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1. 发明申请

US20100249434A1 METHOD FOR THE VINYLATION OF AMIDES 有权
标题翻译：氨基乙酸乙酯的方法
公开(公告)号：US20100249434A1
公开(公告)日：2010-09-30
申请号：US12744428
申请日：2008-12-08
申请人： Regina Vogelsang , Stefan Kaeshammer , Wolfgang Staffel , Ulrich Eiden , Alexandra Brand , Lembit Tuttelberg
发明人： Regina Vogelsang , Stefan Kaeshammer , Wolfgang Staffel , Ulrich Eiden , Alexandra Brand , Lembit Tuttelberg
IPC分类号： C07D207/26 , C07C233/09
CPC分类号： C07D207/267
摘要： A process for preparing an N-vinyl compound by vinylating a compound having at least one nitrogen atom (referred to hereinafter as compound for short) with acetylene, wherein before the vinylation, the compound is reacted with an alkali metal hydroxide in a reaction zone and the mean residence time of the alkali metal hydroxide and of the compound in the reaction zone is less than 6 minutes.
摘要翻译：通过用乙炔将具有至少一个氮原子的化合物（以下简称为化合物）乙烯化制备N-乙烯基化合物的方法，其中在乙烯化之前，化合物与反应区中的碱金属氢氧化物反应，碱金属氢氧化物和化合物在反应区中的平均停留时间小于6分钟。

2. 发明授权

US09249094B2 Method for the vinylation of amides 有权
标题翻译：乙酰化的方法
公开(公告)号：US09249094B2
公开(公告)日：2016-02-02
申请号：US12744428
申请日：2008-12-08
申请人： Regina Vogelsang , Stefan Kaeshammer , Wolfgang Staffel , Ulrich Eiden , Alexandra Brand , Lembit Tuttelberg
发明人： Regina Vogelsang , Stefan Kaeshammer , Wolfgang Staffel , Ulrich Eiden , Alexandra Brand , Lembit Tuttelberg
IPC分类号： C07D207/267
CPC分类号： C07D207/267
摘要： A process for preparing an N-vinyl compound by vinylating a compound having at least one nitrogen atom (referred to hereinafter as compound for short) with acetylene, wherein before the vinylation, the compound is reacted with an alkali metal hydroxide in a reaction zone and the mean residence time of the alkali metal hydroxide and of the compound in the reaction zone is less than 6 minutes.
摘要翻译：通过用乙炔将具有至少一个氮原子的化合物（以下简称为化合物）乙烯化制备N-乙烯基化合物的方法，其中在乙烯化之前，化合物与反应区中的碱金属氢氧化物反应，碱金属氢氧化物和化合物在反应区中的平均停留时间小于6分钟。

3. 发明申请

US20080312432A1 Stabilizers for Use in Nvp Synthesis 失效
标题翻译：稳定剂用于Nvp合成
公开(公告)号：US20080312432A1
公开(公告)日：2008-12-18
申请号：US11659331
申请日：2005-08-04
申请人： Frank Hofer , Alexandra Brand , Arnd Bottcher , Katrin Baumann , Regina Vogelsang
发明人： Frank Hofer , Alexandra Brand , Arnd Bottcher , Katrin Baumann , Regina Vogelsang
IPC分类号： C07D223/10 , C07D207/267
CPC分类号： C07D207/20 , C07C231/08
摘要： A process for preparing N-alkenyl compounds by reacting the corresponding NH compounds with alkynes in the liquid phase in the presence of a catalyst, wherein the reaction is carried out in the presence of at least one stabilizer, and the use of stabilizers for increasing the selectivity in a process for preparing N-alkenyl compounds by reacting the corresponding NH compounds with alkynes in the liquid phase in the presence of a catalyst.
摘要翻译：一种在催化剂存在下使相应的NH化合物与液相中的炔反应制备N-烯基化合物的方法，其中该反应在至少一种稳定剂存在下进行，并且使用稳定剂来增加在催化剂存在下，使相应的NH化合物与液相中的炔反应制备N-烯基化合物的方法中的选择性。

