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1. 发明授权

US4160764A Water-insoluble monoazo-dyestuffs for synthetic fibrous materials 失效
标题翻译：用于合成纤维材料的水不溶性单偶氮染料
公开(公告)号：US4160764A
公开(公告)日：1979-07-10
申请号：US894177
申请日：1978-04-06
申请人： Peter Mischke , Erwin Fleckenstein , Reinhard Mohr
发明人： Peter Mischke , Erwin Fleckenstein , Reinhard Mohr
IPC分类号： C09B29/08 , C09B31/043 , C09B29/26 , C09B31/08
CPC分类号： C09B29/0834 , C09B31/043
摘要： Azo-dyestuff of the formula ##STR1## in which D represents nitrophenylene, ##STR2## DINITRO-PHENYLENE, NITRO-CYANO-PHENYLENE, NITRO-CHLORO-PHENYLENE, NITRO-BROMO-PHENYLENE, TRICHLORO-PHENYLENE, NITRO-DICHLORO-PHENYLENE, DINITRO-CHLORO-PHENYLENE, DINITRO-CYANO-PHENYLENE, NITRO-BROMO-CYANO-PHENYLENE, DINITRO-BROMO-PHENYLENE, PHENYLAZO-PHENYLENE, ##STR3## R represents hydrogen, chlorine, lower alkyl, lower alkoxy, --O--CH.sub.2 --CN, --NH--CO--lower alkyl, --NH--COO lower alkyl or ##STR4## n stands for the integer 1 or 2, X represents cyano, --CO--NH.sub.2 or --COO-lower alkyl, R.sub.1 represents hydrogen, lower alkyl, lower alkylene-OH, lower alkylene-CN, lower alkylene-OCO-lower alkyl or lower alkenyl, and R.sub.2 represents lower alkyl, lower alkylene-O-CO-lower alkyl or lower alkylene-COO-lower alkyl, said dyestuffs being suitable for the dyeing or printing of synthetic fibrous materials, such as fibers of cellulose-di-, -21/2- or -triacetat, polyamides, polyurethanes, polyolefines, polycarbonates and particularly of linear polyesters, the dyeings or prints obtained being distinguished by a very good build up, tinctorial strength and a series of very good fastness properties.
摘要翻译：其中D表示硝基亚苯基，偶氮苯基，硝基 - 苯基，硝基 - 苯基，硝基 - 溴 - 苯基，三氯苯基，硝基 - 二氯苯，苯并噻吩，四甲基氯苯，十一烷基 - 苯乙烯，硝基 - 溴 - 氰基 - 苯乙烯，十一烷基 - 苯乙烯，苯基 - 苯乙烯，<图像> <图像>＆lt; IMA＆gt;＆gt;＆gt; R代表氢，氯，低级烷基，低级烷氧基，-O-CH 2 -CN，-NH-CO-低级烷基，-NH-COO低级烷基或n代表整数1或2，X代表氰基，-CO-NH 2或 - 低级烷基，R 1表示氢，低级烷基，低级亚烷基-OH，低级亚烷基-CN，低级亚烷基-OCO-低级烷基或低级烯基，R 2表示低级烷基，低级亚烷基-O-CO-低级烷基或低级烷基亚烷基-COO-低级烷基，所述染料适用于合成纤维材料的染色或印刷，例如纤维素二 - ，二 - 或2-三乙酸纤维，聚酰胺，聚氨酯，聚烯烃，聚碳酸酯特别是线性聚酯，所获得的染色或印花的特征在于非常好的聚集度，着色强度和一系列非常好的坚牢度性质。

