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1. 发明授权

US06187892B1 Method of making a coated substrate with polyurethane/urea contact adhesive formulations and the coated substrate by this method 失效
标题翻译：通过该方法制备具有聚氨酯/脲接触粘合剂制剂的涂布基材和涂布的基材的方法
公开(公告)号：US06187892B1
公开(公告)日：2001-02-13
申请号：US08483349
申请日：1995-06-07
申请人： Peter H. Markusch , James W. Rosthauser , Robert L. Cline
发明人： Peter H. Markusch , James W. Rosthauser , Robert L. Cline
IPC分类号： C08G1848
CPC分类号： C09J175/12 , C08G18/482 , C08G18/5024 , Y02P20/582 , Y10S528/905 , Y10T428/31551
摘要： The present invention relates to a method of making a coated substrate that requires a polyurethane/urea contact adhesive, and the coated substrates produced by this method. This invention requires a) a polyisocyanate with a functionality of less than about 4, b) optionally, a polyol blend consisting of about 95 to 100% polyether polyols with molecular weights from about 1800 to 12000 and average functionality from about 1.5 to about 4 and up to about 5% of chain extenders with molecular weights from about 60 to 400 and average functionality from about 1.5 to about 3, and c) polyethers having at least two isocyanate reactive groups and a molecular weight of from about 1800 to about 12000 and average functionality from about 1.5 to about 4 in which at least 50% of the isocyanate reactive groups are primary and/or secondary amino groups. The weight ratio of components b) to component c) ranges from about 95:5 to about 0:100, and the amounts of components a), b), and c) are such that the equivalent ratio of isocyanate groups to isocyanate-reactive groups is from about 85:100 to about 115:100 and the sum of the urethane group content plus the urea group content is from about 1 to about 12%.
摘要翻译：本发明涉及一种制备需要聚氨酯/尿素接触粘合剂的涂布基材和通过该方法制备的涂布基材的方法。本发明要求a）具有小于约4的官能度的多异氰酸酯，b）任选地，由约95至100％的分子量为约1800至12000的聚醚多元醇和平均官能度为约1.5至约4的多元醇共混物和高达约5％的分子量为约60至400且平均官能度为约1.5至约3的扩链剂，以及c）具有至少两个异氰酸酯反应性基团和分子量为约1800至约12000的聚醚和平均约1.5至约4的官能度，其中至少50％的异氰酸酯反应性基团是伯和/或仲氨基。组分b）与组分c）的重量比范围为约95:5至约0:100，并且组分a），b）和c）的量使得异氰酸酯基团与异氰酸酯反应性的当量比基团为约85:100至约115:100，并且氨基甲酸酯基含量加上尿素基团含量的总和为约1至约12％。

2. 发明授权

US5733966A Polyurethane contact adhesives with improved temperature resistance properties 失效
标题翻译：具有改善耐温性能的聚氨酯接触粘合剂
公开(公告)号：US5733966A
公开(公告)日：1998-03-31
申请号：US787066
申请日：1997-01-22
申请人： Robert L. Cline , James W. Rosthauser , Peter H. Markusch
发明人： Robert L. Cline , James W. Rosthauser , Peter H. Markusch
IPC分类号： C08G18/48 , C08G18/72 , C09J175/08 , C08J3/00 , C08G18/00 , C08K3/20 , C08L75/00
CPC分类号： C08G18/725 , C08G18/4812 , C09J175/08 , C08G2170/40 , Y02P20/582
摘要： The present invention relates to highly elastic polyurethane contact adhesives, a process to coat substrates with these contact adhesives, and the coated substrates produced by this process. This invention requires a) a polyisocyanate with a functionality of less than about 4 and b) a polyol blend comprising 1) about 90 to 100% polyethers with molecular weights from about 1,800 to 12,000 and average functionality from about 1.5 to about 4, and 2) up to about 10% of chain extenders with molecular weights from about 60 to 400 and average functionality from about 1.5 to about 3. The functionalities and amounts of components a) and b) are such that the molecular weight between crosslinks is from about 7,000 to about 16,000 and the equivalent ratio of isocyanate groups to isocyanate-reactive groups is from about 80:100 to about 120:100 and the urethane group content is from about 1 to about 8%. It is preferred that at least one of components a) and b) have a functionality of greater than about 2.2.
摘要翻译：本发明涉及高弹性聚氨酯接触粘合剂，用这些接触粘合剂涂覆基材的方法以及通过该方法生产的涂布基材。本发明要求a）具有小于约4的官能度的多异氰酸酯和b）多元醇共混物，其包含1）约90至100％分子量为约1,800至12,000的聚醚，平均官能度为约1.5至约4，和2 ）至多约10％的分子量为约60至400且平均官能度为约1.5至约3的扩链剂。组分a）和b）的官能度和量使得交联之间的分子量为约7,000 至约16,000，异氰酸酯基与异氰酸酯反应性基团的当量比为约80:100至约120：100，氨基甲酸酯基含量为约1至约8％。组分a）和b）中的至少一种优选具有大于约2.2的官能度。