4. 发明授权

US07674934B2 Stabilizers for use in NVP synthesis 失效
标题翻译：用于NVP合成的稳定剂
公开(公告)号：US07674934B2
公开(公告)日：2010-03-09
申请号：US11659331
申请日：2005-08-04
申请人： Frank Hoefer , Alexandra Brand , Arnd Boettcher , Katrin Baumann , Regina Vogelsang
发明人： Frank Hoefer , Alexandra Brand , Arnd Boettcher , Katrin Baumann , Regina Vogelsang
IPC分类号： C07C231/12 , C07D233/58 , C07D207/12 , C07D211/02 , C07D201/02
CPC分类号： C07D207/20 , C07C231/08
摘要： A process for preparing N-alkenyl compounds by reacting the corresponding NH compounds with alkynes in the liquid phase in the presence of a catalyst, wherein the reaction is carried out in the presence of at least one stabilizer, and the use of stabilizers for increasing the selectivity in a process for preparing N-alkenyl compounds by reacting the corresponding NH compounds with alkynes in the liquid phase in the presence of a catalyst.
摘要翻译：一种在催化剂存在下使相应的NH化合物与液相中的炔反应制备N-烯基化合物的方法，其中该反应在至少一种稳定剂存在下进行，并且使用稳定剂来增加在催化剂存在下，使相应的NH化合物与液相中的炔反应制备N-烯基化合物的方法中的选择性。

5. 发明授权

US07687667B2 Catalyst for the production of methyl mercaptan from methanol and hydrogen sulfide 有权
标题翻译：用于从甲醇和硫化氢生产甲硫醇的催化剂
公开(公告)号：US07687667B2
公开(公告)日：2010-03-30
申请号：US10554701
申请日：2004-04-23
申请人： Alexandra Brand , Veronika Quaschning
发明人： Alexandra Brand , Veronika Quaschning
IPC分类号： C07C319/00
CPC分类号： B01J37/20 , B01J21/04 , B01J23/30 , B01J27/047 , B01J27/053 , B01J27/188 , B01J37/28 , C07C319/08 , C07C321/04
摘要： The invention relates to a catalyst for the synthesis of methyl mercaptan from hydrogen sulfide and methanol and to a process for preparing methyl mercaptans. The catalyst comprises active aluminum oxide on which an alkali metal tungstate and ammonium salts have been deposited.
摘要翻译：本发明涉及用于从硫化氢和甲醇合成甲硫醇的催化剂以及制备甲硫醇的方法。催化剂包含其上沉积有碱金属钨酸盐和铵盐的活性氧化铝。

6. 发明授权

US06410771B1 Fluorinated copper salts as catalysts for the synthesis of trialkoxysilanes 失效
标题翻译：氟化铜盐作为合成三烷氧基硅烷的催化剂
公开(公告)号：US06410771B1
公开(公告)日：2002-06-25
申请号：US09901893
申请日：2001-07-11
申请人： Alexandra Brand
发明人： Alexandra Brand
IPC分类号： C07F718
CPC分类号： C07F7/025
摘要： In a process for preparing trialkoxysilanes by reaction of silicon metal with an alcohol in an inert solvent in the presence of a copper catalyst, the copper catalyst used is a copper salt whose anion contains at least one nonhydrolyzable fluorine atom, or a mixture thereof with other salts.
摘要翻译：在铜催化剂存在下，通过硅烷与醇在惰性溶剂中反应制备三烷氧基硅烷的方法中，使用的铜催化剂是一种铜盐，其阴离子含有至少一个不可水解的氟原子，或其与其它物质的混合物盐。

