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1. 发明授权

US4263197A Process for dyeing linear polyamides in the melt 失效
标题翻译：在熔体中染色线性聚酰胺的方法
公开(公告)号：US4263197A
公开(公告)日：1981-04-21
申请号：US79292
申请日：1979-09-27
申请人： Paul Lienhard , Abul Iqbal , Heinz Peter
发明人： Paul Lienhard , Abul Iqbal , Heinz Peter
IPC分类号： C08L77/00 , C08J3/20 , C08K5/00 , C08K5/23 , C08L23/00 , C08L33/00 , C08L33/02 , C08L67/00 , C08L101/00 , C09B45/16 , C09B45/40 , C09B45/48 , C09B69/04 , D01F1/06 , D01F6/90 , D06P3/24
CPC分类号： C09B69/045 , C08K5/0091 , C09B45/482
摘要： A process for dyeing linear polyamides in the melt, in which process there are used salts from 1:2 chromium complexes of monoazo dyes and amines containing 1-18 C atoms.
摘要翻译：用于在熔体中染色线性聚酰胺的方法，其中使用来自单偶氮染料的1：2铬络合物和含有1-18个C原子的胺的盐。

2. 发明授权

US4349671A Process for the production of metal complexes of isoindoline azines 失效
标题翻译：生产异吲哚啉吖嗪金属络合物的方法
公开(公告)号：US4349671A
公开(公告)日：1982-09-14
申请号：US241141
申请日：1981-03-05
申请人： Abul Iqbal , Paul Lienhard
发明人： Abul Iqbal , Paul Lienhard
IPC分类号： C07F15/04 , C07D209/44 , C09B26/02 , C09B57/04 , C07D403/14
CPC分类号： C09B57/04 , C07D209/44 , C09B26/02
摘要： The invention relates to a process for the manufacture of 1:1 metal complexes of azines of the formula ##STR1## wherein R.sub.1 is a hydrogen atom, an alkyl or aryl group, R.sub.2 is an isocyclic or heterocyclic radical containing a hydroxyl or mercapto group adjacent to the azomethine group, Y is the radical of a compound which contains active methylene groups, or of an aryl or heteroaryl amine, and the ring A can contain substituents that do not confer solubility in water, which process comprises reacting a compound of the formula ##STR2## wherein R.sub.3 is a hydrogen atom or an alkyl radical, R.sub.4 is an alkyl, aryl or heteroaryl radical or the radical of the formula ##STR3## or R.sub.3 and R.sub.4, together with the nitrogen atom to which they are attached, form a 5- or 6-membered heterocyclic ring, and Y has the given meaning, with a hydrazone of the formula ##STR4## in the presence of a transition metal donor and in a polar organic solvent, at temperatures above 100.degree. C.Compared with pigments obtained by the prior art methods, the pigments of this invention have greater purity and better fastness properties, especially better fastness to migration, overspraying, light, atmospheric influences and heat.
摘要翻译：本发明涉及一种制备式（Ⅰ）吖嗪的1:1金属配合物的方法，其中R1是氢原子，烷基或芳基，R2是含有羟基的杂环或杂环基，或邻氨基甲基基团的巯基，Y是含有活性亚甲基或芳基或杂芳基胺的化合物的基团，并且环A可以含有不赋予溶于水的取代基，该方法包括使化合物式（II）其中R 3是氢原子或烷基，R 4是烷基，芳基或杂芳基或式（ⅩⅧ）或R 3和R 4基团与其中的氮原子一起在过渡金属供体的存在下，在极性有机溶剂中，在式（III）的腙处，在极性有机溶剂中，连接形成5-或6-元杂环，并且Y具有给定的含义温度高于100℃。与颜料相比通过现有技术方法获得，本发明的颜料具有更高的纯度和更好的牢度性能，特别是更好的耐迁移，过喷，光，大气影响和热的牢度。