3. 发明授权

US6040028A Removable polyurethane adhesives with improved temperature resistance properties 失效
标题翻译：具有改善耐温性能的可拆卸聚氨酯胶粘剂
公开(公告)号：US6040028A
公开(公告)日：2000-03-21
申请号：US6129
申请日：1998-01-13
申请人： Robert L. Cline , James W. Rosthauser , Peter H. Markusch
发明人： Robert L. Cline , James W. Rosthauser , Peter H. Markusch
IPC分类号： C08G18/48 , C08G18/75 , C08L75/08 , C09J7/02 , C09J175/08
CPC分类号： C09J175/08 , C08G18/4812 , C08G18/758 , C09J7/0207 , C08G2170/40 , C08L75/08 , C09J2475/00 , Y02P20/582 , Y10T428/1476 , Y10T428/28 , Y10T428/2896
摘要： The present invention relates to highly elastic polyurethane contact adhesives, a process to coat substrates with these contact adhesives, and the coated substrates produced by this process. This invention requires a) a polyisocyanate with a functionality of less than about 4 and b) a polyol blend comprising 1) about 90 to 100% polyethers with molecular weights from about 1,800 to 12,000 and average functionality from about 1.5 to about 4, and 2) up to about 10% of chain extenders with molecular weights from about 60 to 400 and average functionality from about 1.5 to about 3. The functionalities and amounts of components a) and b) are such that the molecular weight between crosslinks is from about 7,000 to about 16,000 and the equivalent ratio of isocyanate groups to isocyanate-reactive groups is from about 80:100 to about 120:100 and the urethane group content is from about 1 to about 8%. It is preferred that at least one of components a) and b) have a functionality of greater than about 2.2.
摘要翻译：本发明涉及高弹性聚氨酯接触粘合剂，用这些接触粘合剂涂覆基材的方法以及通过该方法生产的涂布基材。本发明要求a）具有小于约4的官能度的多异氰酸酯和b）多元醇共混物，其包含1）约90至100％分子量为约1,800至12,000的聚醚，平均官能度为约1.5至约4，和2 ）至多约10％的分子量为约60至400且平均官能度为约1.5至约3的扩链剂。组分a）和b）的官能度和量使得交联之间的分子量为约7,000 至约16,000，异氰酸酯基与异氰酸酯反应性基团的当量比为约80:100至约120：100，氨基甲酸酯基含量为约1至约8％。组分a）和b）中的至少一种优选具有大于约2.2的官能度。

