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1. 发明授权

US5482812A Wax Containing toner aggregation processes 失效
标题翻译：蜡含有调色剂聚集工艺
公开(公告)号：US5482812A
公开(公告)日：1996-01-09
申请号：US344060
申请日：1994-11-23
申请人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Stephan V. Drappel , Paul J. Gerroir
发明人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Stephan V. Drappel , Paul J. Gerroir
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/0815
摘要： A process for the preparation of toner compositions or toner particles comprising:(i) providing an aqueous pigment dispersion comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) providing a wax dispersion comprised of wax, a dispersant comprised of nonionic surfactant, ionic surfactant or mixtures thereof;(iii) shearing a mixture of the wax dispersion and the pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant;(iv) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(v) adding additional ionic surfactant to the aggregated suspension of (iv) to ensure that no, or minimal additional particle growth of the electrostatically bound toner size aggregates occurs on further increasing the temperature to coalesce the aggregates into toner particles (vi);(vi) heating the mixture of (v) with bound aggregates above about or at the Tg of the resin; and optionally(vii) separating the toner particles from the aqueous slurry by filtration and thereafter optionally washing.
摘要翻译：一种制备调色剂组合物或调色剂颗粒的方法，包括：（i）提供由颜料，离子表面活性剂和任选的电荷控制剂组成的水性颜料分散体; （ii）提供由蜡组成的蜡分散体，由非离子表面活性剂，离子表面活性剂或其混合物组成的分散剂; （iii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂组成的胶乳或乳液共混物来剪切蜡分散体和颜料分散体的混合物; （iv）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （v）向（iv）的聚集悬浮液中加入另外的离子表面活性剂，以确保在进一步升高温度以使聚集体聚结成调色剂颗粒（vi）时，静电结合的调色剂尺寸聚集体不会发生或最小的附加颗粒生长。（vi）将（v）混合物加热至高于树脂Tg或高于Tg的结合聚集体; 并且任选地（vii）通过过滤从调色剂颗粒与含水浆料分离，然后任选地洗涤。

2. 发明授权

US5501935A Toner aggregation processes 失效
标题翻译：调色剂聚合过程
公开(公告)号：US5501935A
公开(公告)日：1996-03-26
申请号：US373806
申请日：1995-01-17
申请人： Raj D. Patel , Michael A. Hopper , Paul J. Gerroir , Grazyna E. Kmiecik-Lawrynowicz
发明人： Raj D. Patel , Michael A. Hopper , Paul J. Gerroir , Grazyna E. Kmiecik-Lawrynowicz
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/08706 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/09733 , G03G9/0975
摘要： A process for the preparation of toner compositions consisting essentially of(i) preparing a pigment dispersion, which dispersion is comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant, and a nonionic surfactant;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(iv) subsequently adding further anionic or nonionic surfactant solution to minimize further growth in the coalescence (v); and(v) heating said bound aggregates above about the Tg of the resin and wherein said heating is from a temperature of about 103.degree. to about 120.degree. C., and wherein said toner compositions are spherical in shape.
摘要翻译：一种制备调色剂组合物的方法，其基本上由（i）制备颜料分散体组成，该分散体由颜料，离子表面活性剂和任选的电荷控制剂组成; （ii）用由树脂，具有与所述离子表面活性剂相反的电荷极性的反离子表面活性剂和非离子表面活性剂组成的胶乳或乳液共混物剪切所述颜料分散体; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （iv）随后加入其它阴离子或非离子表面活性剂溶液以最小化聚结中的进一步生长（v）; 和（v）在所述树脂的Tg附近加热所述结合的聚集体，并且其中所述加热温度为约103℃至约120℃，并且其中所述调色剂组合物的形状为球形。

