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1. 发明授权

US07829477B2 Fluorinated water soluble copolymers 失效
标题翻译：氟化水溶性共聚物
公开(公告)号：US07829477B2
公开(公告)日：2010-11-09
申请号：US11978290
申请日：2007-10-29
申请人： Peter Michael Murphy , Jessica Sinks , Ying Wang
发明人： Peter Michael Murphy , Jessica Sinks , Ying Wang
IPC分类号： B32B5/02
CPC分类号： C09D133/16 , C08F220/04 , C08F220/24 , C08F220/32 , C08F220/38 , C08F220/58 , Y10T428/23986 , Y10T428/31544 , Y10T442/2172 , Y10T442/2279 , Y10T442/2287
摘要： A method of providing water repellency, oil repellency, soil resistance, soil release, stain resistance and stain release to substrates comprising contacting said substrate with a composition comprising a copolymer having repeating units of Formula 1 in any sequence: wherein Rf is a straight or branched perfluoroalkyl group having from about 2 to about 8 carbon atoms, or a mixture thereof, which is optionally interrupted by at least one oxygen atom, Q is alkylene of 1 to about 15 carbon atoms, hydroxyalkylene of 2 to about 15 carbon atoms, —O(CnH2n)—, —(CH2CF2)m(CH2)n—, —CONR1(CnH2n)—, —(CnH2n)OCONR1(CnH2n)—, (—CONR1CH2)2CH—, —SO2N(R1)(CnH2n)—, or —(CnH2n)SO2N(R1)(CnH2n)—, each R1 is independently H or alkyl of 1 to about 4 carbon atoms, each n is independently 1 to about 15, each m is independently 1 to about 4, Z is hydrogen or methyl, x is a positive integer, y is zero or a positive integer, t is a positive integer, and M is H+, alkali metal cation, alkaline earth metal cation, or ammonium.
摘要翻译：提供防水性，拒油性，耐土壤性，污垢释放，耐污染性和对基材的污迹释放的方法，包括使所述底物与包含具有任何顺序的具有式1的重复单元的共聚物的组合物接触的组合物接触：其中Rf是直链或支链具有约2至约8个碳原子的全氟烷基或其混合物，其任选被至少一个氧原子间隔，Q为1至约15个碳原子的亚烷基，2至约15个碳原子的羟基亚烷基，-O （CnH2n） - ， - （CH2CF2）m（CH2）n-，-CONR1（CnH2n） - ， - （CnH2n）OCONR1（CnH2n） - ，（-CONR1CH2）2CH-，-SO2N（R1）（CnH2n）或 - （C n H 2n）SO 2 N（R 1）（C n H 2n） - ，每个R 1独立地为H或1至约4个碳原子的烷基，每个n独立地为1至约15，m各自独立地为1至约4，Z为氢或甲基，x为正整数，y为零或正整数，t为正整数，M为H +，碱金属阳离子，碱地球金属阳离子或铵。

