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1. 发明专利

JP2012057255A Method for electrolytic synthesis of fluorine-containing substance using anode for electrolysis 有权
标题翻译：使用阳极进行电解的含氟物质的电解合成方法
公开(公告)号：JP2012057255A
公开(公告)日：2012-03-22
申请号：JP2011266948
申请日：2011-12-06
申请人： Permelec Electrode Ltd , ペルメレック電極株式会社
发明人： TASAKA AKIMASA , UNO MASAHARU , NISHIKI YOSHINORI , FURUTA TSUNETO
IPC分类号： C25B11/12 , C01B31/06 , C25B1/24
摘要： PROBLEM TO BE SOLVED: To provide an anode material for electrolysis in an electrolytic bath containing anhydrous hydrofluoric acid, which is free from the occurrence of an anode effect, does not remarkably produce sludge due to the dissolution of an electrode, is capable of suppressing the production of CFand capable of stably continuing electrolysis without causing the breakdown of the electrode.SOLUTION: An electrolytic bath containing anhydrous hydrofluoric acid or anhydrous hydrofluoric acid to which a material to be fluorinated is added is subjected to electrolysis using an electrode for electrolysis formed by coating at least part of a conductive material base including glassy carbon with a conductive diamond film, whereby fluorine or a fluorine-containing compound is electrolytically synthesized.
摘要翻译：要解决的问题：为了在不含阳极效应的无水氟酸的电解槽中提供用于电解的阳极材料，由于电极的溶解而不能显着地产生污泥，所以能够抑制CF 4 的生产，并能够稳定地继续电解而不引起电极的破坏。解决方案：将含有待被氟化材料的无水氢氟酸或无水氢氟酸的电解浴用电解法进行电解，所述电解电极通过将包含玻璃碳的导电材料基体的至少一部分涂覆至导电金刚石膜，由此氟或含氟化合物被电解合成。版权所有（C）2012，JPO＆INPIT

2. 发明专利

JP2008127583A Membrane-electrode assembly, electrolytic unit using the same, electrolytic water jetting device and sterilization method 有权
标题翻译：膜电极组件，使用其的电解单元，电解水喷射装置和灭菌方法
公开(公告)号：JP2008127583A
公开(公告)日：2008-06-05
申请号：JP2006310591
申请日：2006-11-16
申请人： Institute Of National Colleges Of Technology Japan , Permelec Electrode Ltd , ペルメレック電極株式会社 , 独立行政法人国立高等専門学校機構
发明人： KITAORI NORIYUKI , SEKIDO KOTA , UNO MASAHARU , SHIBATA TOMOYASU , NISHIKI YOSHINORI , FURUTA TSUNETO
IPC分类号： C25B1/30 , A61L2/22 , C02F1/46 , C25B1/13 , C25B11/02 , C25B11/03 , C25B11/06 , C25B11/12
摘要： PROBLEM TO BE SOLVED: To provide a membrane-electrode assembly and an electrolytic unit for producing electrolytic water in which an electrolytic product such as hydrogen peroxide is dissolved in high concentration, an apparatus for jetting the electrolytic water obtained using the same and particularly a small-sized spray device for spraying the resultant electrolytic water in the form of mist. SOLUTION: The membrane-electrode assembly includes a belt-like diaphragm 8 covered around of a rod-like or cylindrical anode 7 and a belt-like porous carbon material made cathode 9 installed on the surface of the diaphragm. The electrolytic unit has the membrane-electrode assembly installed in a tube 5. The electrolytic water spray device 1 has the electrolytic unit 6. Sterilization by electrolytic seeds having a desirable concentration is made possible by spraying or atomizing the resultant electrolytic water to an object. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：解决问题的方案为了提供一种用于生产电解质水的电解质水溶液的电解质水溶液的电解质水溶液的制造方法，其特征在于，提供一种电解水，特别是用于喷雾所形成的电解水的小型喷雾装置。解决方案：膜 - 电极组件包括覆盖在棒状或圆柱形阳极7周围的带状隔膜8和安装在隔膜表面上的带状多孔碳材料制成的阴极9。电解单元具有安装在管5中的膜 - 电极组件。电解喷水装置1具有电解单元6.通过将所得到的电解水喷雾或雾化到物体，可以使具有所需浓度的电解种子进行灭菌。版权所有（C）2008，JPO＆INPIT