4. 发明授权

US06364925B1 Polyurethane encapsulated fertilizer having improved slow-release properties 失效
标题翻译：具有改善缓释性能的聚氨酯包封肥料
公开(公告)号：US06364925B1
公开(公告)日：2002-04-02
申请号：US09458818
申请日：1999-12-10
申请人： Peter H. Markusch , Robert L. Cline , Ashok M. Sarpeshkar , Robert P. Yeater
发明人： Peter H. Markusch , Robert L. Cline , Ashok M. Sarpeshkar , Robert P. Yeater
IPC分类号： C05G500
CPC分类号： C09D175/04 , C08G18/4891 , C08G18/6696
摘要： The present invention relates to polyurethane encapsulated fertilizer particles which exhibit slow-release properties and to a process for their production. The process comprises applying an isocyanate-reactive component to fertilizer particles, to form fertilizer particles coated with an isocyanate-reactive component, applying a polyisocyanate component onto the coated fertilizer particles to form polyurethane encapsulated fertilizer particles, and, optionally, repeating these steps as many times as necessary to form the polyurethane encapsulated fertilizer particles that contain about 2 to 20% by weight of polyurethane, based on the total weight of the encapsulated fertilizer particles. Suitable isocyanate-reactive components include polyesterether polyols that comprise either a blend of or the reaction product of (i) castor oil having an OH number of about 160 to about 170, a viscosity of about 500 to about 900 mPa.s at 25° C., and a water content of less than 0.5% by weight; and (ii) a polyether polyol having an OH number of from 28 to 700, a functionality of from 3 to 8, and a molecular weight of about 240 to about 6,000, and a viscosity of from about 50 to 35,000 mPa.s at 25° C. The polyether polyol must be prepared from a suitable initiator compound and an alkylene oxide comprising at least 70% by weight of propylene oxide.
摘要翻译：本发明涉及具有缓释特性的聚氨酯包封肥料颗粒及其生产方法。该方法包括将异氰酸酯反应性组分施用于肥料颗粒，以形成涂覆有异氰酸酯反应性组分的肥料颗粒，将多异氰酸酯组分施加到涂覆的肥料颗粒上以形成聚氨酯包封的肥料颗粒，以及任选地重复这些步骤以形成包含约2至20重量％的聚氨酯的聚氨酯包封的肥料颗粒，基于包封的肥料颗粒的总重量。合适的异氰酸酯反应性组分包括聚异戊二烯多元醇，其包含（i）OH值为约160至约170的蓖麻油，25℃下约500至约900mPa.s的粘度的混合物或其反应产物含水量小于0.5重量％; 和（ii）OH值为28至700，官能度为3至8，分子量为约240至约6,000，粘度为约50至35,000mPa.s在25的聚醚多元醇聚醚多元醇必须由合适的引发剂化合物和包含至少70重量％环氧丙烷的烯化氧制备。

5. 发明授权

US06358296B1 Slow-release polyurethane encapsulated fertilizer using oleo polyols 失效
标题翻译：使用油脂多元醇缓释聚氨酯包封肥料
公开(公告)号：US06358296B1
公开(公告)日：2002-03-19
申请号：US09613680
申请日：2000-07-11
申请人： Peter H. Markusch , Robert L. Cline , Ashok M. Sarpeshkar
发明人： Peter H. Markusch , Robert L. Cline , Ashok M. Sarpeshkar
IPC分类号： C05G500
CPC分类号： C08G18/36 , C05G3/0029 , C08G18/7664
摘要： This invention relates to polyurethane encapsulated fertilizer particles which exhibit slow-release properties and to a process for their production. The process comprises (1) applying an isocyanate-reactive component or a polyisocyanate component to fertilizer particles, to form coated fertilizer particles, followed by (2) applying a polyisocyanate component or an isocyanate-reactive component onto the coated fertilizer particles to form polyurethane encapsulated fertilizer particles, and, optionally, repeating these steps as many times as necessary to form the polyurethane encapsulated fertilizer particles that contain about 2 to 20% by weight of polyurethane, based on the total weight of the encapsulated fertilizer particles. Alternatively, the isocyanate-reactive component and the polyisocyanate component can be premixed prior to being applied to the fertilizer particles to form polyurethane encapsulated fertilizer particles. Suitable isocyanate-reactive components comprise oleo polyols.
摘要翻译：本发明涉及具有缓释特性的聚氨酯包封的肥料颗粒及其生产方法。该方法包括（1）将异氰酸酯反应性组分或多异氰酸酯组分施用于肥料颗粒，以形成包覆的肥料颗粒，随后将（2）将多异氰酸酯组分或异氰酸酯反应性组分施加到涂覆的肥料颗粒上以形成聚氨酯包封肥料颗粒，并且任选地重复这些步骤，以根据包封的肥料颗粒的总重量形成含有约2至20重量％聚氨酯的聚氨酯包封的肥料颗粒。或者，异氰酸酯反应性组分和多异氰酸酯组分可以在施用于肥料颗粒之前预混合以形成聚氨酯包封的肥料颗粒。合适的异氰酸酯反应性组分包括油醇多元醇。