2. 发明授权

US3947463A Certain 2-amino-nicotinonitrile derivatives 失效
标题翻译：某些2-氨基 - 烟腈衍生物
公开(公告)号：US3947463A
公开(公告)日：1976-03-30
申请号：US521530
申请日：1974-11-06
申请人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
发明人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
IPC分类号： C07D401/06 , C07D401/12 , C07D413/04 , C07D213/57
CPC分类号： C07D413/04 , C07D401/06 , C07D401/12 , Y10S8/917 , Y10S8/922 , Y10S8/927
摘要： Compounds of the formulaWherein X is aliphatic, cycloaliphatic, aromatic, aralkyl, hetaryl, hetarylalkyl or hydrogen; Y is aliphatic, aromatic, aralkyl, --COOR.sub.1, --COR.sub.2, ##EQU1## --SO.sub.2 R.sub.2, ##EQU2## --CN, --NH.sub.2, --NO, --NO.sub.2 or hydrogen with the proviso that when Y is hydrogen, X is other than hydrogen; Z.sub.1 is cyano, ##EQU3## --NH--OR.sub.10, ##EQU4## --OR.sub.12, --SR.sub.12 or --SO.sub.2 R.sub.12 and Z.sub.2 is chlorine, bromine, cyano, hydroxy, mercapto, --OR.sub.12, --SR.sub.12, ##EQU5## --NH--OR.sub.10 or ##EQU6## R.sub.1 is aliphatic; R.sub.2 is aliphatic, cycloaliphatic, aromatic, aralkyl or heterocyclic; R.sub.1 and R.sub.4 when taken separately are hydrogen, aliphatic, cycloaliphatic, aromatic or aralkyl; R.sub.3 and R.sub.4 when taken together with the nitrogen atom to which they are attached form a heterocyclic moiety; R.sub.5 and R.sub.6 when taken separately are aliphatic, aromatic, aralkyl, heterocyclic or hydrogen; R.sub.5 and R.sub.6 when taken together with the nitrogen atom to which they are attached are heterocyclic; R.sub.7 is hydrogen, aliphatic or aromatic; R.sub.8 and R.sub.9 are aliphatic or aromatic, R.sub.10 is hydrogen, aliphatic or aralkyl, R.sub.11 is aliphatic and R.sub.12 is aliphatic, aromatic or aralkyl; R.sub.10 and R.sub.11 when taken together with the nitrogen atom to which they are attached are heterocyclic.
摘要翻译：式WH的化合物是脂族，脂环族，芳族，芳烷基，杂芳基，杂芳基烷基或氢; Y是脂族的，芳族的，芳烷基，-COOR 1，-COR 2，R 3 -CO-N角，R 4 -SO 2 R 2，R 3 -SO 2 -N取代基，R 4 -CN，-NH 2，-NO，-NO 2或氢，条件是当Y是氢时，X不是氢; Z 1是氰基，R 5 -N ANGLE，R 6 R 7 R 8 ANGLE NN ANGLE，R 9 -NH-OR 10，OR 10 -N ANGLE，R 11 -OR 12，-SR 12或-SO 2 R 12，Z 2是氯，溴，氰基，羟基，巯基，-OR 12 ，-SR 12，R 5 -SO 2 R 12，-N ANGLE，R 6 R 7 R 8 ANGLE NN ANGLE，R 9 -NH-OR 10或OR 10 -N角; R11 R1是脂肪族的; R2是脂族，脂环族，芳族，芳烷基或杂环; 单独使用时，R 1和R 4为氢，脂族，脂环族，芳族或芳烷基; 当与它们所连接的氮原子一起形成杂环部分时，R 3和R 4; R5和R6分别为脂族，芳族，芳烷基，杂环或氢时; 当与它们所连接的氮原子一起取代时，R 5和R 6是杂环的; R7是氢，脂族或芳族; R8和R9是脂族或芳族的，R10是氢，脂族或芳烷基，R11是脂族的，R12是脂族的，芳族的或芳烷基; 当与它们所连接的氮原子一起取代时，R 10和R 11是杂环的。

