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1. 发明授权

US06497771B1 Aqueous solution and method for phosphatizing metallic surfaces 失效
标题翻译：水溶液和金属表面磷化的方法
公开(公告)号：US06497771B1
公开(公告)日：2002-12-24
申请号：US09622975
申请日：2001-01-09
申请人： Peter Schubach , Joachim Heitbaum , Thomas Kolberg , Margit Fleischhacker-Jeworrek , Peter Jorns , Michael Deemer , Ralf Stickler , Jurgen Specht , Michael Lenhard
发明人： Peter Schubach , Joachim Heitbaum , Thomas Kolberg , Margit Fleischhacker-Jeworrek , Peter Jorns , Michael Deemer , Ralf Stickler , Jurgen Specht , Michael Lenhard
IPC分类号： C23C2207
CPC分类号： C23C22/182 , C23C22/12 , C23C22/13 , C23C22/365
摘要： An aqueous solution contains phosphate for producing layers of phosphate on metal surfaces selected from the group consisting of iron, steel, zinc, zinc alloys, aluminum and aluminum alloys. The solution contains 0.3 to 5 g Zn2+/1, 0.1 to 2 g nitroguanidine/1 and 0.05 to 0.5 g hydroxylamine/l, with an S-value amounting to 0.03 to 0.3 and the ratio of the weight of Zn2+ to P2O5=1:5 to 1.30.
摘要翻译：水溶液含有磷酸盐，用于在选自铁，钢，锌，锌合金，铝和铝合金的金属表面上生产磷酸盐层。该溶液含有0.3-5g Zn2 + / l，0.1-2g硝基胍/ 1和0.05-0.5g羟胺/ l，S值为0.03-0.3，Zn2 +与P2O5的重量比= 1： 5至1.30。

2. 发明授权

US4559087A Process for phosphating metals 失效
标题翻译：磷化金属的工艺
公开(公告)号：US4559087A
公开(公告)日：1985-12-17
申请号：US600587
申请日：1984-04-17
申请人： Peter Jorns , Norbert Meyer , Werner Rausch , Josef Rothkegel , Gunther Luckhardt , Gudrun Volling
发明人： Peter Jorns , Norbert Meyer , Werner Rausch , Josef Rothkegel , Gunther Luckhardt , Gudrun Volling
IPC分类号： C23C22/73 , C23F7/10
CPC分类号： C23C22/73
摘要： In a process for phosphating composite metals containing steel and zinc surfaces using phosphating solutions based on zinc phosphate by the dipping process, in order to achieve satisfactory formation of the phosphate layer, the composite metals are subjected to preliminary dipping for a maximum of 30 seconds in a phosphating solution based on zinc phosphate in order to initiate the formation of the phosphate layer, and are then conveyed to the main dip-phosphating zone.It is advantageous to spray the composite metals with a phosphating solution based on zinc phosphate while they are being conveyed from the preliminary to the main dip-phosphating zone, and it is advisable to limit the duration of the conveying and thus of the spraying treatment to a maximum of 30 seconds.
摘要翻译：在使用通过浸渍法的磷酸锌的磷化液对含有钢和锌的表面进行磷酸化的复合金属的方法中，为了达到令人满意的磷酸盐层的形成，复合金属经过预浸渍最多30秒钟为了开始磷酸盐层的形成，以磷酸锌为基础的磷化液，然后被输送到主浸渍磷化区。在将磷酸盐从磷酸盐初步输送到主浸渍磷酸盐区时，用磷酸盐磷酸盐溶液喷雾复合金属是有利的，并且建议将输送的持续时间和喷雾处理限制在最多30秒。

3. 发明授权

US4950339A Process of forming phosphate coatings on metals 失效
标题翻译：在金属上形成磷酸盐涂层的工艺
公开(公告)号：US4950339A
公开(公告)日：1990-08-21
申请号：US305214
申请日：1989-02-01
申请人： Horst Gehmecker , Werner Rausch , Peter Jorns
发明人： Horst Gehmecker , Werner Rausch , Peter Jorns
IPC分类号： C23C22/36 , C23C22/78
CPC分类号： C23C22/362 , C23C22/78
摘要： A process to form phosphate coatings on individual parts of metal which at least on part of their surface consists of iron or steel. The individual parts are contacted at a temperature in the range of from 60 to 100 degrees centigrade for 3 to 30 seconds with an aqueous phosphating solution which contains 10 to 80 g/l zinc, 12 to 80 g/l phosphate (calculated as P.sub.2 O.sub.5), 40 to 150 g/l nitrate and, in addition 0.1 to 10 g/l fluoride, 0.01 to 10 g/l nickel, 0.0001 to 0.1 g/l copper, and may also contain tartaric acid, citric acid and/or manganese and in which the ratio of free acid to total acid has been adjusted to (0.1 to 0.3):1 and which contains at least 80 points of total acid and is virtually free of iron(II) ions. Prior to phosphating treatment, the individual parts may be cleaned and may optionally be treated to remove rust, scale and phosphate layers and/or be activated. After the phosphating treatment they may be passivated with an after-rinse solution. Each of said process steps is carried out for 3 to 30 seconds.
摘要翻译：在金属的单个部分上形成磷酸盐涂层的方法，其至少部分表面由铁或钢组成。使用含有10至80g / l锌，12至80g / l磷酸盐（以P2O5计算）的磷酸盐水溶液将各个部件在60至100摄氏度的温度范围内接触3至30秒，，40〜150g / l的硝酸盐，以及0.1〜10g / l的氟化物，0.01〜10g / l的镍，0.0001〜0.1g / l的铜，也可以含有酒石酸，柠檬酸和/或锰，其中游离酸与总酸的比例已经被调节到（0.1〜0.3）：1，并且其含有至少80个总酸，实际上没有铁（II）离子。在磷化处理之前，可以清洁各个部件，并且可以任选地处理以除去锈，鳞屑和磷酸盐层和/或被活化。在磷化处理后，可以用冲洗液进行钝化。每个所述处理步骤进行3至30秒。

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