6. 发明授权

US6152981A Sulfur containing isocyanate compositions 有权
标题翻译：含硫异氰酸酯组合物
公开(公告)号：US6152981A
公开(公告)日：2000-11-28
申请号：US255285
申请日：1999-02-22
申请人： Peter H. Markusch , Donald MacNaughtan, Jr. , William G. Crabtree , Robert L. Cline
发明人： Peter H. Markusch , Donald MacNaughtan, Jr. , William G. Crabtree , Robert L. Cline
IPC分类号： C05G3/00 , C08G18/32 , C08G18/76 , C08K3/06 , A01N25/00 , A01N27/00 , A01N31/00
CPC分类号： C05G3/0023 , C05G3/0029 , C08G18/3206 , C08G18/7664 , C08K3/06 , C08G2230/00
摘要： This invention relates to an isocyanate composition comprising a) at least one isocyanate and b) from 1 to 50% by weight, based on the total weight of component a), of sulfur. These isocyanate compositions are suitable for the preparation of polyurethane/polyurea encapsulated fertilizers. Accordingly, the present invention also relates to an improved process for the production of a polyurea/polyurethane encapsulated fertilizer comprising applying at least one isocyanate-reactive component to the fertilizer particles and applying the isocyanate compositions of the present invention to the fertilizer particles, to form these polyurea/polyurethane encapsulated fertilizers.
摘要翻译：本发明涉及异氰酸酯组合物，其包含a）至少一种异氰酸酯和b）基于组分a）的总重量为1至50重量％的硫。这些异氰酸酯组合物适用于制备聚氨酯/聚脲包封肥料。因此，本发明还涉及用于生产聚脲/聚氨酯包封的肥料的改进方法，包括将至少一种异氰酸酯反应性组分施用于肥料颗粒并将本发明的异氰酸酯组合物施用于肥料颗粒，以形成这些聚脲/聚氨酯包封肥料。

7. 发明授权

US06617412B2 Fertilizer encapsulation using sulfur containing polyols 失效
标题翻译：含硫多元醇的肥料封装
公开(公告)号：US06617412B2
公开(公告)日：2003-09-09
申请号：US09976610
申请日：2001-10-12
申请人： Peter H. Markusch , Robert L. Cline
发明人： Peter H. Markusch , Robert L. Cline
IPC分类号： C08G1840
CPC分类号： C08G18/3206 , C05G3/0023 , C05G3/0029 , C08G18/48
摘要： This invention relates to fertilizer encapsulation with polyurethanes wherein the isocyanate-reactive composition contains sulfur. The process of the present invention comprises applying a polyisocyanate composition to fertilizer particles, applying an isocyanate-reactive composition which contains sulfur to the polyisocyanate coated fertilizer particles, or applying an isocyanate-reactive composition which contains sulfur to fertilizer particles and then applying a polyisocyanate composition to the isocyanate-reactive coated fertilizer particles, and repeating these steps as necessary to form sulfur containing polyurethane encapsulated fertilizer particles.
摘要翻译：本发明涉及具有聚氨酯的肥料封装，其中异氰酸酯反应性组合物含有硫。本发明的方法包括将多异氰酸酯组合物施加到肥料颗粒上，将含有硫的异氰酸酯反应性组合物施加到多异氰酸酯涂覆的肥料颗粒上，或将含有硫的异氰酸酯反应性组合物施用于肥料颗粒，然后施加多异氰酸酯组合物涉及异氰酸酯反应性包被的肥料颗粒，并根据需要重复这些步骤以形成含硫聚氨酯包封的肥料颗粒。

8. 发明授权

US5851261A Process for the production of polyurea encapsulated fertilizer particles and the encapsulated fertilizer particles produced by this process 失效
标题翻译：用于生产聚脲包封的肥料颗粒和通过该方法生产的包封的肥料颗粒的方法
公开(公告)号：US5851261A
公开(公告)日：1998-12-22
申请号：US777426
申请日：1996-12-30
申请人： Peter H. Markusch , Robert L. Cline
发明人： Peter H. Markusch , Robert L. Cline
IPC分类号： C05G3/00 , C05G5/00 , C08G18/50
CPC分类号： C08G18/5024 , C05G3/0029
摘要： This invention relates to a process for the production of polyurea encapsulated fertilizer particles. These are produced by applying an isocyanate-reactive component which contains at least two amine groups to fertilizer particles to form amine coated particles, and applying a polyisocyanate component to the amine coated particles to form polyurea coated particles. These steps may optionally be repeated in successive order. The resultant polyurea encapsulated fertilizer particles contain from about 0.5 to 15% by weight of polyurea, based on the total weight of the encapsulated fertilizer particles. Instead of using an amine group containing isocyanate-reactive component, water can be applied first.
摘要翻译：本发明涉及一种生产聚脲包封肥料颗粒的方法。这些是通过将含有至少两个胺基的异氰酸酯反应性组分施用于肥料颗粒以形成胺包被的颗粒并将多异氰酸酯组分施加到胺涂覆的颗粒上以形成聚脲涂覆的颗粒来制备的。这些步骤可以可选地以连续的顺序重复。基于所包封的肥料颗粒的总重量，所得聚脲包封的肥料颗粒含有约0.5至15重量％的聚脲。代替使用含有异氰酸酯反应性组分的胺基，可以首先施加水。

