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1. 发明授权

US3875087A Multicellular polymers 失效
标题翻译：多孔聚合物
公开(公告)号：US3875087A
公开(公告)日：1975-04-01
申请号：US46324974
申请日：1974-04-23
申请人： RHONE POULENC SA
发明人： GRUFFAZ MAX , ROLLET BERNARD
IPC分类号： C08G73/00 , C08G73/02 , C08G73/12 , C08J9/02 , C08G53/08
CPC分类号： C08J9/02 , C08G73/12 , C08J2379/00 , C08J2379/08
摘要： Multicellular polymers having excellent chemical inertness and heat resistance are produced by heating at a temperature from 100* to 300*C, maleic anhydride and a polyaldimine of the general formula

2. 发明授权

US3903036A Polyamide-imide solutions 失效
标题翻译：聚酰胺酰亚胺溶液
公开(公告)号：US3903036A
公开(公告)日：1975-09-02
申请号：US45155774
申请日：1974-03-15
申请人： RHONE POULENC SA
发明人： GRUFFAZ MAX , ROLLET BERNARD
IPC分类号： C08L79/08 , C08G51/44
CPC分类号： C08K5/05 , C08L79/08
摘要： A process is disclosed for stabilising the viscosity of a solution of a polyamide-imide obtained from trimellitic anhydride and from an aromatic diisocyanate and a solvent which is at least partly 2-N-methylpyrrolidone, which comprises adding thereto 0.1 to 5% by weight of an alcohol of the formula: ROH in which R represents an aliphatic, cycloaliphatic or arylaliphatic radical containing 2 to 9 carbon atoms.
摘要翻译：公开了一种稳定由偏苯三酸酐和芳族二异氰酸酯得到的聚酰胺酰亚胺溶液和至少部分为2-N-甲基吡咯烷酮的溶剂的粘度的方法，该方法包括向其中加入0.1至5重量％下式的醇：ROH，其中R表示含有2至9个碳原子的脂族，脂环族或芳基脂族基团。

3. 发明授权

US3929687A Mullticellular polymers made from the reaction product of maleic anhydride with a polyimine 失效
标题翻译：由马来酸酐与聚亚胺的反应产物制成的纤维状聚合物
公开(公告)号：US3929687A
公开(公告)日：1975-12-30
申请号：US46324874
申请日：1974-04-23
申请人： RHONE POULENC SA
发明人： GRUFFAZ MAX , ROLLET BERNARD
IPC分类号： C08J9/02 , C08J9/06 , C08L63/00 , C08L79/08 , C08J9/00
CPC分类号： C08L79/085 , C08J9/02 , C08J9/06 , C08L63/00 , Y10S525/929 , C08L87/00 , C08L2666/20
摘要： Multicellular materials which are lightweight, heat-resistant and flame-proof are produced by a process which comprises curing a liquid polymer in the presence of a reaction product of maleic anhydride with a polyimine of the general formula
in which n represents a number at least equal to 2, G represents a monovalent organic radical containing less than 35 carbon atoms, R is as defined under G or represents a hydrogen atom, or G and R together form a divalent hydrocarbon radical, and A represents an organic radical of valency n containing 2 to 50 carbon atoms.
摘要翻译：通过包括在马来酸酐与通式A（-N = CG）n的聚亚胺的反应产物（-N = CG）n的存在下固化液态聚合物的方法制备轻质，耐热和阻燃的多细胞材料 I）| R，其中n表示至少等于2的数，G表示含有少于35个碳原子的一价有机基团，R如G中所定义或表示氢原子，或G和R一起形成二价烃自由基，A表示含有2至50个碳原子的价数n的有机基团。

4. 发明授权

US3875113A Thermosetting compositions derived from an epoxy resin, a polyamine and an imide 失效
标题翻译：从环氧树脂，聚氨基甲酸乙酯和三氯乙烯衍生的热固化组合物
公开(公告)号：US3875113A
公开(公告)日：1975-04-01
申请号：US40993573
申请日：1973-10-26
申请人： RHONE POULENC SA
发明人： LEFEBVRE GERARD , ROLLET BERNARD
IPC分类号： C08G59/00 , C08G59/40 , C08G59/56 , C08G73/00 , C08G73/12 , C08G30/14
CPC分类号： C08G59/56 , C08G59/4042 , Y10T428/31511
摘要： IN WHICH THE SYMBOL A represents a divalent hydrocarbon radical containing at least two carbon atoms, the bis-maleimide ( Beta ) being present in an amount up to about 90 percent by weight based on the weight of ( Alpha ) and ( Beta ). These compositions are useful for producing moulded objects and laminates.

