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1. 发明申请

US20100184630A1 BREAKING THE RHEOLOGY OF A WELLBORE FLUID BY CREATING PHASE SEPARATION 审中-公开
标题翻译：通过创建相分离破坏井筒流体的流变学
公开(公告)号：US20100184630A1
公开(公告)日：2010-07-22
申请号：US12354931
申请日：2009-01-16
申请人： Philip F. Sullivan , Gary John Tustin , Mark Turner , Stephania Poulis Cruz
发明人： Philip F. Sullivan , Gary John Tustin , Mark Turner , Stephania Poulis Cruz
IPC分类号： C09K8/60 , C09K8/588
CPC分类号： C09K8/52 , C09K8/685 , C09K2208/08
摘要： Embodiments of this invention relate to compositions and methods of treating a subterranean formation penetrated by a well bore including introducing a Theological polymer into a subterranean formation, introducing a partitioning agent into a subterranean formation and forming a heterogeneous mixture comprising a dispersed Theological polymer-rich phase and a partitioning agent-rich phase, wherein the viscosity of the mixture is lower than the viscosity of the mixture when no partitioning agent is present. Embodiments of this invention relate to compositions and methods of treating a surface in contact with a wellbore and/or a subterranean formation penetrated by a well bore including forming a heterogeneous mixture comprising a dispersed Theological polymer-rich phase and a partitioning agent-rich phase at the surface of the subterranean formation, and introducing the mixture into a subterranean formation, wherein the viscosity of the mixture within the subterranean formation is lower than the viscosity of the mixture when no partitioning agent is present and wherein the viscosity of the mixture within the subterranean formation is lower than the viscosity of the mixture when the mixture is formed at the surface of the subterranean formation.
摘要翻译：本发明的实施方案涉及处理由井眼渗透的地下地层的组合物和方法，包括将神学聚合物引入地下地层，将分配剂引入地下地层并形成包含分散的神经聚合物丰富相的不均匀混合物和分配剂富集相，其中当不存在分配剂时，混合物的粘度低于混合物的粘度。本发明的实施方案涉及处理与井眼和/或穿透井眼的地层接触的表面的组合物和方法，包括形成包含分散的神经聚合物丰富相和富分配剂相的不均匀混合物地下地层的表面，并将混合物引入地下地层，其中当没有分配剂时，地层内的混合物的粘度低于混合物的粘度，并且其中地下混合物的粘度当在地层表面形成混合物时，其形成比混合物的粘度低。

2. 发明申请

US20130319670A1 METHODS FOR SERVICING SUBTERRANEAN WELLS 审中-公开
标题翻译：维修地下水井的方法
公开(公告)号：US20130319670A1
公开(公告)日：2013-12-05
申请号：US13484035
申请日：2012-05-30
申请人： Lijun Lin , Simon Gareth James , Philip F. Sullivan , Gary John Tustin , Richard D. Hutchins , Andrey Mirakyan
发明人： Lijun Lin , Simon Gareth James , Philip F. Sullivan , Gary John Tustin , Richard D. Hutchins , Andrey Mirakyan
IPC分类号： E21B43/22
CPC分类号： C09K8/42 , C09K8/5083 , C09K8/512 , C09K8/516 , E21B21/003
摘要： Process fluids comprising more than 1 wt % polyacrylamide and a non-metallic crosslinker may be used to control lost circulation in subterranean wells. The process fluid is placed into a subterranean lost-circulation zone and allowed to crosslink, thereby forming a gel barrier that limits further flow of process fluid into the zone. The non-metallic crosslinker may preferably comprise one or more polylactams. A pH-adjusting agent may also be incorporated into the process fluid.
摘要翻译：包含大于1重量％聚丙烯酰胺和非金属交联剂的工艺流体可用于控制地下井中的流失。将工艺流体放置在地下缺水循环区域中并使其交联，从而形成限制进一步流入该区域的凝胶屏障。非金属交联剂可优选包含一种或多种聚内酰胺。 pH调节剂也可以并入工艺流体中。

3. 发明申请

US20120138294A1 INTERPOLYMER CROSSLINKED GEL AND METHOD OF USING 审中-公开
标题翻译：内插式交联凝胶和使用方法
公开(公告)号：US20120138294A1
公开(公告)日：2012-06-07
申请号：US13301240
申请日：2011-11-21
申请人： Philip F. Sullivan , Rick D. Hutchins , Audrey Mirakyan , Gary John Tustin , Lijun Lin
发明人： Philip F. Sullivan , Rick D. Hutchins , Audrey Mirakyan , Gary John Tustin , Lijun Lin
IPC分类号： E21B43/00 , C09K8/588
CPC分类号： E21B43/16 , C09K8/52 , C09K8/685 , C09K8/882 , C09K8/887 , C09K2208/28 , C09K2208/30
摘要： Disclosed herein is a gel or a gel concentrate comprising, polyacrylamide crosslinked with a non-metallic crosslinker comprising a polylactam. A well treatment fluid comprising the gel or the gel concentrate, a method of making the gel or the gel concentrate, and a method of using the gel or the gel concentrate are also disclosed.
摘要翻译：本文公开了一种凝胶或凝胶浓缩物，其包含与包含聚内酰胺的非金属交联剂交联的聚丙烯酰胺。还公开了包含凝胶或凝胶浓缩物的良好处理流体，制备凝胶或凝胶浓缩物的方法，以及使用凝胶或凝胶浓缩物的方法。

