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    • 4. 发明申请
    • METHOD FOR PRODUCING POLYACRYLIC ACID (SALT)-BASED WATER ABSORBENT RESIN POWDER
    • 生产聚丙烯酸(盐) - 水吸收树脂粉末的方法
    • US20130102750A1
    • 2013-04-25
    • US13643682
    • 2011-04-27
    • Yusuke WatanabeKazushi ToriiKozo NogiKunihiko IshizakiReiko NakatsuruShigeru Sakamoto
    • Yusuke WatanabeKazushi ToriiKozo NogiKunihiko IshizakiReiko NakatsuruShigeru Sakamoto
    • C08J3/12C08F122/10
    • C08J3/12C08F6/008C08F122/105C08F220/06C08J3/122C08J3/245C08J2333/02C08L33/02
    • A water absorbent resin having less fine powder or powdery dust and a controlled particle size is provided, and the water absorption rate of the water absorbent resin is increased by a simple method at low cost, while maintaining or improving other physical properties such as liquid permeability. Disclosed is a method for producing a polyacrylic acid (salt)-type water absorbent resin powder, which includes, in sequence, a step of polymerizing an aqueous solution of acrylic acid (salt)-type monomer; a step of gel-crushing a gel of a water-containing gel-like crosslinked polymer during polymerization or after polymerization; a step of drying the water-containing gel-like crosslinked polymer; and a step of pulverizing and classifying the dried polymer, wherein water absorbent resin fine particles having a particle size of less than 150 μm or a hydrated-particles thereof is added to a step prior to the drying step, and in the drying step, hot air drying is carried out with a hot air having an average flow velocity of 1.0 to 3.0 [m/s], a dew point of 30° C. to 100° C., and a hot air temperature of 140° C. to 235° C.
    • 提供具有较少粉末或粉末粉尘和受控粒度的吸水性树脂,并且通过简单的方法以低成本提高吸水性树脂的吸水率,同时保持或改善其它物理性质如液体渗透性 。 公开了一种聚丙烯酸(盐)型吸水性树脂粉末的制造方法,其中,依次包括使丙烯酸(盐)型单体的水溶液聚合的工序; 在聚合过程中或聚合后凝胶化凝胶状凝胶状交联聚合物凝胶的步骤; 干燥含水凝胶状交联聚合物的工序; 以及将干燥聚合物粉碎分级的步骤,其中将粒径小于150μm的吸水性树脂细颗粒或其水合物颗粒加入到干燥步骤之前的步骤中,并且在干燥步骤中,热 使用平均流速为1.0〜3.0 [m / s],露点为30℃〜100℃,热风温度为140℃〜235℃的热风进行空气干燥 C。
    • 5. 发明授权
    • Method for producing polyacrylic acid (salt) type water absorbent resin powder
    • 聚丙烯酸(盐)型吸水性树脂粉末的制造方法
    • US08765906B2
    • 2014-07-01
    • US13643682
    • 2011-04-27
    • Yusuke WatanabeKazushi ToriiKozo NogiKunihiko IshizakiReiko NakatsuruShigeru Sakamoto
    • Yusuke WatanabeKazushi ToriiKozo NogiKunihiko IshizakiReiko NakatsuruShigeru Sakamoto
    • C08G63/02C08G63/00
    • C08J3/12C08F6/008C08F122/105C08F220/06C08J3/122C08J3/245C08J2333/02C08L33/02
    • A water absorbent resin having less fine powder or powdery dust and a controlled particle size is provided, and the water absorption rate of the water absorbent resin is increased by a simple method at low cost, while maintaining or improving other physical properties such as liquid permeability. Disclosed is a method for producing a polyacrylic acid (salt)-type water absorbent resin powder, which includes, in sequence, a step of polymerizing an aqueous solution of acrylic acid (salt)-type monomer; a step of gel-crushing a gel of a water-containing gel-like crosslinked polymer during polymerization or after polymerization; a step of drying the water-containing gel-like crosslinked polymer; and a step of pulverizing and classifying the dried polymer, wherein water absorbent resin fine particles having a particle size of less than 150 μm or a hydrated-particles thereof is added to a step prior to the drying step, and in the drying step, hot air drying is carried out with a hot air having an average flow velocity of 1.0 to 3.0 [m/s], a dew point of 30° C. to 100° C., and a hot air temperature of 140° C. to 235° C.
    • 提供具有较少粉末或粉末粉尘和受控粒度的吸水性树脂,并且通过简单的方法以低成本提高吸水性树脂的吸水率,同时保持或改善其它物理性质如液体渗透性 。 公开了一种聚丙烯酸(盐)型吸水性树脂粉末的制造方法,其中,依次包括使丙烯酸(盐)型单体的水溶液聚合的工序; 在聚合过程中或聚合后凝胶化凝胶状凝胶状交联聚合物凝胶的步骤; 干燥含水凝胶状交联聚合物的工序; 将干燥聚合物粉碎并分级的步骤,其中在干燥步骤之前的步骤中加入粒径小于150μm的吸水性树脂微粒或其水合颗粒,并且在干燥步骤中,热 使用平均流速为1.0〜3.0 [m / s],露点为30℃〜100℃,热风温度为140℃〜235℃的热风进行空气干燥 C。