3. 发明授权

US4061642A 2,4,6-Trisubstituted-3-pyridine carboxamides 失效
标题翻译： 2,4,6-三取代-3-吡啶甲酰胺
公开(公告)号：US4061642A
公开(公告)日：1977-12-06
申请号：US687705
申请日：1976-05-19
申请人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
发明人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
IPC分类号： C07D213/69 , C07D213/70 , C07D213/73 , C07D213/74 , C07D213/76 , C07D213/77 , C07D213/80 , C07D213/82 , C07D213/85 , C07D401/06 , C07D401/12 , C07D413/04 , C07D213/56
CPC分类号： C07D213/69 , C07D213/70 , C07D213/73 , C07D213/74 , C07D213/76 , C07D213/77 , C07D213/80 , C07D213/82 , C07D213/85 , C07D401/06 , C07D401/12 , C07D413/04
摘要： Compounds of the formula ##STR1## wherein X is aliphatic, cycloaliphatic, aromatic, aralkyl, hetaryl, hetarylalkyl or hydrogen; Y is aliphatic, aromatic, aralkyl, --COOR.sub.1, --COR.sub.2, ##STR2## --SO.sub.2 R.sub.2, ##STR3## --CN, --NH.sub.2, --NO, --NO.sub.2 or hydrogen with the proviso that when Y is hydrogen, X is other than hydrogen; Z.sub.1 is cyano, ##STR4## --NH--OR.sub.10, ##STR5## --OR.sub.12, --SR.sub.12 or --SO.sub.2 R.sub.12 and Z.sub.2 is chlorine, bromine, cyano, hydroxy, mercapto, --OR.sub.12, --SR.sub.12, --SO.sub.2 R.sub.12, ##STR6## --NH--OR.sub.10 or ##STR7## R.sub.1 is aliphatic; R.sub.2 is aliphatic, cycloaliphatic, aromatic, aralkyl or heterocyclic; R.sub.3 and R.sub.4 when taken separately are hydrogen, aliphatic, cycloaliphatic, aromatic or aralkyl; R.sub.3 and R.sub.4 when taken together with the nitrogen atom to which they are attached form a heterocyclic moiety; R.sub.5 and R.sub.6 when taken separately are aliphatic, aromatic, aralkyl, heterocyclic or hydrogen; R.sub.5 and R.sub.6 when taken together with the nitrogen atom to which they are attached are heterocyclic; R.sub.7 is hydrogen, aliphatic or aromatic; R.sub.8 and R.sub.9 are aliphatic or aromatic, R.sub.10 is hydrogen, aliphatic or aralkyl, R.sub.11 is aliphatic and R.sub.12 is aliphatic, aromatic or aralkyl; R.sub.10 and R.sub.11 when taken together with the nitrogen atom to which they are attached are heterocyclic.
摘要翻译：其中X是脂族，脂环族，芳族，芳烷基，杂芳基，杂芳基烷基或氢的式IMA化合物; Y是脂族，芳族，芳烷基，-COOR1，-COR2，-SO2R2，IMA，-CN，-NH2，-NO，-NO2或氢，条件是当Y是氢时，X不是氢 ; Z 1是氰基，-NH-OR 10，-IG 12，-SR 12或-SO 2 R 12，Z 2是氯，溴，氰基，羟基，巯基，-OR 12，-SR 12，-SO 2 R 12， -OR10或 R1是脂肪族的; R2是脂族，脂环族，芳族，芳烷基或杂环; 单独使用时，R 3和R 4为氢，脂族，脂环族，芳族或芳烷基; 当与它们所连接的氮原子一起形成杂环部分时，R 3和R 4; R5和R6分别为脂族，芳族，芳烷基，杂环或氢时; 当与它们所连接的氮原子一起取代时，R 5和R 6是杂环的; R7是氢，脂族或芳族; R8和R9是脂族或芳族的，R10是氢，脂族或芳烷基，R11是脂族的，R12是脂族的，芳族的或芳烷基; 当与它们所连接的氮原子一起取代时，R 10和R 11是杂环的。