3. 发明授权

US4202814A Process for the mass coloration of polyesters 失效
标题翻译：聚酯的大量着色方法
公开(公告)号：US4202814A
公开(公告)日：1980-05-13
申请号：US861327
申请日：1977-12-16
申请人： Paul Lienhard , Abul Iqbal
发明人： Paul Lienhard , Abul Iqbal
IPC分类号： C08L67/00 , C08K5/00 , C08K5/32 , C09B29/08 , C09B31/04 , D01F6/92 , C08K5/23
CPC分类号： C09B31/04 , C08K5/0041 , C08K5/32 , C09B29/08
摘要： A process for the mass coloration of polyesters which comprises the use of a dye of the formula ##STR1## wherein B represents alkylene of 2 to 4 carbon atoms,Y represents cycloalkyl of 5 to 6 carbon atoms, aralkyl of 7 to 14 carbon atoms or a substituted or unsubstituted carbocyclic or heterocyclic aromatic radical,X represents cyanoalkyl of 1 to 5 carbon atoms or --B--OCO--Y, andA represents an aromatic radical of the formula ##STR2## wherein R.sub.1 represents halogen, cyano, trifluoromethyl or alkylsulphonyl of 1 to 4 carbon atoms, and R.sub.2 represents hydrogen or halogen, or represents the groupD--N.dbd.N--D'--in which D and D' represent substituted or unsubstituted phenyl or naphthyl radicals.
摘要翻译：聚酯的大量着色的方法，其包括使用下式的染料（I）其中B表示2至4个碳原子的亚烷基，Y表示5至6个碳原子的环烷基，7至14个的芳烷基碳原子或取代或未取代的碳环或杂环芳族基团，X表示1至5个碳原子的氰基烷基或-B-OCO-Y，A表示下式的芳族基团其中R 1表示卤素，氰基，三氟甲基或1〜4个碳原子的烷基磺酰基，R2表示氢或卤素，或代表DN = N-D'-基团，其中D和D'表示取代或未取代的苯基或萘基。

4. 发明授权

US4460768A Nickel complex pigments of azines 失效
标题翻译：镍复合颜料
公开(公告)号：US4460768A
公开(公告)日：1984-07-17
申请号：US331440
申请日：1981-12-16
申请人： Abul Iqbal , Paul Lienhard , Andre Pugin
发明人： Abul Iqbal , Paul Lienhard , Andre Pugin
IPC分类号： C09B26/02 , C09B57/04 , C07D403/12
CPC分类号： C09B26/02 , C09B57/04
摘要： 1:1 Nickel complexes of azines of the formula I or of a tautomer thereof ##STR1## wherein R.sub.1 is hydrogen or methyl, R.sub.2 is methyl or carbamoyl, R.sub.3 is hydrogen or chlorine, R.sub.4 is hydrogen, chlorine, methyl, trifluoromethyl or sulfamoyl, R.sub.5 is hydrogen or chlorine, R.sub.6 is hydrogen, chlorine, bromine, methyl, methoxy, trifluoromethyl, carbamoyl or alkanoylamino containing 2 to 4 carbon atoms, with the proviso that, if R.sub.2 is carbamoyl, at least two of the substituents R.sub.3 to R.sub.6 are halogen atoms and/or trifluoromethyl groups, color plastics, lacquers and printing inks in orange to red shades of outstanding fastness properties.
摘要翻译： 1：1式I的吖嗪或其互变异构体的镍络合物其中R 1是氢或甲基，R 2是甲基或氨基甲酰基，R 3是氢或氯，R 4是氢，氯，甲基，三氟甲基或氨基磺酰基，R 5是氢或氯，R 6是含有2至4个碳原子的氢，氯，溴，甲基，甲氧基，三氟甲基，氨基甲酰基或烷酰基氨基，条件是如果R 2是氨基甲酰基，则至少两个取代基R 3 到R6是卤素原子和/或三氟甲基，彩色塑料，漆和印刷油墨，具有优异的牢度特性的橙色至红色色调。