3. 发明授权

US06808851B2 Emulsion aggregation toner containing a mixture of waxes incorporating an improved process to prevent wax protrusions and coarse particles 有权
标题翻译：含有蜡的混合物的乳液聚集调色剂包括改进的方法以防止蜡突起和粗颗粒
公开(公告)号：US06808851B2
公开(公告)日：2004-10-26
申请号：US10248393
申请日：2003-01-15
申请人： Joseph A. Bartel , Patricia A. Burns , Raj D. Patel , Enno E. Agur , Danielle C. Boils , Edward G. Zwartz , Paul J. Gerroir , Maria N. V. McDougall
发明人： Joseph A. Bartel , Patricia A. Burns , Raj D. Patel , Enno E. Agur , Danielle C. Boils , Edward G. Zwartz , Paul J. Gerroir , Maria N. V. McDougall
IPC分类号： G03G9083
CPC分类号： G03G9/0804 , C08J3/215 , G03G9/0815
摘要： A process for the preparation of emulsion aggregation toner particles with high pigment loading having a reduced number of wax protrusions on the surface of the toner particles and fewer coarse toner particles. The process includes the introduction of a wax having a molecular weight between about 500 and 2,500, or a blend of waxes having different a molecular weight between 500 and 2,500.
摘要翻译：一种制备具有高颜料负载的乳液聚集调色剂颗粒的方法，其中调色剂颗粒表面上的蜡突起数量减少，较少的粗调色剂颗粒。该方法包括引入分子量为约500-2,500的蜡，或分子量不同于500至2500之间的蜡的共混物。

4. 发明授权

US08737904B2 Delivery apparatus 有权
标题翻译：送货装置
公开(公告)号：US08737904B2
公开(公告)日：2014-05-27
申请号：US13354022
申请日：2012-01-19
申请人： Yu Liu , Sarah J. Vella , Richard A. Klenkler , Gregory M. McGuire , Nan-Xing Hu , Vladislav Skorokhod , Paul J. Gerroir
发明人： Yu Liu , Sarah J. Vella , Richard A. Klenkler , Gregory M. McGuire , Nan-Xing Hu , Vladislav Skorokhod , Paul J. Gerroir
IPC分类号： G03G15/00
CPC分类号： G03G21/0094
摘要： There is described a delivery member for use in an image forming apparatus. The delivery member includes a cylindrical support member and an outer layer. The outer layer comprises an outer surface. The outer surface comprises a first surface section and a second surface section. The first surface section comprises an elastomeric matrix having a functional material dispersed therein and the second surface section comprises a cleaning material.
摘要翻译：描述了用于图像形成装置中的传送构件。输送构件包括圆柱形支撑构件和外层。外层包括外表面。外表面包括第一表面部分和第二表面部分。第一表面部分包括具有分散在其中的功能材料的弹性体基体，并且第二表面部分包括清洁材料。

5. 发明申请

US20120145947A1 PYROPHORIC IRON NANOPARTICLES AND CONTINUOUS PROCESSES FOR PRODUCTION THEREOF 有权
标题翻译： PYROPHORIC IRON NANOPARTICLES及其连续生产工艺
公开(公告)号：US20120145947A1
公开(公告)日：2012-06-14
申请号：US12962961
申请日：2010-12-08
申请人： Kimberly D. Nosella , Santiago Faucher , Ke Zhou , Paul J. Gerroir , Richard P.N. Veregin , Karen A. Moffat
发明人： Kimberly D. Nosella , Santiago Faucher , Ke Zhou , Paul J. Gerroir , Richard P.N. Veregin , Karen A. Moffat
IPC分类号： C09K5/00 , B82Y30/00
CPC分类号： B82Y30/00
摘要： Pyrophoric nanoparticles and methods of producing the same are provided herein. An exemplary method of producing pyrophoric nanoparticles can include providing a first aqueous solution comprising at least one metal salt and an aliphatic polyether; providing a second solution comprising a metal hydride reducing agent; continuously combining the first and second solutions to produce nanoparticles in a liquid phase; separating the nanoparticles from the liquid phase; and drying the nanoparticles to form pyrophoric nanoparticles. The pyrophoric nanoparticles can have a diameter ranging from about 1 nm to about 50 nm.
摘要翻译：本发明提供发火纳米颗粒及其制备方法。产生自发性纳米颗粒的示例性方法可以包括提供包含至少一种金属盐和脂族聚醚的第一水溶液; 提供包含金属氢化物还原剂的第二溶液; 连续地组合第一和第二溶液以在液相中产生纳米颗粒; 将纳米颗粒与液相分离; 并干燥纳米颗粒以形成自发纳米颗粒。自发纳米颗粒可具有约1nm至约50nm的直径。