4. 发明授权

US3946024A 2-Hydrocarbyloxy-pyridine compounds 失效
标题翻译： 2-烃氧基 - 吡啶化合物
公开(公告)号：US3946024A
公开(公告)日：1976-03-23
申请号：US563848
申请日：1975-03-31
申请人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
发明人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
IPC分类号： C07D401/06 , C07D401/12 , C07D413/04 , C07D213/57
CPC分类号： C07D413/04 , C07D401/06 , C07D401/12 , Y10S8/917 , Y10S8/922 , Y10S8/927
摘要： Compounds of the formula ##SPC1##Wherein X is aliphatic, cycloaliphatic, aromatic, aralkyl, hetaryl, hetarylalkyl or hydrogen; Y is aliphatic, aromatic, aralkyl, --COOR.sub.1, --COR.sub.2, ##EQU1## --SO.sub.2 R.sub.2, ##EQU2## --CN, --NH.sub.2, --NO, --NO.sub.2 or hydrogen with the proviso that when Y is hydrogen, X is other than hydrogen; Z.sub.1 is cyano, ##EQU3## --NH--OR.sub.10, ##EQU4## --OR.sub.12, --SR.sub.12 or --SO.sub.2 R.sub.12 and Z.sub.2 is chlorine, bromine, cyano, hydroxy, mercapto, --OR.sub.12, --SR.sub.12, --SO.sub.2 R.sub.12, ##EQU5## --NH--OR.sub.10 or ##EQU6## R.sub.1 is aliphatic; R.sub.2 is aliphatic, cycloaliphatic, aromatic, aralkyl or heterocyclic; R.sub.3 and R.sub.4 when taken separately are hydrogen, aliphatic, cycloaliphatic, aromatic or aralkyl; R.sub.3 and R.sub.4 when taken together with the nitrogen atom to which they are attached form a heterocyclic moiety; R.sub.5 and R.sub.6 when taken separately are aliphatic, aromatic, aralkyl, heterocyclic or hydrogen; R.sub.5 and R.sub.6 when taken together with the nitrogen atom to which they are attached are heterocyclic; R.sub.7 is hydrogen, aliphatic or aromatic; R.sub.8 and R.sub.9 are aliphatic or aromatic, R.sub.10 is hydrogen, aliphatic or aralkyl, R.sub.11 is aliphatic and R.sub.12 is aliphatic, aromatic or aralkyl; R.sub.10 and R.sub.11 when taken together with the nitrogen atom to which they are attached are heterocyclic.
摘要翻译：式WH的化合物是脂族，脂环族，芳族，芳烷基，杂芳基，杂芳基烷基或氢; Y是脂族的，芳族的，芳烷基，-COOR 1，-COR 2，R 3 -CO-N角，R 4 -SO 2 R 2，R 3 -SO 2 -N取代基，R 4 -CN，-NH 2，-NO，-NO 2或氢，条件是当Y是氢时，X不是氢; Z 1是氰基，R 5 R 7 R 8 -N取代基，取代的炔基，R 6 R 9 -NH-OR 10，OR 10 -N取代基，R 11 -OR 12，-SR 12或-SO 2 R 12，Z 2是氯，溴，氰基，羟基，巯基，-OR 12 ，-SR 12，-SO 2 R 12，R 5 R 7 R 8 -N角，角NN角，R 6 R9 -NH-OR 10或OR 10 -N角; R11 R1是脂肪族的; R2是脂族，脂环族，芳族，芳烷基或杂环; 单独使用时，R 3和R 4为氢，脂族，脂环族，芳族或芳烷基; 当与它们所连接的氮原子一起形成杂环部分时，R 3和R 4; R5和R6分别为脂族，芳族，芳烷基，杂环或氢时; 当与它们所连接的氮原子一起取代时，R 5和R 6是杂环的; R7是氢，脂族或芳族; R8和R9是脂族或芳族的，R10是氢，脂族或芳烷基，R11是脂族的，R12是脂族的，芳族的或芳烷基; 当与它们所连接的氮原子一起取代时，R 10和R 11是杂环的。