5. 发明授权

US4414395A Process for the manufacture of hydrazono-isoindolines 失效
标题翻译：制备肼基 - 异吲哚啉的方法
公开(公告)号：US4414395A
公开(公告)日：1983-11-08
申请号：US241142
申请日：1981-03-06
申请人： Abul Iqbal , Paul Lienhard
发明人： Abul Iqbal , Paul Lienhard
IPC分类号： C07D209/44 , C09B57/04
CPC分类号： C09B57/04 , C07D209/44
摘要： The invention relates to a process for the manufacture of 1-hydrazono-isoindolines of the formula ##STR1## wherein Y is a methine or imine radical and the ring A can contain substituents which do not confer solubility in water, by reacting an iminoisoindoline of the formula ##STR2## with hydrazine or a hydrazine donor, in a polar solvent, which process comprises carrying out the reaction at temperatures below 80.degree. C.These hydrazono-isoindolines are obtained in excellent yield and purity and can be used without further purification as starting materials for further syntheses.
摘要翻译：本发明涉及一种制备下式的1-亚肼基 - 异吲哚啉的方法，其中Y为次甲基或亚胺基，环A可含有不能赋予水溶性的取代基，通过使在极性溶剂中，该方法包括在低于80℃的温度下进行反应。这些亚肼基 - 异吲哚啉以优异的产率和纯度获得，可以不经进一步纯化即可开始使用进一步合成的材料。

6. 发明授权

US4355159A Nickel complex pigments of azines 失效
标题翻译：镍复合颜料
公开(公告)号：US4355159A
公开(公告)日：1982-10-19
申请号：US149406
申请日：1980-05-13
申请人： Abul Iqbal , Paul Lienhard , Andre Pugin
发明人： Abul Iqbal , Paul Lienhard , Andre Pugin
IPC分类号： C09B26/02 , C09B57/04 , C07D403/12
CPC分类号： C09B26/02 , C09B57/04
摘要： 1:1 Nickel complexes of azines of the formula I or of a tautomer thereof ##STR1## wherein R.sub.1 is hydrogen or methyl, R.sub.2 is methyl or carbamoyl, R.sub.3 is hydrogen or chlorine, R.sub.4 is hydrogen, chlorine, methyl, trifluoromethyl or sulfamoyl, R.sub.5 is hydrogen or chlorine, R.sub.6 is hydrogen, chlorine, bromine, methyl, methoxy, trifluoromethyl, carbamoyl or alkanoylamino containing 2 to 4 carbon atoms, with the proviso that, if R.sub.2 is carbamoyl, at least two of the substituents R.sub.3 to R.sub.6 are halogen atoms and/or trifluoromethyl groups, color plastics, lacquers and printing inks in orange to red shades of outstanding fastness properties.
摘要翻译： 1：1式I的吖嗪或其互变异构体的镍络合物其中R 1是氢或甲基，R 2是甲基或氨基甲酰基，R 3是氢或氯，R 4是氢，氯，甲基，三氟甲基或氨基磺酰基，R 5是氢或氯，R 6是含有2至4个碳原子的氢，氯，溴，甲基，甲氧基，三氟甲基，氨基甲酰基或烷酰基氨基，条件是如果R 2是氨基甲酰基，则至少两个取代基R 3 到R6是卤素原子和/或三氟甲基，彩色塑料，漆和印刷油墨，具有优异的牢度特性的橙色至红色色调。