OR A MIXTURE OF SUCH COMPOUNDS; OR A COMPOUND ( Alpha ) AND A BIS-MALEIMIDE ( Beta ) OF THE FORMULA:

The invention provides heat-resistant compositions which comprise an epoxy resin, a polyamine containing at least two primary amine groups and also either a compound ( Alpha ) of the formula:

5. 发明授权

US3597414A Process for the reduction of nitrobenzene-3,4-dicarboxylic acid to azo and azoxy compounds 失效
标题翻译：将硝基苯-3,4-二羧酸还原成AZO和AZOXY化合物的方法
公开(公告)号：US3597414A
公开(公告)日：1971-08-03
申请号：US3597414D
申请日：1967-10-30
申请人： RHONE POULENC SA
发明人： GRUFFAZ MAX , ROLLET BERNARD
IPC分类号： C07C20060101 , C07D27/00
CPC分类号： C09B56/04
摘要： AZOBENZENE-3,3'',4,4''-TETRACARBOXYLIC ACID AND AZOXYBENZENE-3,3'',4,4''-TETRACARBOXYLIC ACID ARE MADE BY REDUCING NITROBENZENE-3,4-DICARBOXYLIC ACID WITH ALUMINUM IN AN AQUEOUS ALKALI METAL HYDROXIDE SOLUTION.

6. 发明专利

AU6820474A POLYMERS 未知
公开(公告)号：AU6820474A
公开(公告)日：1975-10-23
申请号：AU6820474
申请日：1974-04-23
申请人： RHONE POULENC SA
发明人： GRUFFAZ MAX , ROLLET BERNARD
IPC分类号： C08G73/00 , C08G73/02 , C08G73/12 , C08J9/02 , C08G33/02
摘要： 1407939 Polymers from polyaldimines and foams thereof RHONE-POULENC SA 25 April 1974 [26 April 1973] 18167/74 Headings C3R and C3C A process for preparing a multicellular polymer comprises heating, at a temperature from 100 to 300 C., maleic anhydride and a polyaldimine of the general formula in which G represents a monovalent organic radical which contains less than 35 carbon atoms and at least one aromatic or heterocyclic ring in the α-position to the imine group in Formula (I), A represents an organic radical of valency n which contains less than 50 carbon atoms and at least one aromatic or heterocyclic ring in the α position to the imine group in Formula (I), and n represents a number at least equal to 2. A pre-polymer may be formed in a first step and further heated in a second step to obtain the multicellular polymer. In Examples pre-polymers are obtained by heating maleic anhydride with bis - (4 - benzylidene aminophenyl)-methane, with bis-(4-salicylideneaminophenyl)-methane and with 2,6-his- (salicylideneamino)-pyridine, the prepolymers being heated further to obtain multicellular polymers, and a foam is obtained in one step by heating maleic anhydride with bis - (4 - furfurylideneaminophenyl)methane; in some instances azodicarbonamide is added as a pore-forming agent, a polysiloxane is added as a surface-active agent, boric anhydride is added as a heat-stabilizing agent and dihydroxyazobenzene is added as polymerization inhibitor.

7. 发明专利

AU6192573A THERMOSETTING COMPOSITIONS 未知
公开(公告)号：AU6192573A
公开(公告)日：1975-05-01
申请号：AU6192573
申请日：1973-10-29
申请人： RHONE POULENC SA
发明人： LEFEBVRE GERALD , ROLLET BERNARD
IPC分类号： C08G59/00 , C08G59/40 , C08G59/56 , C08G73/00 , C08G73/12 , C08G30/14
摘要： 1412224 Curing epoxy resins; polyimides RHONE-POULENC SA 30 Oct 1973 [31 Oct 1972] 50434/73 Headings C3B and C3R A composition which cures to a heat resistant solid comprises: (I) an epoxy resin, (II) a polyamine containing at least two primary amine groups either a compound or a mixture of III and IV. The composition may optionally contain a bis-maleimide in which case V may comprise up to 90% of the combined weight of V plus III and/or IV. The ratio of the number of maleimide groups introduced by III and/or IV and V when present to the number of NH 2 groups introduced by II may be 0.5-20. The ratio of the weight of III and/or IV and V when present to the weight of I may be 0.1 to 10. I may be an epoxy novolac resin or a tetraglycidyl ether of a tetrahydric tetranuclear phenol. II may be bis-(4-aminomethyl)methane. An example of III is 4-maleimido - 4 1 - acetoxy - succinimido - diphenylmethane. IV may be 1-maleimido-2-acetamidodiphenylmethane and V may be N,N 1 -4,4 1 -di. phenylmethane-bis-maleimide. The compositions may be cured by heating, e.g. for 24 hours at 200 C. followed by 24 hours at 250 C. Reference has been directed by the Comptroller to Specification 1,276,646.