5. 发明授权

US3954782A 2,6-Hydrazino-3-pyridine carboxyamides 失效
标题翻译： 2,6-二肼-3-吡啶羧酰胺
公开(公告)号：US3954782A
公开(公告)日：1976-05-04
申请号：US521408
申请日：1974-11-06
申请人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
发明人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
IPC分类号： C07D401/06 , C07D401/12 , C07D413/04 , C07D295/12
CPC分类号： C07D413/04 , C07D401/06 , C07D401/12
摘要： Compounds of the formula ##SPC1##Wherein X is aliphatic, cycloaliphatic, aromatic, aralkyl, hetaryl, hetarylalkyl or hydrogen; Y is aliphatic, aromatic, aralkyl, --COOR.sub.1, --COR.sub.2, ##EQU1## --SO.sub.2 R.sub.2, ##EQU2## --CN, --NH.sub.2, --NO, --NO.sub.2 or hydrogen with the proviso that when Y is hydrogen, X is other than hydrogen; Z.sub.1 is cyano, ##EQU3## --NH--OR.sub.10, ##EQU4## --OR.sub.12, --SR.sub.12 or --SO.sub.2 R.sub.12 and Z.sub.2 is chlorine, bromine, cyano, hydroxy, mercapto, --OR.sub.12, --SR.sub.12, --SO.sub.2 R.sub.12, ##EQU5## --NH--OR.sub.10 or ##EQU6## R.sub.1 is aliphatic; R.sub.2 is aliphatic, cycloaliphatic, aromatic, aralkyl or heterocyclic; R.sub.3 and R.sub.4 when taken separately are hydrogen, aliphatic, cycloaliphatic, aromatic or aralkyl; R.sub.3 and R.sub.4 when taken together with the nitrogen atom to which they are attached form a heterocyclic moiety; R.sub.5 and R.sub.6 when taken separately are aliphatic, aromatic, aralkyl, heterocyclic or hydrogen; R.sub.5 and R.sub.6 when taken together with the nitrogen atom to which they are attached are heterocyclic; R.sub.7 is hydrogen, aliphatic or aromatic; R.sub.8 and R.sub.9 are aliphatic or aromatic, R.sub.10 is hydrogen, aliphatic or aralkyl, R.sub.11 is aliphatic and R.sub.12 is aliphatic, aromatic or aralkyl; R.sub.10 and R.sub.11 when taken together with the nitrogen atom to which they are attached are heterocyclic.
摘要翻译：式WH的化合物是脂族，脂环族，芳族，芳烷基，杂芳基，杂芳基烷基或氢; Y是脂族的，芳族的，芳烷基，-COOR 1，-COR 2，R 3 -CO-N角，R 4 -SO 2 R 2，R 3 -SO 2 -N取代基，R 4 -CN，-NH 2，-NO，-NO 2或氢，条件是当Y是氢时，X不是氢; Z 1是氰基，R 5 -N ANGLE，R 6 R 7 R 8 ANGLE NN ANGLE，R 9 -NH-OR 10，OR 10 -N ANGLE，R 11 -OR 12，-SR 12或-SO 2 R 12，Z 2是氯，溴，氰基，羟基，巯基，-OR 12 ，-SR 12，-SO 2 R 12，R 5 -N，G 6，R 7 R 8， R11 R1是脂肪族的; R2是脂族，脂环族，芳族，芳烷基或杂环; 单独使用时，R 3和R 4为氢，脂族，脂环族，芳族或芳烷基; 当与它们所连接的氮原子一起形成杂环部分时，R 3和R 4; R5和R6分别为脂族，芳族，芳烷基，杂环或氢时; 当与它们所连接的氮原子一起取代时，R 5和R 6是杂环的; R7是氢，脂族或芳族; R8和R9是脂族或芳族的，R10是氢，脂族或芳烷基，R11是脂族的，R12是脂族的，芳族的或芳烷基; 当与它们所连接的氮原子一起取代时，R 10和R 11是杂环的。