2. 发明申请

US20090111344A1 Fluorinated water soluble copolymers 失效
标题翻译：氟化水溶性共聚物
公开(公告)号：US20090111344A1
公开(公告)日：2009-04-30
申请号：US11978290
申请日：2007-10-29
申请人： Peter Michael Murphy , Jessica Sinks , Ying Wang
发明人： Peter Michael Murphy , Jessica Sinks , Ying Wang
IPC分类号： C11D3/37 , C08F14/20 , B32B5/02 , B32B3/02 , B32B27/08 , B32B27/10 , B32B27/06
CPC分类号： C09D133/16 , C08F220/04 , C08F220/24 , C08F220/32 , C08F220/38 , C08F220/58 , Y10T428/23986 , Y10T428/31544 , Y10T442/2172 , Y10T442/2279 , Y10T442/2287
摘要： A method of providing water repellency, oil repellency, soil resistance, soil release, stain resistance and stain release to substrates comprising contacting said substrate with a composition comprising a copolymer having repeating units of Formula I in any sequence: wherein Rf is a straight or branched perfluoroalkyl group having from about 2 to about 8 carbon atoms, or a mixture thereof, which is optionally interrupted by at least one oxygen atom, Q is alkylene of 1 to about 15 carbon atoms, hydroxyalkylene of 2 to about 15 carbon atoms, —O(CnH2n)—, —(CH2CF2)m(CH2)n—, —CONR1(CnH2n)—, —(CnH2n)OCONR1(CnH2n)—, (—CONR1CH2)2CH—, —SO2N(R1)(CnH2n)—, or —(CnH2n)SO2N(R1)(CnH2n)—, each R1 is independently H or alkyl of 1 to about 4 carbon atoms, each n is independently 1 to about 15, each m is independently 1 to about 4, Z is hydrogen or methyl, x is a positive integer, y is zero or a positive integer, t is a positive integer, and M is H+, alkali metal cation, alkaline earth metal cation, or ammonium.
摘要翻译：提供防水性，拒油性，耐土壤性，污垢释放，耐污染性和对底物的污迹释放的方法，包括使所述底物与包含具有以下任何顺序的式I重复单元的共聚物的组合物接触的组合物：其中Rf是直链或支链具有约2至约8个碳原子的全氟烷基或其混合物，其任选被至少一个氧原子间隔，Q为1至约15个碳原子的亚烷基，2至约15个碳原子的羟基亚烷基，-O （CnH2n） - ， - （CH2CF2）m（CH2）n-，-CONR1（CnH2n） - ， - （CnH2n）OCONR1（CnH2n） - ，（-CONR1CH2）2CH-，-SO2N（R1）（CnH2n）或 - （C n H 2n）SO 2 N（R 1）（C n H 2n） - ，每个R 1独立地为H或1至约4个碳原子的烷基，每个n独立地为1至约15，m各自独立地为1至约4，Z为氢或甲基，x为正整数，y为零或正整数，t为正整数，M为H +，碱金属阳离子，碱土金属阳离子或 onium。

3. 发明授权

US07737307B2 Fluorinated nonionic surfactants 失效
标题翻译：氟化非离子表面活性剂
公开(公告)号：US07737307B2
公开(公告)日：2010-06-15
申请号：US11890375
申请日：2007-08-06
申请人： Peter Michael Murphy , Andrew Edward Feiring , Stephan James McLain , Jessica Sinks
发明人： Peter Michael Murphy , Andrew Edward Feiring , Stephan James McLain , Jessica Sinks
IPC分类号： C07C43/11
CPC分类号： C07C43/126 , C07C43/137 , C08G65/337 , C08L71/02 , C11D1/004 , C11D1/722
摘要： A compound comprising Formula I, or a mixture thereof, Rf—OCFHCF2O—[CH2CH2O]x—[C3H7O]y-A Formula I wherein Rf is CnF2n+1, n is 1 to about 6, x is a mixture of positive integers and is 4 or greater, y is 0 to about 4, provided that the ratio of y to x is equal to or less than 0.25, A is RfOCHFCF2 or CmH2m+1, and m is 1 to about 24 and its use in lowering surface tension and imparting improved surface effects is disclosed.
摘要翻译：包含式I或其混合物的化合物Rf-OCFHCF 2 O - [CH 2 CH 2 O] x - [C 3 H 7 O] y A式I其中R f为C n F 2n + 1，n为1至约6，x为正整数的混合物，为4 或更大，y为0至约4，条件是y与x的比例等于或小于0.25，A为RfOCHFCF2或CmH2m + 1，m为1至约24，并且其用于降低表面张力和赋予公开了改善的表面效果。