6. 发明授权

US07985523B2 Toners containing polyhedral oligomeric silsesquioxanes 有权
标题翻译：含多面体低聚倍半硅氧烷的调色剂
公开(公告)号：US07985523B2
公开(公告)日：2011-07-26
申请号：US12337688
申请日：2008-12-18
申请人： Ke Zhou , Maria N V. McDougall , Yu Qi , Jordan Wosnick , Karen A. Moffat , Paul J. Gerroir , Richard P N. Veregin
发明人： Ke Zhou , Maria N V. McDougall , Yu Qi , Jordan Wosnick , Karen A. Moffat , Paul J. Gerroir , Richard P N. Veregin
IPC分类号： G03G9/087
CPC分类号： G03G9/08755 , G03G9/0804 , G03G9/0819 , G03G9/08708 , G03G9/08773 , G03G9/08786 , G03G9/08791 , G03G9/08795 , G03G9/08797 , G03G9/093
摘要： Disclosed is a toner composition comprising toner particles which comprise (a) a resin having chemically bonded thereto a polyhedral oligomeric silsesquioxane, (b) and an optional colorant.
摘要翻译：公开了包含调色剂颗粒的调色剂组合物，其包含（a）化学键合多面体低聚倍半硅氧烷的树脂，（b）和任选的着色剂。

7. 发明授权

US07723004B2 Ultra low melt toners comprised of crystalline resins 失效
标题翻译：由结晶树脂组成的超低熔体调色剂
公开(公告)号：US07723004B2
公开(公告)日：2010-05-25
申请号：US12353863
申请日：2009-01-14
申请人： Guerino G. Sacripante , Ke Zhou , Michael S. Hawkins , Kimberly D. Nosella , Edward G. Zwartz , Nicoleta D. Mihai , Valerie M. Farrugia , Stephan V. Drappel , Paul J. Gerroir
发明人： Guerino G. Sacripante , Ke Zhou , Michael S. Hawkins , Kimberly D. Nosella , Edward G. Zwartz , Nicoleta D. Mihai , Valerie M. Farrugia , Stephan V. Drappel , Paul J. Gerroir
IPC分类号： G03G9/087
CPC分类号： G03G9/08755 , G03G9/081 , G03G9/08791 , G03G9/08795 , G03G9/08797
摘要： A toner having an amorphous resin, a crystalline resin, and a colorant, wherein the crystalline resin has a melting temperature of at least 70° C. and a recrystallization point of at least 47° C. exhibits improved document offset properties and improved heat cohesion. Annealing the toner further improves the heat cohesion and morphology of the toner.
摘要翻译：具有无定形树脂，结晶性树脂和着色剂的调色剂，其中结晶性树脂的熔融温度为70℃以上，再结晶点为47℃以上，表现出改善的文件偏移性和改善的热粘合性。使调色剂退火进一步提高了调色剂的热粘合性和形态。

8. 发明申请

US20090305159A1 TONER COMPOSITIONS 有权
标题翻译：调色剂组合物
公开(公告)号：US20090305159A1
公开(公告)日：2009-12-10
申请号：US12134494
申请日：2008-06-06
申请人： Ke Zhou , Maria N.V. McDougall , Edward G. Zwartz , Karen Ann Moffat , Paul J. Gerroir
发明人： Ke Zhou , Maria N.V. McDougall , Edward G. Zwartz , Karen Ann Moffat , Paul J. Gerroir
IPC分类号： G03G9/08
CPC分类号： G03G9/0823 , G03G9/0819 , G03G9/08704 , G03G9/08708 , G03G9/08711 , G03G9/08724 , G03G9/08755 , G03G9/08766 , G03G9/08768 , G03G9/08793 , G03G9/08795 , G03G9/08797 , G03G9/09328 , G03G9/09364 , G03G9/09371
摘要： Toner particles are provided which may, in embodiments, include a core possessing at least one polyester resin in combination with a colorant, optional wax, and optional other additives, and a shell over the core including a high molecular weight amorphous polyester resin. The high molecular weight amorphous polyester resin in the shell may prevent any crystalline polyester resin in the core from migrating to the toner surface.
摘要翻译：提供调色剂颗粒，在实施方案中可以包括具有至少一种聚酯树脂的核心，其与着色剂，任选的蜡和任选的其它添加剂组合，以及包含高分子量无定形聚酯树脂的核上的壳。壳中的高分子量无定形聚酯树脂可以防止芯中的任何结晶聚酯树脂迁移到调色剂表面。