6. 发明授权

US3980659A Certain 6-amino-4-hydrocarbyl-nicotinamides 失效
标题翻译：某些6-氨基-4-烃基 - 烟酰胺
公开(公告)号：US3980659A
公开(公告)日：1976-09-14
申请号：US521442
申请日：1974-11-06
申请人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
发明人： Erwin Fleckenstein , Ernst Heinrich , Reinhard Mohr
IPC分类号： C07D401/06 , C07D401/12 , C07D413/04 , C07D213/44
CPC分类号： C07D413/04 , C07D401/06 , C07D401/12 , Y10S8/922
摘要： Compounds of the formula ##SPC1##Wherein X is aliphatic, cycloaliphatic, aromatic, aralkyl, hetaryl, hetarylalkyl or hydrogen; Y is aliphatic, aromatic, aralkyl, --COOR.sub.1, --COR.sub.2, ##EQU1## --SO.sub.2 R.sub.2, ##EQU2## --CN, --NH.sub.2, --NO, --NO.sub.2 or hydrogen with the proviso that when Y is hydrogen, X is other than hydrogen; Z.sub.1 is cyano, ##EQU3## --NH--OR.sub.10, ##EQU4## --OR.sub.12, --SR.sub.12 or --SO.sub.2 R.sub.12 and Z.sub.2 is chlorine, bromine, cyano, hydroxy, mercapto, --OR.sub.12, --SR.sub.12, --SO.sub.2 R.sub.12, ##EQU5## --NH--OR.sub.10 or ##EQU6## R.sub.1 is aliphatic; R.sub.2 is aliphatic, cycloaliphatic, aromatic, aralkyl or heterocyclic; R.sub.3 and R.sub.4 when taken separately are hydrogen, aliphatic, cycloaliphatic, aromatic or aralkyl; R.sub.3 and R.sub.4 when taken together with the nitrogen atom to which they are attached form a heterocyclic moiety; R.sub.5 and R.sub.6 when taken separately are aliphatic, aromatic, aralkyl, heterocyclic or hydrogen; R.sub.5 and R.sub.6 when taken together with the nitrogen atom to which they are attached are heterocyclic; R.sub.7 is hydrogen, aliphatic or aromatic; R.sub.8 and R.sub.9 are aliphatic or aromatic, R.sub.10 is hydrogen, aliphatic or aralkyl, R.sub.11 is aliphatic and R.sub.12 is aliphatic, aromatic or aralkyl; R.sub.10 and R.sub.11 when taken together with the nitrogen atom to which they are attached are heterocyclic.
摘要翻译：式WH的化合物是脂族，脂环族，芳族，芳烷基，杂芳基，杂芳基烷基或氢; Y是脂族的，芳族的，芳烷基，-COOR 1，-COR 2，R 3 -CO-N角，R 4 -SO 2 R 2，R 3 -SO 2 -N取代基，R 4 -CN，-NH 2，-NO，-NO 2或氢，条件是当Y是氢时，X不是氢; Z 1是氰基，R 5 R 7 R 8 -N取代基，ANGLE NN ANGLE，R 6 R 9 -NH-OR 10，OR 10 -N ANGLE，R 11 -OR 12，-SR 12或-SO 2 R 12，Z 2是氯，溴，氰基，羟基，巯基，-OR 12 - SR12，-SO2R12，R5R7R8-AN，ANGLE NN ANGLE，R6R9 -NH-OR10或OR10 -N ANGLE; R11 R1是脂肪族的; R2是脂族，脂环族，芳族，芳烷基或杂环; 单独使用时，R 3和R 4为氢，脂族，脂环族，芳族或芳烷基; 当与它们所连接的氮原子一起形成杂环部分时，R 3和R 4; R5和R6分别为脂族，芳族，芳烷基，杂环或氢时; 当与它们所连接的氮原子一起取代时，R 5和R 6是杂环的; R7是氢，脂族或芳族; R8和R9是脂族或芳族的，R10是氢，脂族或芳烷基，R11是脂族的，R12是脂族的，芳族的或芳烷基; 当与它们所连接的氮原子一起取代时，R 10和R 11是杂环的。

7. 发明授权

US4028321A Basic azo amino-phenylene dyestuffs 失效
标题翻译：碱性偶氮氨基亚苯基染料
公开(公告)号：US4028321A
公开(公告)日：1977-06-07
申请号：US491175
申请日：1974-07-23
申请人： Erwin Fleckenstein , Peter Mischke
发明人： Erwin Fleckenstein , Peter Mischke
IPC分类号： C09B27/00 , C09B44/00 , C09B44/04 , C09B44/10 , C09B29/06 , C09B29/08 , C09B29/36 , C09B43/00
CPC分类号： C09B44/10 , C09B44/04
摘要： A basic dyestuff of the formula ##STR1## wherein R.sub.1 is hydrogen, alkyl of 1 to 5 carbon atoms, hydroxyalkyl of 1 to 4 carbon atoms, cyanoalkyl of 1 to 4 carbon atoms in the alkyl moiety or chloroalkyl of 1 to 4 carbon atoms, R'.sub.2 is phenyl or naphthyl or is phenyl or naphthyl substituted by alkyl of 1 to 4 C-atoms and/or alkoxy of 1 to 4 carbon atoms or nitro or cyano and/or chlorine, R.sub.5 is an optionally substituted alkyl or aralkyl radical, R.sub.6 and R.sub.7 being the same or different, each is hydrogen or an alkyl radical or, both together, substituents which complete to form an anellated aromatic ring, Y is a bivalent atom or a bivalent group necessary to complete a 5- or 6-ring, R.sub.10 is hydrogen, fluorine, bromine or chlorine or alkyl of 1 to 4 C-atoms and X.sup..sup.-`is an anion, which are suitable for the dyeing or printing of tannined cellulose fibers, silk, leather or fully synthetic fibers, such as acetate silk, polyamide fibers or acid modified polyamide or polyester fibers, especially of fibers which contain polyacrylonitrile or polyvinylidene cyanide. Their dyeings are in general very intense and have, for example, good fastnesses to light and to wetting processes, to chlorine and perspiration. They are resistant to a large degree to a change of the pH-value of the dyebath and can therefore be used both in a slightly acidic and in a strongly acidic bath. Wool is completely reserved by the dyestuffs under normal dyeing conditions.
摘要翻译：其中R 1为氢，1至5个碳原子的烷基，1至4个碳原子的羟基烷基，1至4个碳原子的烷基部分的氰基烷基或1个氯代烷基的基本染料至4个碳原子，R'2是苯基或萘基，或是被1-4个碳原子的烷基和/或1-4个碳原子的烷氧基或硝基或氰基和/或氯取代的苯基或萘基，R5是任意的取代的烷基或芳烷基，R 6和R 7相同或不同，各自为氢或烷基，或两者一起为完成形成Anellated芳环的取代基，Y为二价原子或完成 5-或6-环，R 10为氢，氟，溴或氯或1〜4个C原子的烷基，X 1'为阴离子，适用于染色或印花单宁纤维素纤维，丝绸，皮革或全合成纤维，如醋酸丝，聚酰胺纤维或酸改性聚酰胺或聚酯纤维，特别是含有聚丙烯腈或聚偏二氰乙烯的纤维。它们的染色通常非常强烈，并且具有例如良好的耐光牢度和湿润过程，氯和汗水。它们在很大程度上抵抗染浴的pH值的变化，因此可以在轻微酸性和强酸性浴中使用。在正常染色条件下，羊毛完全由染料保留。