4. 发明申请

US20090043133A1 Fluorinated nonionic surfactants 失效
标题翻译：氟化非离子表面活性剂
公开(公告)号：US20090043133A1
公开(公告)日：2009-02-12
申请号：US11890375
申请日：2007-08-06
申请人： Peter Michael Murphy , Andrew Edward Feiring , Stephan James McLain , Jessica Sinks
发明人： Peter Michael Murphy , Andrew Edward Feiring , Stephan James McLain , Jessica Sinks
IPC分类号： C07C409/00
CPC分类号： C07C43/126 , C07C43/137 , C08G65/337 , C08L71/02 , C11D1/004 , C11D1/722
摘要： A compound comprising Formula I, or a mixture thereof, Rf—OCFHCF2O—[CH2CH2O]x—[C3H7O]y-A Formula I wherein Rf is CnF2n+1, n is 1 to about 6, x is a mixture of positive integers and is 4 or greater, y is 0 to about 4, provided that the ratio of y to x is equal to or less than 0.25, A is RfOCHFCF2 or CmH2m+1, and m is 0 to about 24 and its use in lowering surface tension and imparting improved surface effects is disclosed.
摘要翻译：包含式I或其混合物的化合物<？在线公式描述=“在线式”末端=“铅”→Rf-OCFHCF 2 O- [CH 2 CH 2 O] x - [C 3 H 7 O] y A式I < in-line-formula description =“In-line Formulas”end =“tail”？>其中Rf为CnF2n + 1，n为1至约6，x为正整数的混合物，为4或更大，y为0 至约4，条件是y与x的比例等于或小于0.25，A为RfOCHFCF2或CmH2m + 1，m为0至约24，并且其用于降低表面张力并赋予改善的表面效果。

5. 发明授权

US07399887B1 Fluorinated sulfonate surfactants 失效
标题翻译：氟化磺酸盐表面活性剂
公开(公告)号：US07399887B1
公开(公告)日：2008-07-15
申请号：US11890374
申请日：2007-08-06
申请人： Peter Michael Murphy , Andrew Edward Feiring , Stephan James McLain , Jessica Sinks
发明人： Peter Michael Murphy , Andrew Edward Feiring , Stephan James McLain , Jessica Sinks
IPC分类号： C07C321/00 , C07C323/00 , C07C381/00
CPC分类号： C07C309/14 , A61K8/466 , C09D5/027 , C09D7/47 , C09G1/04 , C11D1/004
摘要： A compound comprising Formula I, or a mixture thereof, wherein Y is a bond or CmH2m−p(OA)p wherein m is 0 to 4, and p is 0 or 1, X′ is X or H, X is CH2CH2OA, CH(CH2OA)2, C(CH2OA)3, or X and X′ combine to form (CH2CH2)2NCH2CH2OA or (CH2CH2)2O, provided that when X and X′ combine to form (CH2CH2)2O then Y is CH2CH(OA)CH2, A is CF2CFHO—Rf or H, Rf is CnF2n+1 wherein n is an integer of 1 to about 6, M is a cation having a charge equal to a, and a is a positive integer equal to 1 or 2, provided that at least one of X, X′, or Y contains A equal to CF2CFHO—Rf, and its use in lowering surface tension and imparting improved surface effects.
摘要翻译：包含式I或其混合物的化合物，其中Y是键或C m H 2 m-p（OA）p p其中m 为0〜4，p为0或1，X'为X或H，X为CH 2 CH 2 OA，CH（CH 2） C（CH 2 OA）3，或X和X'结合形成（CH 2）2， 2/2个2或2个或2个或更多个（CH 2）2 其中X和X'组合形成（CH 2 CH 2 CH 2）2 O，）2 O，则Y是CH 2 CH（OA）CH 2，A是CF 2 CO 2 -OR 2 或H，R f是C n H 2n + 1，其中n是1至约的整数如图6所示，M是电荷等于a的阳离子，a是等于1或2的正整数，条件是X，X'或Y中的至少一个包含等于CF 2 CFHO-R f的A， / SUB>，其用于降低表面张力并赋予改善的表面效果。