7. 发明授权

US4496727A Process for the manufacture of metal complexes of isoindoline azines 失效
标题翻译：制备异吲哚啉吖嗪金属络合物的方法
公开(公告)号：US4496727A
公开(公告)日：1985-01-29
申请号：US423353
申请日：1982-09-24
申请人： Abul Iqbal , Paul Lienhard
发明人： Abul Iqbal , Paul Lienhard
IPC分类号： C07D209/44 , C07D403/06 , C07D413/06 , C07D417/06 , C09B26/02 , C09B57/04 , C07F1/08 , C07F3/00 , C07F15/00
CPC分类号： C09B57/04 , C07D209/44 , C09B26/02
摘要： The invention relates to a simplified process for the manufacture of 1:1 metal complexes of isoindoline azines of the formula ##STR1## wherein R is hydrogen, alkyl or aryl, Q contains an isocyclic or heterocyclic radical, acyl, carbamoyl or thiocarbamoyl, and Y is the radical of an active methylene group or aromatic amine, which comprises reacting a compound HQ or a hydrazone with an ortho ester or amidine in the presence of a metal donor at elevated temperature in a polar solvent. Pigments made by this process are lightfast and are useful in coloring plastics.
摘要翻译：本发明涉及用于制备式（1）的异吲哚啉吖嗪的1:1金属络合物的简化方法，其中R是氢，烷基或芳基，Q包含一个或多个杂环基，酰基，氨基甲酰基或硫代氨基甲酰基并且Y是活性亚甲基或芳族胺的基团，其包括在金属供体存在下，在高温下在极性溶剂中使化合物HQ或腙与原酸酯或脒反应。通过该方法制备的颜料是耐光的并且可用于着色塑料。

8. 发明授权

US4385174A Isoindoline compounds and the manufacture and use thereof 失效
标题翻译：异二氢吲哚化合物及其制备和应用
公开(公告)号：US4385174A
公开(公告)日：1983-05-24
申请号：US242005
申请日：1981-03-09
申请人： Abul Iqbal , Paul Lienhard
发明人： Abul Iqbal , Paul Lienhard
IPC分类号： C07D209/44 , C07D403/06 , C07D413/06 , C07D417/06 , C09B26/02 , C09B57/04 , C07D403/12 , C07D413/12 , C07D417/12
CPC分类号： C09B57/04 , C07D209/44 , C09B26/02
摘要： The invention relates to a simplified process for the manufacture of 1:1 metal complexes of isoindoline azines of the formula ##STR1## wherein R is hydrogen, alkyl or aryl, Q contains an isocyclic or heterocyclic radical, acyl, carbamoyl or thiocarbamoyl, and Y is the radical of an active methylene group or aromatic amine, which comprises reacting a compound HQ or a hydrazone with an ortho ester or amidine in the presence of a metal donor at elevated temperature in a polar solvent. Pigments made by this process are lightfast and are useful in coloring plastics.
摘要翻译：本发明涉及用于制备式（1）的异吲哚啉吖嗪的1:1金属络合物的简化方法，其中R是氢，烷基或芳基，Q包含一个或多个杂环基，酰基，氨基甲酰基或硫代氨基甲酰基并且Y是活性亚甲基或芳族胺的基团，其包括在金属供体存在下，在高温下在极性溶剂中使化合物HQ或腙与原酸酯或脒反应。通过该方法制备的颜料是耐光的并且可用于着色塑料。