9. 发明授权

US06562932B1 Light stable one-shot urethane-urea elastomers 有权
标题翻译：光稳定的一次性尿素 - 尿素弹性体
公开(公告)号：US06562932B1
公开(公告)日：2003-05-13
申请号：US09976397
申请日：2001-10-12
申请人： Peter H. Markusch , Robert L. Cline , Richard S. Pantone , Ralf Guether , Thomas L. Sekelik , Karl W. Haider
发明人： Peter H. Markusch , Robert L. Cline , Richard S. Pantone , Ralf Guether , Thomas L. Sekelik , Karl W. Haider
IPC分类号： C08G1810
CPC分类号： C08G18/758 , B32B17/1077 , C08G18/10 , C08G18/73 , C08G18/755 , C08G18/6674 , C08G18/6685
摘要： This invention relates to a process for the production of an optically clear, light-stable polyurethane-urea elastomer having an onset softening point of at least 130° C., processed at ambient temperature and casted in a mold at an isocyanate index of 95 to 120. This process comprises reacting: A) a liquid polyisocyanate or polyisocyanate prepolymer having an NCO group content of about 5 to about 50%, an average functionality of 2 to 3, a viscosity of less than 5,000 mPa.s at 25° C.; and B) an isocyanate-reactive component; in the presence of C) at least one organometallic catalyst. The present invention also relates to the optically clear, light-stable polyurethane-urea elastomers produced by this process.
摘要翻译：本发明涉及一种生产具有至少130℃起始软化点的光学透明，轻质稳定的聚氨酯 - 脲弹性体的方法，在环境温度下加工并浇铸在异氰酸酯指数为95至该方法包括使A）具有NCO基团含量为约5至约50％，平均官能度为2至3，25℃时粘度小于5,000mPa.s的液体多异氰酸酯或多异氰酸酯预聚物 ; 和B）异氰酸酯反应性组分; 在C）存在下至少有一种有机金属催化剂。本发明还涉及通过该方法制备的光学透明的，轻质的聚氨酯 - 脲弹性体。

10. 发明授权

US5770673A Non-sagging, light stable polyurethane compositions, a process for producing them, and their use as seam sealants 失效
标题翻译：非流挂，轻质聚氨酯组合物，其制备方法及其作为缝隙密封剂的用途
公开(公告)号：US5770673A
公开(公告)日：1998-06-23
申请号：US630660
申请日：1996-04-10
申请人： Peter H. Markusch , Robert L. Cline , A. M. Sarpeshkar
发明人： Peter H. Markusch , Robert L. Cline , A. M. Sarpeshkar
IPC分类号： C08G18/28 , C08G18/66 , C08G18/79 , C08G18/48
CPC分类号： C08G18/792 , C08G18/2865 , C08G18/6681 , C08G2190/00
摘要： The present invention relates to non-sagging, light stable polyurethane compositions. These non-sagging, light stable polyurethane compositions are the reaction product of a liquid hexamethylene diisocyanate adduct with a mixture of an organic compound containing hydroxyl groups, an aliphatic and/or alicyclic diamine, and an alkanolamine. It also relates to a process for producing these non-sagging, light stable compositions, and their use as seam sealants.
摘要翻译：本发明涉及非流挂，轻质聚氨酯组合物。这些不流挂的轻质聚氨酯组合物是液体六亚甲基二异氰酸酯加合物与含羟基的有机化合物，脂族和/或脂环族二胺和链烷醇胺的混合物的反应产物。它还涉及一种用于生产这些非流挂，轻质组合物的方法及其作为缝隙密封剂的用途。

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