8. 发明授权

US3939142A Phenylazophenyl dyestuff 失效
标题翻译：苯基苯基染料
公开(公告)号：US3939142A
公开(公告)日：1976-02-17
申请号：US495191
申请日：1974-08-06
申请人： Erwin Fleckenstein
发明人： Erwin Fleckenstein
IPC分类号： C07D213/85 , C09B29/00 , C09B44/02 , C09B62/51 , D06P1/90 , C07C115/00
CPC分类号： C09B44/02 , C09B29/00 , D06P1/908
摘要： Basic azo dyestuffs, free from sulfo groups and having the formulaWherein Z is the radical of a tertiary amino group or of a quaternary ammonium group, Alk is alkylene of two to five carbon atoms, X is oxygen, Ar is phenylene unsubstituted or substituted by alkyl of one to four carbon atoms, alkoxy of one to four carbon atoms and/or chlorine or bromine, and K as the radical of a coupling component is the radical of a tertiary amine of the benzene series, the radical of 2,6-diamino-3-cyano-4-methyl pyridine or a derivative thereof or the radical of the 2-hydroxynaphthalene series, which are suitable for the preparation of writing and stamping inks or pastes for ball-point pens as well as suitable in offset printing and for the dyeing, printing or mass dyeing of, for example, tannined cellulose fibers, silk, hair, leather, acetate silk, polyamide fibers or acid modified polyolefins, polyamide or polyester fibers and fibers containing polyacrylonitrile or polyvinylidene cyanide. The dyeings obtained on these fibers have, in general, a high color intensity and, in general, good fastness to light and to wet processing. The dyestuffs can be used in slightly acid and strongly acid baths and are stable at a temperature above 100.degree.C as used in high-temperature dyeing. Wool is completely reserved by the dyestuffs under normal dyeing conditions.
摘要翻译：碱性偶氮染料，不含磺基，具有式WHEREIN Z为叔氨基或季铵基团的基团，Alk为2至5个碳原子的亚烷基，X为氧，Ar为未取代的苯基或被 1-4个碳原子的烷基，1-4个碳原子的烷氧基和/或氯或溴，作为偶合组分基团的K是苯系的叔胺基团，二氨基-3-氰基-4-甲基吡啶或其衍生物或2-羟基萘系列的基团，其适用于制备用于圆珠笔的书写和冲压油墨或糊料，以及适用于胶版印刷和用于例如单宁纤维素纤维，丝绸，毛发，皮革，醋酸丝，聚酰胺纤维或酸改性聚烯烃，聚酰胺或聚酯纤维和含有聚丙烯腈或聚偏二氰乙烯的纤维的染色，印花或大量染色。在这些纤维上获得的染色通常具有高的颜色强度，并且通常具有良好的耐光牢度和湿润的加工性。该染料可用于轻酸和强酸浴中，并且在高温染色中使用的高于100℃的温度下是稳定的。在正常染色条件下，羊毛完全由染料保留。

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