4. 发明授权

US07703521B2 Polymeric microspheres as degradable fluid loss additives in oilfield applications 失效
标题翻译：聚合微球作为油田应用中的可降解流体损失添加剂
公开(公告)号：US07703521B2
公开(公告)日：2010-04-27
申请号：US12353810
申请日：2009-01-14
申请人： Philip F. Sullivan , Gary John Tustin , Don Williamson , Hemant K. Ladva
发明人： Philip F. Sullivan , Gary John Tustin , Don Williamson , Hemant K. Ladva
IPC分类号： E21B33/13 , E21B43/267
CPC分类号： C09K8/512 , C09K8/516 , C09K8/685 , C09K8/887
摘要： Methods and apparatus for forming a fluid for use within in a subterranean formation including crosslinking a polymer along the surface of microspheres in a water-in-water emulsion and introducing the microspheres into the subterranean formation. Methods and apparatus for forming a fluid for use within in a subterranean formation including crosslinking a polymer along the surface of microspheres in a water in water emulsion, isolating the microspheres from the emulsion, and introducing the microspheres into the subterranean formation. Methods and apparatus for forming a fluid to treat a subterranean formation including introducing a crosslinkable polymer, partitioning agent, and crosslinker into a solvent, crosslinking the crosslinkable polymer, isolating beads of the crosslinkable polymer from the partitioning agent, introducing the beads into a fluid for treating a subterranean formation.
摘要翻译：用于形成在地下地层内使用的流体的方法和装置，包括在水包油乳液中沿着微球表面交联聚合物，并将微球引入地下地层。用于形成在地层内使用的流体的方法和装置，包括在水包油乳液中沿着微球表面交联聚合物，从微乳液中分离出微球体，并将微球引入到地层中。用于形成用于处理地下地层的流体的方法和装置，包括将可交联聚合物，分配剂和交联剂引入溶剂中，交联可交联聚合物，将可交联聚合物的珠子与分配剂隔离，将珠粒引入用于处理地层。

5. 发明申请

US20120132422A1 INTERPOLYMER CROSSLINKED GEL AND METHOD OF USING 审中-公开
标题翻译：内插式交联凝胶和使用方法
公开(公告)号：US20120132422A1
公开(公告)日：2012-05-31
申请号：US13306561
申请日：2011-11-29
申请人： Andrey Mirakyan , Philip F. Sullivan , Rick D. Hutchins , Lijun Lin , Gary John Tustin , Bruno Drochon
发明人： Andrey Mirakyan , Philip F. Sullivan , Rick D. Hutchins , Lijun Lin , Gary John Tustin , Bruno Drochon
IPC分类号： E21B43/00 , C09K8/588
CPC分类号： E21B43/16 , C09K8/52 , C09K8/685 , C09K8/882 , C09K8/887 , C09K2208/28 , C09K2208/30
摘要： Disclosed herein is a gel comprising, polyacrylamide crosslinked with a non-metallic crosslinker, the non-metallic crosslinker comprising a polyamine. A method of making the gel and a method of using the gel are also disclosed.
摘要翻译：本文公开了一种凝胶，其包含用非金属交联剂交联的聚丙烯酰胺，所述非金属交联剂包含多胺。还公开了制备凝胶的方法和使用该凝胶的方法。