3. 发明专利

JP2008073604A Membrane-electrode assembly, electrolytic unit using the same, electrolytic water ejecting apparatus, and method of sterilization 有权
标题翻译：膜电极组件，使用其的电解单元，电解水喷射装置和灭菌方法
公开(公告)号：JP2008073604A
公开(公告)日：2008-04-03
申请号：JP2006254874
申请日：2006-09-20
申请人： Institute Of National Colleges Of Technology Japan , Permelec Electrode Ltd , ペルメレック電極株式会社 , 独立行政法人国立高等専門学校機構
发明人： KITAORI NORIYUKI , SEKIDO KOTA , YAMANE GENZO , HAMAGUCHI KATSUMI , TANAKA HOZUMI , NISHIKI YOSHINORI , FURUTA TSUNETO
IPC分类号： C02F1/46 , A61L2/22 , C25B9/00
CPC分类号： C25B11/02 , A61L2/0088 , A61L2/18 , A61L2/183 , A61L2/186 , A61L2202/11 , A61L2202/15 , C02F1/4618 , C02F1/66 , C02F2001/46138 , C02F2001/46152 , C02F2201/003 , C02F2201/46115 , C02F2201/46125 , C02F2305/04 , C25B1/13 , C25B13/02
摘要： PROBLEM TO BE SOLVED: To provide a membrane-electrode assembly for producing electrolytic water dissolving an electrolytic product such as ozone of concentration higher than before, to provide an electrolytic unit, and to provide an apparatus ejecting electrolytic water obtained using them, particularly, a compact spray apparatus spraying the obtained electrolytic water so as to be mist-like. SOLUTION: This invention relates to: the membrane-electrode assembly constituted so that the circumference of a first electrode 7 having a shape of a rod-form or a cylindrical-form is covered with a strip-form diaphragm 8, and a second electrode 9 is installed in the surface of the diaphragm; the electrolytic unit 6 with the membrane-electrode assembly installed in a tube 5; the electrolytic water ejecting apparatus 1 having the electrolytic unit 6, wherein the diaphragm can be easily installed in the electrolytic water ejecting apparatus, and further, when it is fitted in the tube, by adjusting the size of the rod-form electrode, the electrolyte species concentration of the obtained electrolytic water can be set to a desired value. By ejecting or spraying the obtained electrolytic water to an object, sterilization with electrolysis species having a desired concentration is made possible. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种用于生产溶解电解质产物的电解水的膜 - 电极组件，所述电解水溶解比以前高的浓度的臭氧，以提供电解单元，并且提供一种喷射使用它们获得的电解水的装置，特别是将得到的电解水喷雾成雾状的紧凑型喷雾装置。解决方案：本发明涉及：膜电极组件，其构造成使得具有棒状或圆柱形形状的第一电极7的圆周被带状隔膜8覆盖，并且第二电极9安装在隔膜的表面上; 具有膜电极组件的电解单元6安装在管5中; 电解水喷射装置1具有电解单元6，其中隔膜可以容易地安装在电解水喷射装置中，此外，当其安装在管中时，通过调节棒状电极的尺寸，电解质所获得的电解水的物质浓度可以设定为期望值。通过将获得的电解水喷射或喷射到物体上，使具有期望浓度的电解物种的灭菌成为可能。版权所有（C）2008，JPO＆INPIT

