只用一当量的醇化物，例如碱金属醇盐或氢氧化物与相应的醇化物完全反应， 2当量的二醇单醚，然后醇化物与1当量的烯基卤反应，然后将所需产物和碱金属卤化物的二醇单醚的混合物过滤或蒸除，然后将该混合物与第二当量的醇化物因此，通过蒸馏从反应混合物中回收产物，然后在从产物回收的残余物中加入另外当量的二醇单醚后，重复第一步骤和随后步骤的反应。

4. 发明授权

US09908781B2 Process and use of amino-functional resins for dismutating halosilanes and for removing extraneous metals 有权
公开(公告)号：US09908781B2
公开(公告)日：2018-03-06
申请号：US13383681
申请日：2010-05-18
申请人： Ekkehard Mueh , Hartwig Rauleder , Jaroslaw Monkiewicz , Reinhold Schork
发明人： Ekkehard Mueh , Hartwig Rauleder , Jaroslaw Monkiewicz , Reinhold Schork
IPC分类号： C01B33/107
CPC分类号： C01B33/107 , C01B33/10773 , C01B33/10784 , C01P2006/80
摘要： The invention relates to a process for dismutating at least one halosilane and reducing the content of extraneous metal and/or a compound containing extraneous metal in the at least one halosilane and in the at least one silane obtained, by contacting at least one halosilane of the general formula I, HnSiClm (I), where n and m are integers and n=1, 2 or 3 and m=1, 2 or 3 and n+m=4, with a particulate, organic, amino-functional resin to obtain at least one silane of the general formula II, HaSiClb (II), where a and b are integers and a=0, 2, 3 or 4 and b=0, 1, 2 or 4 where a+b=4, in one step, in which the content of extraneous metal and/or compounds containing extraneous metal has been reduced compared to the halosilane of the formula I. The invention further provides for the use of this resin for dismutating halosilanes and as an absorbent of extraneous metals or compounds containing extraneous metal in a process for preparing monosilane.

5. 发明授权

US09618466B2 Use of specific resistivity measurement for indirect determination of the purity of silanes and germanes and a corresponding process 有权
公开(公告)号：US09618466B2
公开(公告)日：2017-04-11
申请号：US13580843
申请日：2010-12-28
申请人： Ekkehard Mueh , Hartwig Rauleder , Rainer Amend , Martin Hajduk
发明人： Ekkehard Mueh , Hartwig Rauleder , Rainer Amend , Martin Hajduk
IPC分类号： C23C16/00 , G01N27/04 , G01N33/00
CPC分类号： G01N27/04 , G01N2033/0095
摘要： The invention relates to a method for indirectly determining the purity of silanes and germanes using a device for measuring specific resistance. The invention further relates to a system for industrially producing and/or filling containers with silanes or germanes, including a quality control in which a device is used for measuring specific resistance.

6. 发明授权

US09593021B2 Method for processing finely divided solids during production of chlorosilanes 有权
标题翻译：在氯硅烷生产过程中加工细碎固体的方法
公开(公告)号：US09593021B2
公开(公告)日：2017-03-14
申请号：US14649353
申请日：2013-11-21
申请人： Janaina Marinas Perez , Ekkehard Mueh , Hartwig Rauleder , Frank Kropfgans
发明人： Janaina Marinas Perez , Ekkehard Mueh , Hartwig Rauleder , Frank Kropfgans
IPC分类号： C01B33/107 , C01B33/00 , C08K11/00
CPC分类号： C01B33/00 , C01B33/107 , C01B33/10742 , C08K11/005
摘要： The invention provides a method for the processing of finely divided solids during the production of chlorosilanes, which is characterized in that the finely divided solids are hydraulically pressed to give bodies of increased density. Moreover, also provided is the compact obtained by the process according to the invention which is characterized by a filling factor of the finely divided solids to be hydraulically pressed of 3.9 to 4.5.
摘要翻译：本发明提供了在制备氯代硅烷期间处理细碎固体的方法，其特征在于将细碎的固体液压地挤压以提供增加密度的体。此外，还提供了通过根据本发明的方法获得的压块，其特征在于待液压压制的细碎固体的填充因子为3.9至4.5。

7. 发明授权

US09481580B2 Selective splitting of high order silanes 有权
标题翻译：选择性分裂高阶硅烷
公开(公告)号：US09481580B2
公开(公告)日：2016-11-01
申请号：US13884473
申请日：2011-10-24
申请人： Ekkehard Mueh , Hartwig Rauleder
发明人： Ekkehard Mueh , Hartwig Rauleder
IPC分类号： C01B33/107 , C01B33/04 , C01B33/08 , B01J37/06 , B01J21/08 , B01J37/02
CPC分类号： C01B33/10742 , B01J21/08 , B01J37/0215 , B01J37/06 , C01B33/043 , C01B33/08 , C01B33/107 , C01B33/1071 , C01B33/10773
摘要： The invention relates to a process for preparing monomeric and/or dimeric halogen- and/or hydrogen-containing silicon compounds from oligomeric inorganic silanes having three or more directly covalently interconnected silicon atoms substituted by substituents selected from halogen, hydrogen and/or oxygen by reacting the oligomeric silane over a nitrogen-containing catalyst in the presence of hydrogen halide.
摘要翻译：本发明涉及一种由低聚无机硅烷制备单体和/或二聚的卤素和/或含氢硅化合物的方法，其具有三个或更多个直接共价连接的硅原子，其被选自卤素，氢和/或氧的取代基取代，在卤化氢存在下，在含氮催化剂上的低聚硅烷。