6. 发明授权

US08044000B2 Polymer delivery in well treatment applications 有权
标题翻译：聚合物输送在井处理应用中
公开(公告)号：US08044000B2
公开(公告)日：2011-10-25
申请号：US12166774
申请日：2008-07-02
申请人： Philip F. Sullivan , Gary John Tustin , Yenny Christanti , Gregory Kubala , Bruno Drochon , Yiyan Chen , Marie Noelle Dessinges , Paul R. Howard
发明人： Philip F. Sullivan , Gary John Tustin , Yenny Christanti , Gregory Kubala , Bruno Drochon , Yiyan Chen , Marie Noelle Dessinges , Paul R. Howard
IPC分类号： C09K8/90
CPC分类号： C09K8/035 , B01F3/1214 , B01F3/2276 , B01F15/06 , B01F2003/1285 , B01F2015/062 , B01F2215/0081 , C09K8/5756 , C09K8/68 , C09K8/685 , C09K8/70 , C09K8/887 , C09K8/90
摘要： This invention relates to compositions and methods for treating subterranean formations, in particular, oilfield stimulation compositions and methods using water-in-water polymer emulsions to uniformly dissolve a rheologically active polymer, such as a thickener or friction reducer, in the treatment fluid. The emulsions have a low viscosity and are easily pumped for mixing into a treatment fluid, where upon dilution with an aqueous medium, the polymer is easily hydrated without forming fish-eyes. The partitioning agent in the water-in-water emulsion does not generally affect the rheology of the treatment fluid. The invention also relates to further processing of the emulsion by wet grinding, high shear mixing and/or heating to enhance the hydration rate in the preparation of the well treatment fluid.
摘要翻译：本发明涉及用于处理地下地层的组合物和方法，特别是油田刺激组合物和使用水包水聚合物乳液在处理液中均匀溶解流变学活性聚合物如增稠剂或摩擦减小剂的方法。乳液具有低粘度并且容易地泵入以混合到处理流体中，其中当用水性介质稀释时，聚合物容易水合而不形成鱼眼。水包油乳液中的分配剂通常不影响处理液的流变性。本发明还涉及通过湿法研磨，高剪切混合和/或加热进一步处理乳液，以提高在井处理流体的制备中的水化速率。

7. 发明申请

US20090205829A1 Polymeric Microspheres as Degradable Fluid Loss Additives in Oilfield Applications 失效
标题翻译：聚合物微球作为油田应用中可降解的流体损失添加剂
公开(公告)号：US20090205829A1
公开(公告)日：2009-08-20
申请号：US12033630
申请日：2008-02-19
申请人： Philip F. Sullivan , Gary John Tustin , Bruno Drochon , Marie Noelle Dessinges , Gregory Kubala , Christelle Vatry
发明人： Philip F. Sullivan , Gary John Tustin , Bruno Drochon , Marie Noelle Dessinges , Gregory Kubala , Christelle Vatry
IPC分类号： E21B33/13
CPC分类号： C09K8/516 , C09K8/426
摘要： A method of plugging a fracture in a subterranean formation which includes placing into the fracture a composition comprising microspheres or microbeads, wherein the microspheres are created by surface crosslinking of droplets in a water-in-water emulsion. Such microspheres may form a filter cake in the formation. The microspheres may include a chemical agent to be released when the microspheres dissolve.
摘要翻译：一种在地层中堵塞裂缝的方法，其包括将包含微球或微珠的组合物放入裂缝中，其中微球通过水包油乳液中的液滴的表面交联而产生。这种微球可以在地层中形成滤饼。微球可以包括当微球溶解时要释放的化学试剂。

8. 发明授权

US09334438B2 Polymer delivery in well treatment applications 有权
标题翻译：聚合物输送在井处理应用中
公开(公告)号：US09334438B2
公开(公告)日：2016-05-10
申请号：US13225823
申请日：2011-09-06
申请人： Philip F. Sullivan , Gary John Tustin , Yenny Christanti , Gregory Kubala , Bruno Drochon , Yiyan Chen , Marie Noelle Dessinges , Paul R. Howard
发明人： Philip F. Sullivan , Gary John Tustin , Yenny Christanti , Gregory Kubala , Bruno Drochon , Yiyan Chen , Marie Noelle Dessinges , Paul R. Howard
IPC分类号： C09K8/68 , C09K8/70 , C09K8/90
CPC分类号： C09K8/035 , B01F3/1214 , B01F3/2276 , B01F15/06 , B01F2003/1285 , B01F2015/062 , B01F2215/0081 , C09K8/5756 , C09K8/68 , C09K8/685 , C09K8/70 , C09K8/887 , C09K8/90
摘要： This invention relates to compositions and methods for treating subterranean formations, in particular, oilfield stimulation compositions and methods using water-in-water polymer emulsions to uniformly dissolve a rheologically active polymer, such as a thickener or friction reducer, in the treatment fluid. The emulsions have a low viscosity and are easily pumped for mixing into a treatment fluid, where upon dilution with an aqueous medium, the polymer is easily hydrated without forming fish-eyes. The partitioning agent in the water-in-water emulsion does not generally affect the rheology of the treatment fluid. The invention also relates to further processing of the emulsion by wet grinding, high shear mixing and/or heating to enhance the hydration rate in the preparation of the well treatment fluid.
摘要翻译：本发明涉及用于处理地下地层的组合物和方法，特别是油田刺激组合物和使用水包水聚合物乳液在处理液中均匀溶解流变学活性聚合物如增稠剂或摩擦减小剂的方法。乳液具有低粘度并且容易地泵入以混合到处理流体中，其中当用水性介质稀释时，聚合物容易水合而不形成鱼眼。水包油乳液中的分配剂通常不影响处理液的流变性。本发明还涉及通过湿法研磨，高剪切混合和/或加热进一步处理乳液，以提高在井处理流体的制备中的水化速率。