4. 发明专利

JP2007070705A Apparatus for synthesizing peroxycarboxylate compound, and synthesizing method 有权
标题翻译：合成过氧羧酸酯化合物的装置及其合成方法
公开(公告)号：JP2007070705A
公开(公告)日：2007-03-22
申请号：JP2005260820
申请日：2005-09-08
申请人： Permelec Electrode Ltd , Tokyo Institute Of Technology , ペルメレック電極株式会社 , 国立大学法人東京工業大学
发明人： OSAKA TAKEO , BEGUM NADIRA FERDOUSI , NISHIKI YOSHINORI , FURUTA TSUNETO
IPC分类号： C25B3/02 , C02F1/46 , C07B61/00 , C07C407/00 , C07C409/24 , C07C409/26
摘要： PROBLEM TO BE SOLVED: To solve a problem that a conventional method for synthesizing a peroxycarboxylate compound with only an electrochemical technique has been an obstacle for industrializing the synthesis because of an insufficient yield.
SOLUTION: This apparatus comprises: an electrolysis cell 1 (21); and a reactor 41 which is installed in the downstream side and accommodates a solid acid-catalytic component. The apparatus supplies a liquid of the peroxycarboxylate compound, unreacted carboxylic acid and hydrogen peroxide, which is produced in the electrolysis cell, to the reactor; makes the solid acid-catalytic component react the unreacted carboxylic acid with hydrogen peroxide to form the peroxycarboxylic acid; and thereby increases the yield as the whole.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：解决的问题为了解决仅由电化学技术合成过氧化羧酸酯化合物的常规方法由于产率不足而成为工业化合成的障碍的问题。解决方案：该装置包括：电解槽1（21）; 以及安装在下游侧并容纳固体酸催化组分的反应器41。该装置将在电解池中产生的过氧化羧酸酯化合物，未反应的羧酸和过氧化氢的液体提供给反应器; 使固体酸催化组分与未反应的羧酸与过氧化氢反应形成过氧羧酸; 从而提高整体的产量。版权所有（C）2007，JPO＆INPIT

5. 发明专利

JP2007039720A Electroconductive diamond electrode and its producing method 有权
标题翻译：电焊金刚石电极及其制造方法
公开(公告)号：JP2007039720A
公开(公告)日：2007-02-15
申请号：JP2005222974
申请日：2005-08-01
申请人： Permelec Electrode Ltd , ペルメレック電極株式会社
发明人： HOSONUMA MASASHI , UNO MASAHARU , SHIBATA TOMOYASU , NISHIKI YOSHINORI , FURUTA TSUNETO
IPC分类号： C25B11/04 , C02F1/461 , C25B11/06 , C25B11/10
CPC分类号： C25B11/0442 , C02F1/46109 , C02F2001/46138 , C23C16/0281 , C23C16/271 , C23C16/278 , Y10T428/12535 , Y10T428/12625
摘要： PROBLEM TO BE SOLVED: To provide an electroconductive diamond electrode excellent in stability, economical advantage and specific strength: and a method for producing the same. SOLUTION: In the electroconductive diamond electrode 1, a metal or alloy coating layer 3 containing at least one of Nb and Ta is formed between an electroconductive base material 2 and an electroconductive diamond layer 4. The metal or alloy coating layer 3 is formed by at least one method selected from the group comprising molten-salt plating, CVD, PVD and brazing. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供稳定性，经济性和比强度优异的导电金刚石电极及其制造方法。解决方案：在导电金刚石电极1中，在导电基材2和导电金刚石层4之间形成含有Nb和Ta中的至少一种的金属或合金涂层3.金属或合金涂层3 通过选自熔融盐电镀，CVD，PVD和钎焊的组中的至少一种方法形成。版权所有（C）2007，JPO＆INPIT