8. 发明申请

US20150102070A1 CONTAINER FOR HANDLING AND TRANSPORTING OF HIGH-PURITY AND ULTRA-HIGH-PURITY CHEMICALS 审中-公开
标题翻译：用于处理和运输高纯度和超高纯化学品的容器
公开(公告)号：US20150102070A1
公开(公告)日：2015-04-16
申请号：US14383757
申请日：2013-02-11
申请人： Ekkehard Mueh , Hartwig Rauleder , Bernd Nowitzki , Harald Klein
发明人： Ekkehard Mueh , Hartwig Rauleder , Bernd Nowitzki , Harald Klein
IPC分类号： B67D7/02 , B65B3/00 , B67D7/84
CPC分类号： B67D7/0294 , B65B3/00 , B67D7/025 , B67D7/0261 , B67D7/0272 , B67D7/0283 , B67D7/84
摘要： The invention relates to an empty container (1) for accommodating high-purity and ultra-high-purity, air- and/or moisture-sensitive liquid or condensable compounds, comprising a cylindrical jacket (3), a bottom (4a) and an upper end piece (4b, 4b′) at the two ends of the cylindrical jacket, an associated connection unit (2) including shut-off/multiple-way and rinsing system (5), and an associated immersion pipe (7), characterized in that the lower end of the immersion pipe (7a) protrudes into a recess (4c) (depression), which is introduced in the bottom (4a) and which is the lowest point of the bottom, and/or the lower end of the immersion pipe (7a) is tapered and is brought close to the lowest point of the bottom (4a) to within less than 2 mm by means of the tip of the tapered immersion pipe (7b) or touches the lowest point of the bottom with the tip of the tapered immersion pipe (7b). The invention further relates to the use of empty containers according to the invention for storing, handling, and/or transporting such high-purity and ultra-high-purity compounds.
摘要翻译：本发明涉及一种用于容纳高纯度和超高纯度空气和/或湿度敏感性液体或可冷凝化合物的空容器（1），其包括圆柱形护套（3），底部（4a）和包括关闭/多路和冲洗系统（5）的关联连接单元（2）和相关联的浸入式管道（7），其特征在于，所述圆柱形套管两端的上端件（4b，4b'）浸入管（7a）的下端突出到凹入部（4c）（凹陷部）（凹部），该凹部被引入到底部（4a）中，并且是底部的最低点，和/ 浸入管（7a）是锥形的，并且通过锥形浸入管（7b）的尖端使其靠近底部（4a）的最低点到小于2mm内，或者接触底部的最低点锥形浸入管（7b）的尖端。本发明还涉及根据本发明的用于储存，处理和/或运输这种高纯度和超高纯度化合物的空容器的用途。

9. 发明授权

US08722913B2 Method for producing higher silanes 有权
标题翻译：生产高级硅烷的方法
公开(公告)号：US08722913B2
公开(公告)日：2014-05-13
申请号：US12524371
申请日：2007-12-20
申请人： Juergen Erwin Lang , Hartwig Rauleder , Ekkehard Mueh
发明人： Juergen Erwin Lang , Hartwig Rauleder , Ekkehard Mueh
IPC分类号： C07F7/12
CPC分类号： B01J19/088 , B01J2219/0803 , B01J2219/0894 , C01B21/068 , C01B21/0823 , C01B32/907 , C01B33/04 , C01B33/107 , C01B33/12 , C01B33/36 , C01G17/00 , C01P2002/86 , C07F7/083 , C07F7/30
摘要： The invention relates to a method for producing dimeric and/or trimeric silicon compounds, in particular silicon halogen compounds. The claimed method is also suitable for producing corresponding germanium compounds. The invention also relates to a device for carrying out said method to the use of the produced silicon compounds.
摘要翻译：本发明涉及二聚和/或三聚硅化合物，特别是硅卤素化合物的制备方法。所要求保护的方法也适用于生产相应的锗化合物。本发明还涉及用于实施所述方法来使用所生产的硅化合物的装置。

10. 发明申请

US20140072803A1 HIGH-PURITY SILICON DIOXIDE GRANULES FOR QUARTZ GLASS APPLICATIONS AND METHOD FOR PRODUCING SAID GRANULES 审中-公开
标题翻译：用于石墨玻璃应用的高纯度二氧化硅颗粒和生产颗粒的方法
公开(公告)号：US20140072803A1
公开(公告)日：2014-03-13
申请号：US14000954
申请日：2012-02-10
申请人： Christian Panz , Guido Titz , Sven Müller , Markus Ruf , Bodo Frings , Hartwig Rauleder , Jürgen Behnisch
发明人： Christian Panz , Guido Titz , Sven Müller , Markus Ruf , Bodo Frings , Hartwig Rauleder , Jürgen Behnisch
IPC分类号： C01B33/12 , C03C14/00
CPC分类号： C01B33/193 , C01B33/124 , C01B33/126 , C01B33/128 , C01P2004/60 , C01P2006/14 , C01P2006/17 , C01P2006/80 , C03B19/1065 , C03B19/1095 , C03C1/022 , C03C14/008 , Y10T428/2982
摘要： It has been found that conventional cheap waterglass qualities in a strongly acidic medium react to give high-purity silica grades, the treatment of which with a base leads to products which can be processed further to give glass bodies with low silanol group contents.
摘要翻译：已经发现，在强酸性介质中常规的廉价水玻璃质量反应以得到高纯度二氧化硅等级，用碱处理可以进一步处理可以进一步提供具有低硅烷醇基含量的玻璃体的产品。

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