9. 发明授权

US06180315B2 Compositions for making structured color images and application thereof 失效
标题翻译：用于制作结构化彩色图像的组合及其应用
公开(公告)号：US06180315B2
公开(公告)日：2001-01-30
申请号：US09458771
申请日：1999-12-10
申请人： Ulrich Sch{umlaut over (a)}deli , John S. Zambounis , Abul Iqbal , Zhimin Hao , Henri Dubas
发明人： Ulrich Sch{umlaut over (a)}deli , John S. Zambounis , Abul Iqbal , Zhimin Hao , Henri Dubas
IPC分类号： G03C802
CPC分类号： G03F7/105 , B41M3/003 , B41M5/26 , B41M5/265 , B41M5/30 , B41M5/382 , B41M5/5254 , B41M5/5272 , C09B67/0077 , C09B68/443 , C09B68/46 , G03F7/0007 , G03F7/0045 , Y10S430/145 , Y10S430/146 , Y10S430/156 , Y10S430/163 , Y10S430/165
摘要： Novel compositions for making structured color images and application thereof Compositions for making structured color images comprising (a) a soluble pigment precursor which can be transformed to an insoluble pigment by means of chemical, thermal, photolytic or radiation-induced method, and (b) a binder polymer or prepolymer, or a positive or negative resist-type resin which can be structured by crosslinking, polymerization or depolymerization by applying heat or electromagnetic irradiation. The compositions can be applied to optical and thermal recording, printing, and the production of color filters for Liquid Crystal Displays, with high accuracy, high transparency and high stability.
摘要翻译：用于制造结构化彩色图像的新型组合物及其应用用于制备结构化彩色图像的组合物包括（a）可通过化学，热，光解或辐射诱导方法转化为不溶性颜料的可溶性颜料前体，和（b）粘合剂聚合物或预聚物，或正或负的抗蚀剂型树脂，其可以通过施加热或电磁辐射的交联，聚合或解聚来构成。组合物可以应用于光学和热记录，印刷和生产滤色器用于液晶显示器，具有高精度，高透明度和高稳定性。

10. 发明授权

US6120944A Highly transparent, color-pigmented high molecular weight material 失效
标题翻译：高透明度的着色高分子材料
公开(公告)号：US6120944A
公开(公告)日：2000-09-19
申请号：US57089
申请日：1998-04-08
申请人： Ulrich Schadeli , Eric Tinguely , Veronique Hall-Goulle , Heinz Wolleb , Zhimin Hao , Abul Iqbal
发明人： Ulrich Schadeli , Eric Tinguely , Veronique Hall-Goulle , Heinz Wolleb , Zhimin Hao , Abul Iqbal
IPC分类号： G02B5/20 , C08K5/34 , C08L101/00 , C09B29/33 , C09B33/153 , C09B35/035 , C09B67/22 , C09B67/28 , G02B5/22 , G03F1/56 , G03F7/00 , G03F7/105 , G02F1/1335 , G03C1/73
CPC分类号： G03F1/56 , C09B29/338 , C09B33/153 , C09B35/035 , C09B67/0033 , C09B67/0077 , G03F7/0007 , G03F7/105 , G02B5/22
摘要： The invention relates to a color-pigmented high molecular weight organic material structured from a radiation-sensitive precursor by irradiation, the pigmentation of which material consists of extremely fine particles, at least 80 mol % of the pigmentation consisting of a pigment of the class diketopyrrolopyrrole, dioxazine, isoindoline, isoindolinone, disazo condensation yellow or benzimidazolonazo, each containing at least one --NHCO-- group, and, where appropriate, a second pigment of the class diketopyrrolopyrrole, dioxazine, isoindoline, isoindolinone, benzimidazolonazo, disazo or phthalocyanine, and, when the structure of the main pigment is point-symmetrical, the two pigments being present in a balanced molar ratio of from 1:1 to 7:3. Those materials are used preferably in the form of thin layers which are built up in patterns in one or more layers on a transparent substrate and can be used, for example, as optical color filters.
摘要翻译：本发明涉及通过照射由辐射敏感性前体构成的着色着色高分子量有机材料，其颜料由极细颗粒组成，至少80mol％由二酮吡咯并吡咯类颜料组成的色素沉积，二恶嗪，异二氢吲哚，异吲哚啉酮，双偶氮缩合黄或苯并咪唑烷，各自含有至少一个-NHCO-基，以及适当时为二酮吡咯并吡咯，二恶嗪，异二氢吲哚，异吲哚啉酮，苯并咪唑并唑，二偶氮或酞菁的第二颜料，当主颜料的结构是点对称的时，两种颜料的平衡摩尔比为1：1至7：3。这些材料优选地以薄层的形式使用，其以透明基底上的一个或多个层的图案构成，并且可以用于例如光学滤色器。

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