6. 发明专利

JP2006183102A Porous diamond layer, method for producing porous diamond particle and electrode for electrochemistry using them 有权
标题翻译：多孔金刚石层，生产多孔金刚石颗粒的方法和使用它们的电化学电极
公开(公告)号：JP2006183102A
公开(公告)日：2006-07-13
申请号：JP2004378657
申请日：2004-12-28
申请人： Permelec Electrode Ltd , Shinshu Univ , ペルメレック電極株式会社 , 国立大学法人信州大学
发明人： TAKASU YOSHIO , MURAKAMI YASUSHI , SUGIMOTO WATARU , UNO MASAHARU , NISHIKI YOSHINORI , FURUTA TSUNETO
IPC分类号： C25B11/06 , C01B31/06 , C25B11/03 , C25B11/12 , C25C7/02 , C25D17/10 , C30B29/04
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a diamond electrode having fine pores more than those of the conventional diamond layer, and having high electrode activity. SOLUTION: Metallic particles deposited on a diamond layer are heat-treated in a reducing gas atmosphere, thus carbon reduction reaction with the above metal as a catalyst is progressed, and fine pores are formed on the surface of the diamond layer. Since the metal particles carried on the surface of the diamond layer is utilized, the diamond layer and diamond particles in which the fine pores are formed on an atomic level or a level close to the same can be obtained. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种具有比常规金刚石层更多的具有细孔并具有高电极活性的金刚石电极的方法。解决方案：沉积在金刚石层上的金属颗粒在还原气体气氛中进行热处理，因此进行与作为催化剂的上述金属的还原反应，并且在金刚石层的表面上形成细孔。由于使用了金刚石层表面上的金属粒子，所以可以获得在原子级或接近原子级的水平上形成微细孔的金刚石层和金刚石粒子。版权所有（C）2006，JPO＆NCIPI

7. 发明专利

JP2005240074A Electrically conductive diamond electrode and its production method 有权
标题翻译：电导电石墨电极及其生产方法
公开(公告)号：JP2005240074A
公开(公告)日：2005-09-08
申请号：JP2004048460
申请日：2004-02-24
申请人： Permelec Electrode Ltd , ペルメレック電極株式会社
发明人： SHIBATA TOMOYASU , HOSONUMA MASASHI , FURUTA TSUNETO
IPC分类号： C25B11/06 , C02F1/461 , C23C16/02 , C23C16/27 , C25B11/04
CPC分类号： C23C16/278 , C02F2001/46133 , C23C16/02 , C23C16/271 , C25B11/041 , C25B11/0447
摘要： PROBLEM TO BE SOLVED: To solve such a problem that the conventional electrically conductive diamond electrode obtained by coating the surface of an electrode base material with an electrically conductive diamond film, has insufficient adhesion between the base material and the electrically conductive diamond film, thereby causing peeling or the like to invite the shortening of its service life.
SOLUTION: The electrically conductive diamond electrode includes: an electrode base material containing a material selected from valve metals and these metal-based alloys whose surface has been subjected to plastic working and also has been subjected to heating treatment in a vacuum or an inert atmosphere; and an electrically conductive diamond film formed on the plastic-worked face of the electrode base material. When the electrode base material is subjected to the plastic working and heating treatment, the peeling resistance of the electrically conductive diamond film is improved to elongate the service life of the electrode.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：解决的问题为了解决通过用导电金刚石膜涂覆电极基材的表面而获得的常规导电金刚石电极的问题，基材和导电金刚石膜之间的粘附性不足，从而引起剥离等引起其使用寿命的缩短。解决方案：导电金刚石电极包括：电极基材，其包含选自阀金属和这些金属基合金的材料，其表面已经经过塑性加工，并且还在真空中进行了加热处理惰性气氛; 以及形成在电极基材的塑性加工面上的导电金刚石膜。当对电极基材进行塑性加工和加热处理时，改善导电金刚石膜的耐剥离性，延长电极的使用寿命。版权所有（C）2005，JPO＆NCIPI