6. 发明申请

US20090148653A1 FLUOROPOLYMER EMULSIONS 审中-公开
标题翻译：氟聚乳酸
公开(公告)号：US20090148653A1
公开(公告)日：2009-06-11
申请号：US12237446
申请日：2008-09-25
申请人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
发明人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
IPC分类号： B32B5/02 , C08L67/06 , C08L81/00 , C08L79/02 , D03D27/00 , B32B27/10 , C08L77/00 , C08L63/00 , C08L83/00
CPC分类号： C08F220/24 , C08F2/44 , Y10T428/23986 , Y10T428/249921 , Y10T428/3154 , Y10T428/31993 , Y10T442/20 , Y10T442/2172
摘要： A fluoropolymer composition comprising monomers copolymerized in the following percentages by weight: (a) from about 20% to about 95% of a fluoroalkyl monomer, or mixture of monomers, of formula (I) Rf1-L-X—C(O)—C(R)═CH2 (I) whereinRf1 is a monovalent, partially or fully fluorinated, linear or branched, alkyl radical having from about 2 to about 100 carbon atoms; optionally interrupted by 1 to about 50 oxygen atoms; wherein the ratio of carbon atoms to oxygen atoms is at least about 2:1 and no oxygen atoms are bonded to each other;L is a linear or branched divalent linking group having 1 to about 20 carbon atoms; optionally interrupted by 1 to about 4 hetero-radicals selected from the group consisting or —O—, —NR1—, —S—, —SO—, —SO2—, —N(R1)C(O)—; wherein R1 is H or C1 to C6 alkyl;X is —O—, —NR1—, or —S—;R is hydrogen, Cl, F or CH3; (b) from about 5% to about 80% of at least one of: (i) an alkyl(meth)acrylate monomer having a linear, branched or cyclic alkyl group of from about 6 to about 18 carbons; or (ii) one or more ionizable water solvatable monomers; and (c) from about 0.05% to about 2% polymerizable nanoparticles.
摘要翻译：一种含氟聚合物组合物，其包含按以下重量百分比共聚的单体：（a）约20％至约95％的式（I）的氟代烷基单体或单体混合物<？在线公式描述=“In 线型式“end =”lead“→Rf1-LXC（O）-C（R）-CH2（I）<βin-line-formula description =”In-line Formulas“end =”tail“？>其中 Rf1是具有约2至约100个碳原子的单价，部分或完全氟化的直链或支链烷基; 任选地被1至约50个氧原子中断; 其中碳原子与氧原子的比例为至少约2:1且没有氧原子彼此键合; L是具有1至约20个碳原子的直链或支链二价连接基团; 任选地被1至大约4个选自以下的杂原子中断：-NR 1 - ， - S - ， - SO - ， - SO 2 - ， - N（R 1）C（O） - ; 其中R1是H或C1-C6烷基; X是-O-，-NR1-或-S-; R是氢，Cl，F或CH 3; （b）约5％至约80％的至少一种：（i）具有约6至约18个碳原子的直链，支链或环状烷基的（甲基）丙烯酸烷基酯单体; 或（ii）一种或多种可离子化的水可溶性单体; 和（c）约0.05％至约2％的可聚合纳米颗粒。