8. 发明专利

DE2420424A1 未知
公开(公告)号：DE2420424A1
公开(公告)日：1974-11-14
申请号：DE2420424
申请日：1974-04-26
申请人： RHONE POULENC SA
发明人： GRUFFAZ MAX , ROLLET BERNARD
IPC分类号： C08G73/00 , C08G73/02 , C08G73/12 , C08J9/02 , C08G33/02
摘要： 1407939 Polymers from polyaldimines and foams thereof RHONE-POULENC SA 25 April 1974 [26 April 1973] 18167/74 Headings C3R and C3C A process for preparing a multicellular polymer comprises heating, at a temperature from 100 to 300 C., maleic anhydride and a polyaldimine of the general formula in which G represents a monovalent organic radical which contains less than 35 carbon atoms and at least one aromatic or heterocyclic ring in the α-position to the imine group in Formula (I), A represents an organic radical of valency n which contains less than 50 carbon atoms and at least one aromatic or heterocyclic ring in the α position to the imine group in Formula (I), and n represents a number at least equal to 2. A pre-polymer may be formed in a first step and further heated in a second step to obtain the multicellular polymer. In Examples pre-polymers are obtained by heating maleic anhydride with bis - (4 - benzylidene aminophenyl)-methane, with bis-(4-salicylideneaminophenyl)-methane and with 2,6-his- (salicylideneamino)-pyridine, the prepolymers being heated further to obtain multicellular polymers, and a foam is obtained in one step by heating maleic anhydride with bis - (4 - furfurylideneaminophenyl)methane; in some instances azodicarbonamide is added as a pore-forming agent, a polysiloxane is added as a surface-active agent, boric anhydride is added as a heat-stabilizing agent and dihydroxyazobenzene is added as polymerization inhibitor.

9. 发明专利

CA720520A ELASTOMERES ET LEUR FABRICATION 未知
公开(公告)号：CA720520A
公开(公告)日：1965-10-26
申请号：CA720520D
申请人： RHONE POULENC SA
发明人： GRUFFAZ MAX , ROLLET BERNARD , PHELISSE JEAN-AUGUSTE

10. 发明专利

CA1052042A RESINES THERMOSTABLES 未知
公开(公告)号：CA1052042A
公开(公告)日：1979-04-03
申请号：CA205245
申请日：1974-07-18
申请人： RHONE POULENC SA
发明人： BALME MAURICE , GRUFFAZ MAX , ROLLET BERNARD
IPC分类号： C08G18/00 , C08G18/32 , C08G18/38 , C08G18/40 , C08G73/12 , C08G73/06 , C08L79/04
摘要： Polymère thermostables, caractérisés en ce qu'ils sont obtenus par réaction de : a) un maléimide de formule moyenne : (I) dans laquelle le symbole A représente un radical organique de valence n, renfermant jusqu'à 50 atomes de carbone, le symbole Y représente H, -CH3 ou Cl et n représente un nombre au moins égal à 1,5. b) un composé renfermant au moins un groupement -NH2c) un composé renfermant au moins un groupement -?R, la nature du composé aminé et du composé carbonylé étant telle que l'imine résultant de leur réaction ait pour formule moyenne: (II) dans laquelle m représente un nombre au moins égal à 1, le symbole B représente un atome d'hydrogène ou un radical organique de valence m, renfermant jusqu'à 50 atomes de carbone, le symbole G représente un radical organique monovalent (G1) renfermant jusqu'à 35 atomes de carbone ou un radical de formule -G'-CR=N-B1 dans laquelle le symbole G' représente un radical divalent renfermant jusqu'à 35 atomes de carbone et le symbole B1 représente l'un des radicaux monovalents pouvant être représentés par le symbole B, ou encore, lorsque m = 2, un radical de formule: -G'-CR=N-B2?N=CR-G'-CR=-N-B2)w .SIGMA. dans laquelle G' possède la signification donnée ci-avant, B2 représente l'un des radicaux divalents pouvant être représentés par le symbole B et les deux symboles 2 représentant les terminaisons de chaîne qui peuvent être toutes deux des radicaux de formule -N=CR-G'-CRO ou représenter l'une le radical -N=CR-G'-CRO et l'autre un groupement -NH2, le symbole R représente un atome d'hydrogène ou un radical organique monovalent renfermant jusqu'à 35 atomes de carbone, les symboles G1 et R pouvant représenter ensemble un radical divalent ; w représente un nombre compris entre 1 et 10, les quantités de réactifs mises en oeuvre étant telles qu'il y ait en présence au moins un groupement -?-R ainsi qu'au moins une et au plus dix doubles liaisons, de maléimide (I) par groupement -NH2 apporté par le composé aminé b).

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