8. 发明专利

JP2004211182A Electrolytic synthesis method of percarbonic acid compound, and electrolytic synthesis cell 有权
公开(公告)号：JP2004211182A
公开(公告)日：2004-07-29
申请号：JP2003001312
申请日：2003-01-07
申请人： Permelec Electrode Ltd , ペルメレック電極株式会社
发明人： MADOU SUDAN SHAHA , UNO MASAHARU , WAKITA SHUHEI , NISHIKI YOSHINORI , FURUTA TSUNETO
IPC分类号： C01B15/10 , C25B1/28 , C25B1/30 , C25B11/12
摘要： PROBLEM TO BE SOLVED: To provide an electrolytic synthesis method capable of synthesizing a percarbonic acid compound at a high electric current efficiency and an electrolytic synthesis cell used therefor.
SOLUTION: A percarbonic acid compound is synthesized by oxidizing an electrolytic solution 2 containing carbonate ions or bicarbonate ions by using an anode 3 having conductive diamond as an anode substance. Since the water electrolysis overpotential of the conductive diamond anode is high, oxygen generation due to water electrolysis hardly occurs, thus efficiently causing the formation of a percarbonic acid compound due to the anode oxidation of carbonate ions or bicarbonate ions.
COPYRIGHT: (C)2004,JPO&NCIPI

9. 发明专利

JP2004099914A Method for producing peroxodisulfate 审中-公开
公开(公告)号：JP2004099914A
公开(公告)日：2004-04-02
申请号：JP2002259218
申请日：2002-09-04
申请人： Chlorine Eng Corp Ltd , Permelec Electrode Ltd , クロリンエンジニアズ株式会社 , ペルメレック電極株式会社
发明人： KISHI TAKEMICHI , TANAKA HOZUMI , NISHIKI YOSHINORI , SEKIMOTO MASAO , WAKITA SHUHEI , FURUTA TSUNETO
IPC分类号： C01B15/08 , C25B1/28 , C25B11/12
摘要： PROBLEM TO BE SOLVED: To solve the problem that, when a no-diaphragm electrolytic cell with a simple structure is used for producing peroxodisulfate from sulfuric acid ions and/or hydrogen sulfate ions by electrolysis as the conventional method, peroxodisulfate as a product is decomposed by cathode reduction, and current efficiency declines.
SOLUTION: An electrolytic solution 7 comprising sulfuric acid ions and/or hydrogen sulfate ions is electrolyzed in a non-diaphragm electrolytic cell 1 to produce peroxodisulfate. In this case, hexavalent chromium ions are dissolved in the electrolytic solution, so that the reducing decomposition of the resultant peroxodisulfate is suppressed by the hexavalent chromium ions to realize high current efficiency.
COPYRIGHT: (C)2004,JPO

10. 发明专利

JP2007265936A Gas diffusion electrode and its manufacturing method, and fuel cell and electrolytic cell for sodium chloride using the gas diffusion electrode 有权
标题翻译：气体扩散电极及其制造方法，以及使用气体扩散电极的氯化钠的燃料电池和电解槽
公开(公告)号：JP2007265936A
公开(公告)日：2007-10-11
申请号：JP2006092914
申请日：2006-03-30
申请人： Permelec Electrode Ltd , Shinshu Univ , ペルメレック電極株式会社 , 国立大学法人信州大学
发明人： TAKASU YOSHIO , SUGIMOTO WATARU , NISHIKI YOSHINORI , FURUTA TSUNETO
IPC分类号： H01M4/86 , H01M4/88 , H01M4/90 , H01M8/10
CPC分类号： Y02P70/56
摘要： PROBLEM TO BE SOLVED: To solve problems that a conventional gas diffusion electrode increases a manufacturing cost in order to contain platinum as an essential catalyst component and its increase becomes an obstacle of practice use. SOLUTION: A catalyst is constituted of two or more metals and/or metal compounds selected from Ru, Ti, Mo, W, V, Ir, Nb, W, Cu, Ni, La, Ca, Cu, Zr, and Ta. These metals are inexpensive by one digit or more as compared with the platinum, and although oxygen over-voltage is a little inferior to the platinum, the catalyst is stable and has high practicability. COPYRIGHT: (C)2008,JPO&INPIT

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