7. 发明申请

US20080202384A1 Fluoropolymer compositions and method of use 审中-公开
公开(公告)号：US20080202384A1
公开(公告)日：2008-08-28
申请号：US11712324
申请日：2007-02-28
申请人： Sheng Peng , Stephen James Getty , Patrick Henry Fitzgerald , Peter Michael Murphy , Ying Wang , Ernest Byron Wysong
发明人： Sheng Peng , Stephen James Getty , Patrick Henry Fitzgerald , Peter Michael Murphy , Ying Wang , Ernest Byron Wysong
IPC分类号： C09K3/18 , C08F10/00 , C08F14/18
CPC分类号： C08F214/18 , C08F214/186 , C08F220/18 , C08F220/24 , C08F220/28 , C08F220/58 , C09D133/16 , D06M15/263 , D06M15/267 , D06M15/277 , D06M2200/01 , D06M2200/11 , D06M2200/12
摘要： A composition comprising monomers copolymerized in the following percentages by weight: (a) from about 20% to about 95% of a monomer, or mixture of monomers, of formula (I): Rf—(CH2CF2)q(CH2CH2)r-Z-C(O)—C(R)═CH2 (I) wherein q and r are each independently integers of 1 to 3; Rf is a linear or branched perfluoroalkyl group having 2 to 6 carbon atoms; Z is —O—, —NR1— or —S—; R is hydrogen, Cl, F or CH3; R1 is hydrogen, or a C1 to C4 alkyl; and (b) from about 5% to about 80% of at least one of: (i) an alkyl (meth)acrylate monomer having a linear, branched or cyclic alkyl group of 6 to 18 carbons; or (ii) a monomer of formula (II): (R2)2N—R3—O—C(O)—C(R)═CH2 (II) wherein R is as defined above; each R2 is independently a C1 to C4 alkyl; and R3 is a divalent linear or branched C1 to C4 alkylene; and wherein the nitrogen is from about 40% to 100% salinized; or (iii) a mixture thereof; said composition providing oil repellency, water repellency, and stain resistance to substrates contacted therewith; and a method for treating substrates with such copolymer compositions; are disclosed.

8. 发明申请

US20090149096A1 FLUOROPOLYMER EMULSIONS 有权
标题翻译：氟聚乳酸
公开(公告)号：US20090149096A1
公开(公告)日：2009-06-11
申请号：US12268470
申请日：2008-11-11
申请人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
发明人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
IPC分类号： B32B27/12 , B32B27/04 , B32B27/00 , C08F220/24
CPC分类号： C08F220/24 , C08F2/44 , Y10T428/23986 , Y10T428/249921 , Y10T428/3154 , Y10T428/31993 , Y10T442/20 , Y10T442/2172
摘要： A fluoropolymer composition comprising monomers copolymerized in the following percentages by weight: (a) from about 20% to about 95% of a fluoroalkyl monomer, or mixture of monomers, (b) from about 5% to about 80% of at least one of: (i) an alkyl (meth)acrylate monomer having a linear, branched or cyclic alkyl group of from about 6 to about 18 carbons; or (ii) one or more ionizable water solvatable monomers; and (c) from about 0.05% to about 2% non-fluorinated polymerizable nanoparticles.
摘要翻译：一种含氟聚合物组合物，其包含按以下重量百分比共聚的单体：（a）约20％至约95％的氟烷基单体或单体混合物，（b）约5％至约80％：（i）具有约6至约18个碳原子的直链，支链或环状烷基的（甲基）丙烯酸烷基酯单体; 或（ii）一种或多种可离子化的水可溶性单体; 和（c）约0.05％至约2％的非氟化可聚合纳米颗粒。

9. 发明授权

US08314037B2 Fluoropolymer emulsions 有权
标题翻译：含氟聚合物乳液
公开(公告)号：US08314037B2
公开(公告)日：2012-11-20
申请号：US12268470
申请日：2008-11-11
申请人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
发明人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
IPC分类号： B32B5/02 , B32B27/00 , C08F18/20 , A01K1/015
CPC分类号： C08F220/24 , C08F2/44 , Y10T428/23986 , Y10T428/249921 , Y10T428/3154 , Y10T428/31993 , Y10T442/20 , Y10T442/2172
摘要： A fluoropolymer composition comprising monomers copolymerized in the following percentages by weight: (a) from about 20% to about 95% of a fluoroalkyl monomer, or mixture of monomers, (b) from about 5% to about 80% of at least one of: (i) an alkyl (meth)acrylate monomer having a linear, branched or cyclic alkyl group of from about 6 to about 18 carbons; or (ii) one or more ionizable water solvatable monomers; and (c) from about 0.05% to about 2% non-fluorinated polymerizable nanoparticles.
摘要翻译：一种含氟聚合物组合物，其包含按以下重量百分比共聚的单体：（a）约20％至约95％的氟烷基单体或单体混合物，（b）约5％至约80％：（i）具有约6至约18个碳原子的直链，支链或环状烷基的（甲基）丙烯酸烷基酯单体; 或（ii）一种或多种可离子化的水可溶性单体; 和（c）约0.05％至约2％的非氟化可聚合纳米颗粒。