9. 发明授权

US07563318B1 Method of making nanoscale particles of AZO pigments in a microreactor or micromixer 有权
标题翻译：在微反应器或微混合器中制备AZO颜料的纳米级颗粒的方法
公开(公告)号：US07563318B1
公开(公告)日：2009-07-21
申请号：US12166949
申请日：2008-07-02
申请人： Santiago Faucher , Rina Carlini , Emily L. Moore , Christine M. Thompson , Sandra J. Gardner , Paul J. Gerroir , C. Geoffrey Allen
发明人： Santiago Faucher , Rina Carlini , Emily L. Moore , Christine M. Thompson , Sandra J. Gardner , Paul J. Gerroir , C. Geoffrey Allen
IPC分类号： C09B63/00 , C09B67/20 , C09B41/00
CPC分类号： C09B63/005 , B01F13/0059 , B82Y30/00 , C09B67/0005 , C09B67/0091 , C09B67/0096 , C09D17/003
摘要： A process for preparing nanoscale azo pigment particles includes providing an organic pigment precursor that contains at least one functional moiety, providing a sterically bulky stabilizer compound that contains at least one functional group, and carrying out a chemical reaction to form a pigment composition in a microreactor or micromixer, whereby the functional moiety found on the pigment precursor is incorporated within the pigment and non-covalently associated with the functional group of the stabilizer, so as to allow the formation of nanoscale-sized pigment particles and the production of such in a microreactor under laminar or turbulent flow conditions without clogging.
摘要翻译：制备纳米级偶氮颜料颗粒的方法包括提供含有至少一个官能部分的有机颜料前体，提供含有至少一个官能团的空间庞大稳定剂化合物，并在微反应器中进行化学反应以形成颜料组合物或微混合器，由此在颜料前体上发现的官能部分被并入颜料中并且与稳定剂的官能团非共价缔合，从而允许形成纳米级颜料颗粒并在微反应器中生产在层流或湍流条件下无堵塞。

10. 发明申请

US20080193869A1 ULTRA LOW MELT EMULSION AGGREGATION TONERS HAVING A CHARGE CONTROL AGENT 有权
标题翻译：具有充电控制剂的超低浓度乳胶聚集体
公开(公告)号：US20080193869A1
公开(公告)日：2008-08-14
申请号：US11672723
申请日：2007-02-08
申请人： Daryl W. Vanbesien , Cuong Vong , Paul J. Gerroir , Richard P.N. Veregin , Karen A. Moffat , Peter J.G. Rehbein
发明人： Daryl W. Vanbesien , Cuong Vong , Paul J. Gerroir , Richard P.N. Veregin , Karen A. Moffat , Peter J.G. Rehbein
IPC分类号： G03G9/087 , G03G9/097
CPC分类号： G03G9/0821 , G03G9/0804 , G03G9/0823 , G03G9/08748 , G03G9/08795 , G03G9/08797 , G03G9/09733
摘要： Toner compositions comprising toner particles including an amorphous resin, a crystalline resin and a charge control agent. The toner compositions having the charge control agent exhibit improved charge performance in the C-zone and the A-zone, and improved RH sensitivity.
摘要翻译：包含调色剂颗粒的调色剂组合物包括无定形树脂，结晶树脂和电荷控制剂。具有电荷控制剂的调色剂组合物在C区和A区具有改进的充电性能，并提高了RH灵敏度。

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