9. 发明申请

US20100175881A1 Using A Biphasic Solution As A Recyclable Coiled Tubing Cleanout Fluid 有权
标题翻译：使用双相溶液作为可回收的卷管清洗液
公开(公告)号：US20100175881A1
公开(公告)日：2010-07-15
申请号：US12354500
申请日：2009-01-15
申请人： Philip F. Sullivan , Gary John Tustin , Yiyan Chen , Lijun Lin
发明人： Philip F. Sullivan , Gary John Tustin , Yiyan Chen , Lijun Lin
IPC分类号： E21B43/00 , E21B36/00
CPC分类号： C09K8/52 , C09K8/536 , C09K2208/28 , Y10S507/904
摘要： Methods and apparatus for forming a fluid for use within in a subterranean formation including combining a partitioning agent and viscosifying polymer into a fluid, introducing the fluid into the subterranean formation, and recovering at least a portion of the fluid at a uppermost surface of the subterranean formation. Methods and apparatus of forming a fluid for use within in a subterranean formation including combining a partitioning agent and viscosifying polymer into a fluid, introducing the fluid into the subterranean formation at a temperature of about 45° C. or higher, and recovering at least a portion of the fluid at a uppermost surface of the subterranean formation at a temperature of about 45° C. or lower.
摘要翻译：用于形成在地层内使用的流体的方法和装置，包括将分配剂和增粘聚合物组合成流体，将流体引入地下地层，以及在地下最上表面处回收至少一部分流体形成。形成在地层内使用的流体的方法和装置，包括将分配剂和增粘聚合物混合到流体中，在大约45℃或更高的温度下将流体引入地层，并回收至少一种部分流体在地下层的最上表面处于约45℃或更低的温度。

10. 发明申请

US20090133868A1 Aqueous Two-Phase Emulsion Gel Systems for Zone Isolation 有权
标题翻译：用于区域隔离的水性两相乳液凝胶体系
公开(公告)号：US20090133868A1
公开(公告)日：2009-05-28
申请号：US11944681
申请日：2007-11-26
申请人： Philip F. Sullivan , Gary John Tustin , Yenny Christanti , Gregory Kubala , Bruno Drochon , Trevor LLoyd Hughes
发明人： Philip F. Sullivan , Gary John Tustin , Yenny Christanti , Gregory Kubala , Bruno Drochon , Trevor LLoyd Hughes
IPC分类号： E21B33/124
CPC分类号： C09K8/514 , C09K8/501 , C09K8/508 , C09K8/52 , C09K8/5751 , C09K8/588 , C09K8/68 , C09K8/88
摘要： A low viscosity wellbore polymer fluid gelling system comprising an aqueous medium and a water-in-water emulsion comprising a plurality of polymers or oligomers, including at least one removable polymer or oligomer, and at least one gelling polymer or oligomer, wherein said fluid has a low viscosity when injected, and the gelling polymer forms a gel downhole which has a storage modulus of at least about 60 Pa after the removable polymer is removed from the fluid. The invention also provides a method of isolating at least one zone of a subterranean formation penetrated by a wellbore, including the steps of preparing a water-in-water emulsion comprising a plurality of polymers or oligomers including at least one removable polymer or oligomer, and at least one gellable polymer or oligomer; combining the water-in-water emulsion with an aqueous medium to prepare a low viscosity polymer fluid; introducing the fluid into a zone in the formation, removing the at least one removable polymer or oligomer, and allowing a remaining gellable oligomer, polymer or polymers to form a gel, isolating the zone from at least one other zone in the formation.
摘要翻译：一种低粘度井筒聚合物流体胶凝体系，其包含含水介质和包含多种聚合物或低聚物（包括至少一种可除去的聚合物或低聚物）和至少一种胶凝聚合物或低聚物的水包油乳液，其中所述流体具有注射时具有低粘度，并且胶凝聚合物形成凝胶井下，其中可除去的聚合物从流体中除去后具有至少约60Pa的储能模量。本发明还提供了一种分离由井筒渗透的地层的至少一个区域的方法，包括以下步骤：制备包含多个聚合物或低聚物的水包油乳液，所述聚合物或低聚物包括至少一种可除去的聚合物或低聚物，以及至少一种可凝胶聚合物或低聚物; 将水包油乳液与水性介质结合以制备低粘度聚合物流体; 将流体引入地层中的区域，除去至少一种可除去的聚合物或低聚物，并允许剩余的可凝胶低聚物，聚合物或聚合物形成凝胶，将该区域与地层中的至少一个其它区域隔离。

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