7. 发明授权

US06255514B1 Isolation of trimethoxysilane from a TMS/methanol mixture 失效
标题翻译：从TMS /甲醇混合物中分离三甲氧基硅烷
公开(公告)号：US06255514B1
公开(公告)日：2001-07-03
申请号：US09677863
申请日：2000-10-03
申请人： Alexandra Brand , Hans-Josef Sterzel
发明人： Alexandra Brand , Hans-Josef Sterzel
IPC分类号： C07F708
CPC分类号： C07F7/045
摘要： In an extraction process for isolating trimethoxysilane (TMS) from a TMS/methanol mixture by formation of two phases, namely a TMS-rich extract phase and a methanol-rich raffinate phase, by addition of one or more methanol-soluble inorganic and/or organic salts and, if desired, an additional nonpolar organic solvent and subsequent phase separation, the amount of salt added is selected so that the weight ratio of trimethoxysilane to methanol in the extract phase is at least 94% by weight:6% by weight (normalized to 100% by weight). The use of one or more inorganic salts in an extraction process for isolating trimethoxysilane from a trimethoxysilane/methanol mixture is also claimed.
摘要翻译：在通过形成两相（即富含TMS的提取相和富含甲醇的萃余相）从TMS /甲醇混合物中分离三甲氧基硅烷（TMS）的萃取方法中，通过加入一种或多种甲醇溶解的无机和/或有机盐，并且如果需要，另外的非极性有机溶剂和随后的相分离，选择加入的盐的量，使得萃取相中三甲氧基硅烷与甲醇的重量比为至少94重量％：6重量％归一化至100重量％）。还要求在三甲氧基硅烷/甲醇混合物中分离三甲氧基硅烷的提取方法中使用一种或多种无机盐。

8. 发明申请

US20070015941A1 Catalyst for the production of methyl mercaptan from methanol and hydrogen sulfide 有权
标题翻译：用于从甲醇和硫化氢生产甲硫醇的催化剂
公开(公告)号：US20070015941A1
公开(公告)日：2007-01-18
申请号：US10554701
申请日：2004-04-23
申请人： Alexandra Brand , Veronika Quaschning
发明人： Alexandra Brand , Veronika Quaschning
IPC分类号： C07C319/02
CPC分类号： B01J37/20 , B01J21/04 , B01J23/30 , B01J27/047 , B01J27/053 , B01J27/188 , B01J37/28 , C07C319/08 , C07C321/04
摘要： The invention relates to a catalyst for the synthesis of methyl mercaptan from hydrogen sulfide and methanol and to a process for preparing methyl mercaptans. The catalyst comprises active aluminum oxide on which an alkali metal tungstate and ammonium salts have been deposited.
摘要翻译：本发明涉及用于从硫化氢和甲醇合成甲硫醇的催化剂以及制备甲硫醇的方法。催化剂包含其上沉积有碱金属钨酸盐和铵盐的活性氧化铝。

9. 发明授权

US06380414B2 Freshly precipitated CuO as catalyst for the trialkoxysilane synthesis 失效
标题翻译：新近沉淀的CuO作为三烷氧基硅烷合成的催化剂
公开(公告)号：US06380414B2
公开(公告)日：2002-04-30
申请号：US09860485
申请日：2001-05-21
申请人： Alexandra Brand
发明人： Alexandra Brand
IPC分类号： C07F708
CPC分类号： C07F7/025
摘要： Trialkoxysilanes are prepared by reacting silicon metal with an alcohol in an inert solvent in the presence of a copper catalyst by a process in which the copper catalyst contains copper(II) oxide having a BET surface area of ≧10 m2/g. Furthermore, this copper catalyst is used for the preparation of trialkoxysilanes by reacting silicon metal with an alcohol.
摘要翻译：三烷氧基硅烷通过使铜催化剂含有BET表面积> 10m 2 / g的氧化铜（II）的方法，在铜催化剂的存在下，在惰性溶剂中使硅金属与醇反应制备。此外，该铜催化剂用于通过使硅金属与醇反应来制备三烷氧基硅烷。

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