10. 发明申请

US20110178260A1 FLUOROPOLYMER COMPOSITIONS AND METHOD OF USE 审中-公开
标题翻译：氟聚合物组合物和使用方法
公开(公告)号：US20110178260A1
公开(公告)日：2011-07-21
申请号：US12690674
申请日：2010-01-20
申请人： Sheng Peng , Stephen James Getty , Patrick Henry Fitzgerald , Peter Michael Murphy , Ying Wang , Ernest Byron Wysong
发明人： Sheng Peng , Stephen James Getty , Patrick Henry Fitzgerald , Peter Michael Murphy , Ying Wang , Ernest Byron Wysong
IPC分类号： C08F220/22
CPC分类号： C08F220/24 , C08F2220/1891 , D06M15/263 , D06M15/267 , D06M15/277 , D06M15/295 , D06M2200/01 , C08F2220/1858 , C08F2220/281 , C08F220/58 , C08F2220/325 , C08F2220/286
摘要： A composition comprising monomers copolymerized in the following percentages by weight: (a) from about 20% to about 95% of a monomer, or mixture of monomers, of formula (I): Rf—(CH2CF2)q(CH2CH2)r—Z—C(O)—C(R)═CH2 (I) wherein q and r are each independently integers of 1 to 3; Rf is a linear or branched perfluoroalkyl group having 2 to 6 carbon atoms; Z is —O—, —NR1— or —S—; R is hydrogen, Cl, F or CH3; R1 is hydrogen, or a C1 to C4 alkyl; and (b) from about 5% to about 80% of at least one of: (i) an alkyl (meth)acrylate monomer having a linear, branched or cyclic alkyl group of 6 to 18 carbons; or (ii) a monomer of formula (II): (R2)2N—R3—O—C(O)—C(R)═CH2 (II) wherein R is as defined above; each R2 is independently a C1 to C4 alkyl; and R3 is a divalent linear or branched C1 to C4 alkylene; and wherein the nitrogen is from about 40% to 100% salinized; or (iii) a mixture thereof; said composition providing oil repellency, water repellency, and stain resistance to substrates contacted therewith; and a method for treating substrates with such copolymer compositions; are disclosed.
摘要翻译：包含按以下重量百分比共聚单体的组合物：（a）约20％至约95％的式（I）单体或单体混合物：Rf-（CH 2 CF 2）q（CH 2 CH 2）r-Z -C（O）-C（R）= CH 2（I）其中q和r各自独立地为1至3的整数; Rf是具有2-6个碳原子的直链或支链全氟烷基; Z是-O-，-NR1-或-S-; R是氢，Cl，F或CH 3; R1是氢或C1-C4烷基; 和（b）约5％至约80％的至少一种：（i）具有6至18个碳原子的直链，支链或环状烷基的（甲基）丙烯酸烷基酯单体; 或（ii）式（II）的单体：（R2）2N-R3-O-C（O）-C（R）= CH2（Ⅱ）其中R定义同上; 每个R 2独立地为C 1至C 4烷基; 并且R 3是二价直链或支链C1至C4亚烷基; 并且其中所述氮为约40％至100％盐碱化; 或（iii）其混合物; 所述组合物对与其接触的基材提供拒油性，拒水性和耐污染性; 和用这种共聚物组合物处理底物的方法; 被披露。

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