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    • 3. 发明授权
    • Apparatus and method for introducing small amounts of refractory elements into a vapor deposition coating
    • 将少量难熔元素引入气相沉积涂层的装置和方法
    • US06689199B2
    • 2004-02-10
    • US10272236
    • 2002-10-16
    • Reed Roeder CordermanMelvin Robert JacksonRichard Arthur Nardi, Jr.
    • Reed Roeder CordermanMelvin Robert JacksonRichard Arthur Nardi, Jr.
    • C23C1606
    • C23C14/30C23C14/16Y02T50/67
    • A method of introducing small amounts of a refractory element into a vapor deposition coating. A second material (30), containing at least two elements which are desired to be deposited as a coating on a base material, has placed over it a first material (20) substantially comprising such two elements and a refractory element. The first material (20) is adapted to permit transport of the at least two elements in the second material (30) through the first material (20) when the first (20) and second (30) material are in a molten state and in touching contact with the other so as to permit evaporation of the two elements and the refractory element from an exposed surface. Heat is supplied to the first (20) and second (30) materials to permit evaporation of the at least two elements of second material (30) and the refractory element in the first material (20), and the resulting vapors are condensed as a deposit on a base material (50). A particular method of heating is further disclosed to assist in maintaining adequate rates of evaporation for the aforesaid method, wherein the supplied heat is supplied to an inner heated area (91) and a surrounding outer heated area (92) and at least a portion of the inner heated area (91) is heated to a greater temperature than the outer heated area (92).
    • 将少量耐火材料引入气相沉积涂层的方法。 包含至少两个期望作为涂层涂覆在基材上的元件的第二材料(30)已经在其上放置了基本上包含这两个元件和难熔元件的第一材料(20)。 当第一(20)和第二(30)材料处于熔融状态时,第一材料(20)适于允许第二材料(30)中的至少两个元件通过第一材料(20) 与另一个接触,以允许两个元件和耐火元件从暴露的表面蒸发。 将热量供应到第一(20)和第二(30)材料以允许第一材料(20)中的第二材料(30)的至少两个元件和耐火元件蒸发,并且所得到的蒸气被冷凝为 沉积在基材(50)上。 进一步公开了一种特定的加热方法,以有助于为上述方法保持足够的蒸发速率,其中供应的热量被供应到内部加热区域(91)和周围的外部加热区域(92)和至少一部分 内加热区域(91)被加热到比外部加热区域(92)更高的温度。
    • 4. 发明授权
    • Apparatus and method for introducing small amounts of refractory elements into a vapor deposition coating
    • 将少量难熔元素引入气相沉积涂层的装置和方法
    • US06849299B2
    • 2005-02-01
    • US10272256
    • 2002-10-16
    • Reed Roeder CordermanMelvin Robert JacksonRichard Arthur Nardi, Jr.
    • Reed Roeder CordermanMelvin Robert JacksonRichard Arthur Nardi, Jr.
    • C23C14/16C23C14/30
    • C23C14/30C23C14/16Y02T50/67
    • A method of introducing small amounts of a refractory element into a vapor deposition coating. A second material (30), containing at least two elements which are desired to be deposited as a coating on a base material, has placed over it a first material (20) substantially comprising such two elements and a refractory element. The first material (20) is adapted to permit transport of the at least two elements in the second material (30) through the first material (20) when the first (20) and second (30) material are in a molten state and in touching contact with the other so as to permit evaporation of the two elements and the refractory element from an exposed surface. Heat is supplied to the first (20) and second (30) materials to permit evaporation of the at least two elements of second material (30) and the refractory element in the first material (20), and the resulting vapors are condensed as a deposit on a base material (50). A particular method of heating is further disclosed to assist in maintaining adequate rates of evaporation for the aforesaid method, wherein the supplied heat is supplied to an inner heated area (91) and a surrounding outer heated area (92) and at least a portion of the inner heated area (91) is heated to a greater temperature than the outer heated area (92).
    • 将少量耐火材料引入气相沉积涂层的方法。 包含至少两个期望作为涂层涂覆在基材上的元件的第二材料(30)已经在其上放置了基本上包含这两个元件和难熔元件的第一材料(20)。 当第一(20)和第二(30)材料处于熔融状态时,第一材料(20)适于允许第二材料(30)中的至少两个元件通过第一材料(20) 与另一个接触,以允许两个元件和耐火元件从暴露的表面蒸发。 将热量供应到第一(20)和第二(30)材料以允许第一材料(20)中的第二材料(30)的至少两个元件和耐火元件蒸发,并且所得到的蒸气被冷凝为 沉积在基材(50)上。 进一步公开了一种特定的加热方法,以有助于为上述方法保持足够的蒸发速率,其中供应的热量被供应到内部加热区域(91)和周围的外部加热区域(92)和至少一部分 内加热区域(91)被加热到比外部加热区域(92)更高的温度。
    • 5. 发明授权
    • Method of using a substrate offset to obtain a specific alloy chemistry from a metal alloy EB-PVD coating process
    • 使用基板偏移以从金属合金EB-PVD涂覆工艺获得特定合金化学的方法
    • US06174571B1
    • 2001-01-16
    • US09387373
    • 1999-08-31
    • Reed Roeder CordermanRichard Arthur Nardi, Jr.
    • Reed Roeder CordermanRichard Arthur Nardi, Jr.
    • C23C1430
    • C23C14/548C23C14/24
    • A method of making an evaporated deposit of a material comprising the steps of: (i) positioning at least one test substrate above a vapor source wherein at least a portion of the at least one test substrate is not perpendicularly disposed to vapor source, (ii) heating the vapor source in a vacuum to evaporate the vapor source, (iii) condensing a deposit evaporated from the vapor source on the at least one test substrate such that at least a portion of the deposit is not perpendicularly deposed to the vapor source, (iv) measuring the chemical composition of the deposit at various positions relative to a line normal to the vapor source, (v) repeating steps (i) through (iv) until a deposit having a desired chemical composition is measured, (vi) removing each of the at least one test substrate, (vii) positioning a workpiece above the vapor source at a location corresponding to that of the test substrate upon which a deposit of desired chemical composition is condensed and measured, (viii) heating the vapor source in a vacuum to evaporate the vapor source, and (ix) condensing a deposit evaporated from the vapor source on the workpiece.
    • 一种制造材料的蒸发沉积的方法,包括以下步骤:(i)将至少一个测试衬底定位在蒸气源上方,其中至少一部分测试衬底不垂直于蒸气源放置,(ii )在真空中加热蒸气源以蒸发蒸气源,(iii)将来自蒸气源的沉积物冷凝在至少一个测试基板上,使得沉积物的至少一部分不垂直于蒸气源, (iv)测量相对于垂直于蒸汽源的线的各个位置的沉积物的化学成分,(v)重复步骤(i)至(iv),直到测量具有所需化学成分的沉积物,(vi) 所述至少一个测试基板中的每一个,(vii)将工件放置在所述蒸汽源上方的位置处,所述位置对应于所述测试基板的位置,在所述测试基板上凝结和测量所需化学组成的沉积物, 在真空中加热蒸气源以蒸发蒸气源,和(ix)将从蒸气源蒸发的沉积物冷凝在工件上。